• 대한금속재료학회지
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• 제49권1호
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• pp.1-8
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• 2011

To measure the sensitivity of the hydrogen embrittlement from plated high strength bolts (SWCH18A, F11T), the bolt was stressed by a corresponding to the amount of tensile strain of 5% and 20%, and then the bolt developed a crack on the surface. The bolt that didn't have concentrated hydrogen, even though it was stressed by a corresponding the amount of tensile strain of 5% and 20%, no crack developed. However, the bolt that had concentrated hydrogen, developed cracks from the thread crest to the root. It is impossible to measure the hydrogen amount from plated high strength bolts using Hydrogen-Determinator, because of the limitation of the minimum sample size (about 1g as a mass or $5{\times}5{\times}5 mm^3$ as a volume). Therefore, the sensitivity of hydrogen embrittlement can be measured by observing the presence of cracks on the surface of plated high strength bolts which are stressed by a corresponding to the amount of tensile strain of 5% and 20%.

• International Journal of Internet, Broadcasting and Communication
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• 제15권1호
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• pp.140-144
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• 2023

In recent years, there are so many serious crashes involving coaches, especially the frontal collision occupies 40% of the front of the vehicle, Frontal collisions account for 100% of the front of the vehicle affecting the driver and side-impact collisions that injure the person in the vehicle. Therefore, the research into improving and optimizing the structure is necessary for risk of injury for passengers in frontal accidents. In this paper, we have designed a Shock absorber that can absorb collision energy. Research using HYPERMESH software. to build the finite element model and calculate the meshing to suit the mesh size of 5mm. apply LS-DYNA software to calculate structural strength. In the study, for a vehicle to collide with a hard obstacle occupying 100% of the head of the vehicle. Then, the experimental design method, Minitab is used for find the structural parameters in the design. Improvement results showed that the acceleration of the impact on passengers and the driver is decreased by 55,17%. The mass of texture improvements is reduced by 11%, according to the requirements of European Standards ECE R94.

• Animal cells and systems
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• 제13권3호
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• pp.331-337
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• 2009

Twenty-eight Anopheles species has been so-far identified in Iran, while only 8 species was proved as malaria vector. In this study, we principally examined the cuticular hydrocarbon (CHC) potency in identification of Iranian vectors of malaria and then differentiation of vector and non-vector species of Anopheles. Seven species of malaria vectors and the non-vector species, Anopheles claviger were collected throughout Iran. Female extracts were made out of every five conspecific specimens by surface immersion in pure n-hexane. Each sample was injected into a FID-GC instrument along with the known concentrations of standards. CHC profiles of the eight Anopheles species indicated no qualitative difference. The average mass of each eluted CHC were compared using Repeated ANOVA and Mann-Whitney tests. Results confirmed a significant difference in mass of each single CHC at a specific retention time (RT). Statistical comparison of CHC mass in An. sacharovi, An. stephensi, An. culicifacies and An. fluviatilis at RT 39.6 indicated significant differences (P<0.05) among these species. Analysis of CHC mass of An. dthali, An. superpictus & An. sacharovi at RT 28.5, An. stephensi & An. sacharovi at RT 30.7 and An. sacharovi & An. claviger at RT 30.6 similarly indicated significant differences (P<0.05). An. sacharovi could be distinguished from other species, which showed only trace, by integratable peaks at retention times of 29.7, 31 and 32.6. Similarly, An. claviger could be distinguished from the other species with a trace peak at RT 30.6. In order to separate An. stephensi from the five other species, the integratable peak at RT 30.7 was used. An. dthali could be identified at RT 26.2 by an integratable peak v.s. the trace peaks of other species. An. superpictus had indicator peaks at RTs 27.4 & 28.5 v.s. trace peaks of other species. An. maculipennis with its trace peak at RT 39.6 could be easily differentiated from An. fluviatilis & An. culicifacies. This study proved that all of the examined species of Anopheles could be well identified based on their quantitative differences in CHCs, except for An. fluviatilis & An. culicifacies for which no CHC indicator peak was detected.

