• Bulletin of the Korean Chemical Society
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• 제23권11호
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• pp.1541-1544
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• 2002

The concentration of B in steels is important due to its influence on mechanical properties of steel such as hardenability, hot workability, and creep resistance. An analytical method has been developed to determine B in steel samples by high-resolution inductively coupled plasma mass spectrometry (HR-ICP-MS). National Institute of Standard and Technology Standard Reference Material (NIST SRM) 348a was analyzed to validate the analytical method. The steel sample was digested in a centrifuge bottle with addition of aqua regia and $^{10}B$ spike isotope. Sample pH was then adjusted to higher than 10 to precipitate most matrix elements such as Fe, Cr, and Ni. After centrifugation, the supernatant solution was passed through a cation exchange column to enhance the matrix separation efficiency. B recovery efficiency was about 37%, while matrix removal efficiency was higher than 99.9% for major matrix elements. The isotope dilution method was used for quantification and the determined B concentration was in good agreement with the certified value.

• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2017년도 제48회 춘계학술대회논문집
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• pp.1122-1126
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• 2017

KSLV-II 가속모터는 한국형발사체에 사용하는 단분리모터의 한 종류이며 역추진모터와 동시에 작동하여 단분리를 수행한다. 가속모터의 목표 성능에 맞는 내탄도 설계, 추진제 조성 적용, 연소관 및 경사형 노즐 설계를 수행하였다. 연소관 및 노즐의 소재로 티타늄 합금을 적용하였으며 알루미늄이 다량 함유된 추진제에 대한 내열 성능 확보를 위한 노즐 내열재 소재를 선정하였다. 지상연소시험을 수행하여 KSLV-II 요구조건에 맞는 가속모터의 연소 성능을 확보하였다.

• 한국전기전자재료학회논문지
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• 제32권3호
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• pp.187-191
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• 2019

Advances in laser technology have enabled ultra-high-speed ultra-precise processing, thus expanding potential applications to the semiconductor, medical, and photovoltaic industries. In particular, laser scribing technology has been applied to the production of shingled solar modules. In this work, we analyze the effect of laser scribing conditions, e.g., scribing depth, on the characteristics of the resulting divided solar cells. When the scribing depth was greater than $100{\mu}m$, the solar cells were well separated. In addition, the desired scribing depths were reached in fewer scans when the laser spot overlap was 100%. The efficiency of the divided cells decreased due to the high series resistance at scribing depths of less than $100{\mu}m$. However, at scribing depths of approximately $100{\mu}m$, the series resistance was low and efficiency reduction was minimized.

• 전기화학회지
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• 제2권2호
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• pp.88-92
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• 1999

리튬이온전지용 $LiCoO_2$ 전극의 도전재료인 흑연과 블랙에 대하여 도전재료 함량에 따른 복합체 전극의 겉보기 밀도, 전해액 중에서 집전체로부터 전극복합체의 자기박리 및 전자전도 저항 특성을 조사하였다. $LiCoO_2$복합전극의 겉보기 밀도는 도전재료의 함량 증가에 따라 감소하였으며, 복합체 중 $LiCoO_2$ 단독의 겉보기 밀도는 보다 큰 감소를 나타내었다. $4.7\%w/w$ 이상의 super s black 도전재료를 사용한 전극은 propylene carbonate와 diethyl carbonate의 1: 1 체적비 혼합용매 중의 1 mol/I $LiPF_6$ 전해액 함침으로 자기박리하였으며, 흑연 도전재료에서는 자기박리가 없었다 복합전극의 전자전도에 대한 비저항은 도전재료의 함량 증가에 따라 감소하였으며, super s black도전재료 $2\~3\%w/w$ 함량의 비저항은 Lonza KS6흑연 도전재료 $12\%w/w$ 함량의 비저항과 유사하였다. 본 연구에서 나타낸 범위 내에서 super s black도전재료를 사용할 때 전극 복합체 중의 $LiCoO_2$밀도가 높아 고용량을 나타내었다.

• 전기학회논문지P
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• 제59권4호
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• pp.462-466
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• 2010

The purpose of this study is to evaluate the safety of a wire connector fabricated for the effective installation of a lighting fixture including its contact resistance, insulation resistance, withstanding voltage characteristics, etc., and to provide the basis for the analysis and judgment of PL(Product Liability) dispute by presenting a damage pattern due to a general flame and overcurrent. This study applied the Korean Standard (KS) for the incombustibility test of the connector using a general flame and performed an overcurrent characteristics test of the connector using PCITS (Primary Current Injection Test System). The contact resistance of the housing connector was measured using a high resistance meter and the insulation resistance was measured using a multimeter. In addition, a supply voltage of AC 1,500V for testing the withstanding voltage characteristics was applied to both ends of the connector. Measurement was performed on 5 specimens and the measured values were used as a basis for judgment. Since the connector is fabricated in the form of a housing, it can be connected and separated easily and has a structure that allows no foreign material to enter. In addition, since it has a structure that allows wires to be connected only when their polarity is identical, any misconnection that may occur during installation can be prevented. When the incombustibility test was performed by applying a general flame to the connector, it showed outstanding incombustibility characteristics and the blade and blade holder connected to the housing remained firmly secured even after the insulation sheath (PVC) was completely destroyed by fire. In addition, the mechanism of the damaged connecting wire showed a comparatively uniform carbonization pattern and it was found that some residual melted insulation material was attached to both ends. In the accelerated life test (ALT) to which approximately 500% of the rated current was applied, the connector damage proceeded in the order of white smoke generation, wire separation, spark occurrence and carbonization. That is, it could be seen that the connector damaged by overcurrent lost its own metallic color with traces of discoloration and carbonization. The contact resistance of the connector at a normal state was 2.164mV/A on average. The contact resistance measured after the high temperature test was 3.258mV/A. In addition, the insulation resistance after the temperature test was completed was greater than $10G\Omega$ and the withstanding voltage test result showed that no insulation breakdown occurred to all specimens showing stable withstanding voltage and insulation resistance characteristics.

