• Title/Summary/Keyword: Mass standards

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Determination of Iron, Copper, and Zinc in Rainwater by Ion Chromatography (이온 크로마토그래피법에 의한 강수 중 철, 구리, 아연의 정량)

  • 이용근;이계형;이동수
    • Journal of Korean Society for Atmospheric Environment
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    • v.7 no.2
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    • pp.137-142
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    • 1991
  • A method is developed for the simultaneous determination of dissolved iron, copper, and zinc in rainwater. The method involves 25-fold evaporative concentration, ion chromatographic separation and subsequent spectrophotometric detection after post-column reaction with 4-(2-pyridylazo) resorcinol. Analytical sensitivities, being defined by the slopes of calibration curves, are 0.93, 0.54, and 0.11 Abs/ $\mu$g/ml for iron, copper, zinc, respectively. Detection limits render around a few tenth of one ng/ml. Precisions evaluated by replicate analysis of real sample are better than 10% RSD. Due to the lack of certified standards for rainwater, the accuracy of the method could not be assessed directly. However, the results of this method agree well with those by inductively coupled plasma mass spectrometry. Analytical results for a suite of Seoul rainwaters are presented herein.

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A Study of Operation Performance Prediction Method for the Gasification Melting Furnace (가스화 용융로의 운전성능 예측기법에 관한 연구)

  • Lee, Min-Do;Choi, Sang-Min
    • 한국연소학회:학술대회논문집
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    • 2005.10a
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    • pp.43-49
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    • 2005
  • Social interest and request about low pollution waste treatment process are growing and gasification melting method, as a new technology concept, is risen. The necessity of engineering analysis to determine design standards and operation condition is required. In this study, the objective and function of components and operation process of various gasification melting furnaces such as shaft type, fluidized bed and Rotary Kiln type gasification melting furnace are reviewed and the design standard and operation range of gasification melting furnace are determined by inspecting the change of output and operation condition with input condition change.

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Air Pollution by Automobiles and Ways of Reduction (자동차가 대기오염에 미치는 영향과 저감방안)

  • 김대식
    • Journal of the Korean Professional Engineers Association
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    • v.34 no.4
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    • pp.69-73
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    • 2001
  • Due to the rapid increase of automobiles and daily driving distances, air pollution by automobiles is still dominant problem of large city in spite of strict emission refutation and development of reduction technologies. Among the air pollution resources of automobile , industry. electricity generation and heating. automobile keeps 51% of total nationwide air pollution in 1998 and this proportion Is increasing in large cities from 65% to 85%. To reduce these air pollution. catalytic converter and electronic engine control, exhaust gas re-circulation and evaporative emission control system have continuously developed and applied to automobiles since 1987. Also strong emission standards and emission durability warranty have enforced and monitored annually by sampling several vehicle models. But technologies and regulations are incomplete, driver should participate in reducing air pollution for himself by planning driving, avoiding unnecessary idle and air conditioning, keeping periodic maintenance and using mass transportation.

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Enhanced LTPS Manufacturing Equipment employing Excimer Laser Crystallization

  • Herbst, Ludolf;Simon, Frank;Rebhan, Ulrich;Geuking, Thorsten;Klaft, Ingo;Fechner, Burkhard
    • 한국정보디스플레이학회:학술대회논문집
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    • 2005.07b
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    • pp.1123-1126
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    • 2005
  • For creation of low temperature polycrystallinesilicon (LTPS) the line beam excimer laser annealing (ELA) is a well known and established technique in mass production. With introduction of Sequential Lateral Solidification (SLS) some aspects such as crystalline quality, throughput and flexibility regarding the substrate size could be improved, but for OLED manufacturing still further process development is necessary. This paper discusses line beam ELA and SLS techniques that might enable process engineers to make polycrystalline-silicon (poly-Si) films with a high degree of uniformity and quality as required for system on glass (SOG) and active matrix organic light emitting displays (AMOLED). Equipment requirements are discussed and compared to previous standards. SEM images of process examples are shown in order to demonstrate the viability.