• Nutrition Research and Practice
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• 제4권2호
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• pp.128-135
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• 2010

Obesity was characterized in Korean elementary students using different obesity assessment tests on 103 overweight elementary students from three schools of Jeonbuk Province. The body mass index (BMI) and obesity index (OI) were compared, and the data using DEXA and CT were compared with the data using BIA and a tape measure. The results of this study are as follows: first, 27 students who were classified as obese by OI were classified as overweight by BMI, and 3 students who were classified as standard weight by BMI were classified as overweight by OI. Secondly, by DEXA and BIA measurements, there was 1.51% difference in body fat percentage (boys 1.66%, girls 1.17%) and the difference in body fat mass between boys and girls was 0.77 kg (boys 0.85 kg, girls 0.59 kg), but those differences in body fat percentage and mass were not statistically significant. Thirdly, the average total abdominal fat (TAF) measured by CT scans of obese children was more significantly related with subcutaneous fat (r = 0.983, P < 0.01) than visceral fat (r = 0.640, P < 0.01). Also, TAF were highest significant with waist circumference by a tape measure (r = 0.744, P < 0.01). In summary, as there are some differences of assessment results between two obesity test methods (BMI, OI), we need more definite standards to determine the degree of obesity. The BIA seems to be the most simple and effective way to measure body fat mass, whereas waist/hip ratio (WHR) using a tape measurer is considered to be the most effective method for assessing abdominal fat in elementary students.

• 한국터널지하공간학회 논문집
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• 제18권2호
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• pp.235-244
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• 2016

해저터널 시공 중 단층, 파쇄대 및 미고결층 등의 취약한 지반조건에서 일어나는 문제점을 극복하기 위해 시공 중 그라우팅을 진행한다. 암반에서 그라우팅은 주로 불연속면을 따라 주입되므로 절리의 분포, 거칠기 또는 폭과 같은 절리 인자들이 그라우팅 보강암반의 물성에 지대한 영향을 미친다. 해저터널 주변의 그라우팅 보강암반은 해저환경에서 정수압을 다 부담하여 장기적인 열화와 미세구조변화 및 균열 등이 발생하며 암반물성이 시간에 따라 변하므로 그라우팅으로 인한 해저터널 주변암반의 장기적인 거동평가가 요구된다. 본 연구에서는 실내실험을 통해 다양한 축 응력, 양생기간 및 절리조건에서 그라우팅 보강암반의 탄성파 전달특성을 분석하였고 국내에서 사용되는 다양한 암반분류법들의 탄성파 기준을 고려하여 그라우팅 보강암반의 보강정도를 탄성파 속도로 추론하였다.

• 한국방사선학회논문지
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• 제10권8호
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• pp.591-596
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• 2016

본 연구의 목적은 실험으로 6 MV X-선 빔의 등가에너지를 결정하는 데 있다. 6 MV X-선 빔에 대한 납의 반가층은 전리함을 사용하여 측정하였다. 선감쇠계수는 측정된 반가층을 사용하여 계산하였다. 그리고 질량감쇠계수는 납의 밀도로 선감쇠계수를 나누어 얻었다. 얻어진 질량감쇠계수의 등가에너지는 미국표준기술연구소에서 주어진 납의 광자에너지 대 질량감쇠계수 자료를 사용하여 결정하였다. 그 결과로서, 6 MV X-선 빔에 대한 등가에너지는 1.61 MeV로 결정되었다. 이 등가에너지는 Reft가 보고한 것 보다 약 30% 낮게 결정되었다. 그 원인은 납 감쇠기 사이의 공기공동의 존재에 기인한 것으로 추정된다.

• Mass Spectrometry Letters
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• 제5권4호
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• pp.104-109
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• 2014

Nonmedical use of prescription stimulants such as methylphenidate (MPH) and amphetamine (AP) by normal persons has been increased to improve cognitive functions. Due to high potential for their abuse, reliable analytical methods were required to detect these prescription stimulants in biological samples. A direct injection liquid chromatography-tandem mass spectrometric (LC-MS/MS) method was developed and implemented for simultaneous determination of MPH, AP and their metabolites ritalinic acid (RA) and 4-hydroxyamphetamine (HAP) in human urine. Urine sample was centrifuged and the upper layer ($100{\mu}L$) was mixed with $800{\mu}L$ of distilled water and $100{\mu}L$ of internal standards ($0.2{\mu}g/mL$ in methanol). The mixture was then directly injected into the LC-MS/MS system. The mobile phase was composed of 0.2% formic acid in distilled water (A) and acetonitrile (B). Chromatographic separation was performed by using a Capcell Pak MG-II C18 ($150mm{\times}2.0mm$ i.d., $5{\mu}m$, Shiseido) column and all analytes were eluted within 5 min. Linear least-squares regression with a 1/x weighting factor was used to generate a calibration curve and the assay was linear from 20 to 1500 ng/mL (HAP), 40-3000 ng/mL (AP and RA) and 2-150 ng/mL (MPH). The intra- and inter-day precisions were within 16.4%. The intra- and inter-day accuracies ranged from -15.6% to 10.8%. The limits of detection for all the analytes were less than 4.7 ng/mL. The suitability of the method was examined by analyzing urine samples from drug abusers.