• 한국지반환경공학회 논문집
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• 제18권7호
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• pp.13-20
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• 2017

쏘일 네일링은 원지반의 전단강도와 네일의 인발 전단 저항력을 이용한 지반 보강 공법이다. 쏘일 네일링 공법은 주로 절취사면, 흙막이 구조물 및 옹벽 보강 등에 사용된다. 흙막이 구조물과 옹벽의 경우 네일의 인발저항만을 고려하여 설계하여도 무방하나, 비탈면의 경우 인발은 물론 전단 및 휨 저항까지 고려하여 설계하여야 한다. 하지만 인발저항만 고려한 보수적인 설계가 이루어지고 있으며, 대부분이 네일의 재료, 형상, 시공방법 등의 개선을 통한 인발저항 증대에 관한 연구이다. 실제 쏘일네일로 보강된 지반은 활동면을 중심으로 전단 휨 변형이 발생하게 된다. 상대적으로 강도가 취약한 그라우트는 파괴되고 보강재와 분리되어 지반은 마찰저항력이 급감하면서 붕괴된다. 따라서 네일과 그라우트체의 분리를 억제하면서 전단저항력을 증가시킬 수 있는 공법개발이 필요한 실정이다. 본 연구에서는 이형철근 외측에 패커를 설치한 후 가압식 그라우팅을 통해 돌기를 형성함으로써 전단저항력을 증대시킬 수 있는 새로운 쏘일 네일링 공법에 대하여 실험적 연구를 수행하였다.

• Advances in nano research
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• 제10권3호
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• pp.211-219
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• 2021

The evaluation of the corrosion resistance of titanium with a TiO2 nanotubes top layer was carried out (TiO2 NT). These nanostructures were evolved into anatase nanoparticles without heat treatment in an aqueous medium, which is a novel phenomenon. This work analyzes the layer between the nanotube bottom and the substrate, which is thin and still susceptible to corrosion. The bottom of TiO2 nanotubes having Fluor resulting from the synthesis process changed between amorphous to crystalline anatase with a crystallite size of about 4 nm, which influenced the corrosion rates. Four kinds of samples were evaluated. A) NT by Ti anodizing; B) NTSB for Ti plates, either modifying its surface or anodizing the modified surface; C) NT-480 for anodized Ti and heat-treated (480℃) for reaching the anatase phase; D) NTSB-480 for Ti plates, first, modifying its surface using sandblast, after that, anodizing the modified surface, and finally, heat-treated to 480℃ to compare with samples having induced crystallization and passivation. Four electrochemical techniques were used to evaluate the corrosion rates. The surfaces having TiO2 nanotubes with a sandblast pre-treatment had the highest resistance to corrosion.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2001년도 봄 학술발표회 논문집
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• pp.757-762
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• 2001

CFT concrete has high flowing, high strength and resistance to material separation to use skyscraper structure. It is considered that concrete could fill the lower part of Diaphragm up. This kinds of CFT concrete hardly apply to building below 20 stories. Using the common use strength concrete to building below 20 stories brings to reduce construction cost. This concrete is needed that valid fluidity and packing ability with unit cement content as common use strength concrete. Offering a fundamental data and proportioning in CFT concrete of below 20 stories, it is executed basic property test, analysis of proportioning and mock up test.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 2002년도 봄 학술발표회 논문집
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• pp.569-574
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• 2002

Generally, the limestone powder is known to have some advantages in rheology of fresh concrete, resistance of material separation, and enhancement of strength at early ages. Recently, great attention is being paid to limestone blended cements in the manufacture of concrete, especially in the countries of Europe. The purpose of the present study is to establish the mechanical and durable properties of concrete containing slag and limestone powder. In this paper, the chloride ion penetration test, rapid carbonation test and rapid freezing-thawing test is carried out to study durability of concrete with various content of limestone powder. Futhermore, the strength of concrete is evaluated with various ages.

• Steel and Composite Structures
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• 제21권3호
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• pp.461-477
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• 2016

Steel-concrete-steel (SCS) sandwich composite wall has been proposed for building and offshore constructions. An ultra-lightweight cement composite with density1380 kg/m3 and compressive strength up to 60 MPa is used as core material and inter-locking J-hook connectors are welded on the steel face plates to achieve the composite action. This paper presents the numerical models using nonlinear finite element analysis to investigate the load displacement behavior of SCS sandwich walls subjected to axial compression. The results obtained from finite element analysis are verified against the test results to establish its accuracy in predicting load-displacement curves, maximum resistance and failure modes of the sandwich walls. The studies show that the inter-locking J-hook connectors are subjected to tension force due to the lateral expansion of cement composite core under compression. This signifies the important role of the interlocking effect of J-hook connectors in preventing tensile separation of the steel face plates so that the local buckling of steel face plates is prevented.