• 한국방사선학회논문지
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• 제9권6호
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• pp.375-379
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• 2015

이 연구의 목적은 다종에너지 X선 빔의 유효에너지를 결정하는데 있다. 80 kVp X선 빔에 대한 알루미늄의 반가층은 광자극형광나노닷선량계들(OSLnDs)을 사용하여 측정하였다. 선감쇠계수(${\mu}$)는 측정된 반가층을 사용하여 계산하였다. 그리고 질량감쇠계수(${\mu}/{\rho}$)는 알루미늄의 밀도로 선감쇠계수를 나누어 얻었다. 얻어진 질량감쇠계수의 유효에너지($E_{eff}$)는 미국표준기술연구소(NIST)에서 주어진 알루미늄의 광자에너지들에 대한 X선질량감쇠계수들의 자료를 사용하여 결정하였다. 결과로서, 반가층, 선감쇠계수 및 질량감쇠계수는 각각 2.262 mmAl, $3.06cm^{-1}$, $1.114cm^2/g$이다. 그리고 유효에너지는 29.79 keV에서 결정되었다.

• Mass Spectrometry Letters
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• 제8권3호
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• pp.59-64
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• 2017

In clinical diagnosis, it's well known that the abnormal level of uric acid (UA) in human body is implicated in diverse human diseases, for instance, chronic heart failure, gouty arthritis, diabetes, and so on. As a primary method, an isotope dilution mass spectrometry (IDMS) has been used to obtain the accurate quantity of UA in blood or serum and also develop the certificated reference material (CRM) so as to provide a SI-traceability to clinical laboratories. Due to the low solubility of UA in water, an ammonium hydroxide ($NH_4OH$) has been considered as a promising solvent to increase the solubility of UA that enables the preparation of both UA and its isotope standard solution for next IDMS-based absolute quantification. But, because of using this $NH_4OH$ solvent, it gives rise to the unwanted degradation of UA. In this study, we sought to optimize condition for the stability of UA in $NH_4OH$ solution by varying the mole ratios of UA to $NH_4OH$, followed by ID-LC-MRM analysis. In addition, we also inspected minutely the effect of the storage temperatures. Additionally, we also performed the quantitative analysis of UA in the KRISS serum certificated reference material (CRM, 111-01-02A) with diverse mixing ratios of UA to $NH_4OH$ and then compared those values to its certification value. Based on our experiments, adjusting the mole ratio of 1/2 ($UA/NH_4OH$) with the storage temperature of $-20^{\circ}C$ is an effective way to secure both the solubility and stability of UA in $NH_4OH$ solution for next IDMS-based quantification of UA in serum.

• 분석과학
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• 제30권5호
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• pp.226-233
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• 2017

In general, quantitative chemical analysis in various areas including food, the environment, in vitro diagnostics, etc., requires traceability in order to increase the reliability of the measurements. Measurement traceability is a property of an unbroken chain of comparisons relating an instrument's measurements to SI units. Purity analysis is the first process for establishing traceability to SI units in chemical measurements. The purpose of this study is to develop and validate a method of purity assignment for establishing the traceability of $17{\beta}$-estradiol measurements in an in vitro diagnostics field. The establishment of this method is very important as it can be applied to the development of CRM and to the analysis of the purity of other hormones. The method of assignment of the purity of $17{\beta}$-estradiol was developed using the mass balance method and was validated through participation in an International comparison. In the mass balance method, impurities are categorized into four classes as follows: total related structure impurities, water, residual organic solvents, and nonvolatiles/inorganics. In this study, total related structure impurities were characterized by a gas chromatography-flame ionization detector (GC-FID) and a high-performance liquid chromatography-ultraviolet (HPLC-UV) detector, water content was determined by a Karl-Fisher coulometer, and total residual solvents and nonvolatiles/inorganics were checked simultaneously by thermogravimetric analysis (TGA). The purity of the $17{\beta}$-estradiol was 985.6 mg/g and the expanded uncertainty was 2.1 mg/g at 95% confidence. The developed method can be applied to the development of certified reference materials, which play a critical role in traceability.