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DEVELOPMENT OF POINT KERNEL SHIELDING ANALYSIS COMPUTER PROGRAM IMPLEMENTING RECENT NUCLEAR DATA AND GRAPHIC USER INTERFACES

  • Kang, Sang-Ho;Lee, Seung-Gi;Chung, Chan-Young;Lee, Choon-Sik;Lee, Jai-Ki
    • Journal of Radiation Protection and Research
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    • v.26 no.3
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    • pp.215-224
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    • 2001
  • In order to comply with revised national regulationson radiological protection and to implement recent nuclear data and dose conversion factors, KOPEC developed a new point kernel gamma and beta ray shielding analysis computer program. This new code, named VisualShield, adopted mass attenuation coefficient and buildup factors from recent ANSI/ANS standards and flux-to-dose conversion factors from the International Commission on Radiological Protection (ICRP) Publication 74 for estimation of effective/equivalent dose recommended in ICRP 60. VisualShieid utilizes graphical user interfaces and 3-D visualization of the geometric configuration for preparing input data sets and analyzing results, which leads users to error free processing with visual effects. Code validation and data analysis were performed by comparing the results of various calculations to the data outputs of previous programs such as MCNP 4B, ISOSHLD-II, QAD-CGGP, etc.

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A Study on the Precision Processing of Thin Stamper with Global Area (대면적 박판 스탬퍼 정밀 가공을 위한 연구)

  • 최두선;제태진;서승호
    • Proceedings of the Korean Society of Precision Engineering Conference
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    • 2003.06a
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    • pp.632-635
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    • 2003
  • As a process technology of nano pattern with a new conception for economic and practical technology of alternative nano process. process technologies such as Embossing, Imprinting. Molding and Inking are beginning to make its appearance. Among these alternative processes, nano mold process is a process that is of benefit to mass production and keeps excellency of reproduction and high quality of parts. In this study, we experienced micro precision machining technology of nano stamper for the injection mold of optical disk with big capacity. Especially, Flatness and uniformity are important for nano stamper with global area, for the purpose of developing polishing technology of micro precision of Back polishing only being used for nano stamper, we carried out a basic study to secure flatness standards

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Use of Lycopene, an Antioxidant Carotinoid, in Laying Hens for Egg Yolk Pigmentation

  • Kang, D.-K.;Kim, S.-I.;Cho, C.-H.;Yim, Y.-H.;Kim, H.-S.
    • Asian-Australasian Journal of Animal Sciences
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    • v.16 no.12
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    • pp.1799-1803
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    • 2003
  • The possibility of lycopene affecting egg yolk pigmentation was studied with lycopene diets containing 0, 4, 8, and $12{\mu}g/g$ meal, respectively. The addition of lycopene above $4{\mu}g/g$ meal significantly improved yolk color after four days of supplementation. The transfer of lycopene into egg yolk was confirmed by thin layer chromatography, and high-performance liquid chromatography-mass spectrometry (HPLC-MS). The deposition rate of lycopene into egg yolk was approximately 2%, which was quantitatively determined using a HPLC with a UV detector. The result indicates that lycopene is a good candidate for egg yolk pigmentation and for making functional eggs.

Setup and Atomic Calibration of Particle Induced X-ray Emission System

  • Song, Jin-Ho;Song, Jae-Bong;;Kim, Jun-Gon
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.206.2-206.2
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    • 2014
  • Recently, particle induced X-ray emission (PIXE) analysis system was installed at the 2MV ion acceleration system in Korea institute science and technology (KIST). This installation is for complement to low atomic resolution of heavy atoms at Rutherford backscattering spectrometry (RBS) system. For quantitative analysis, a mass calibration of the PIXE set-up has been done with thin film standards and. The GUPIX software package has been used to process the PIXE spectra and the results are compared with the values from RBS system. Therefore, the instrumental constant H (solid angle and correction factor) is determined relying completely on the GUPIX data base (cross-sections, fluorescence and Coster-Kronig probabilities, stopping powers and attenuation coefficients) for a large set of elements. These H values can be used in future analysis.

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Some Way for Three-phase Induction Motors Electromagnetic Noise Reduction

  • Sarbu, Mircea A.
    • Journal of KSNVE
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    • v.13 no.2
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    • pp.119-128
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    • 2003
  • Abstract Increasing awareness of industrial noise pollution and emerging stricter standards have made noise an important topic of research in electric motors. The standard three-phase induction motors. see Fig. 1, (abbreviated further as TPIM) are mass-produced as being simple, robust and rather inexpensive, as opposed to other types of electric motors. Electric motors use over half of all electricity consumed in most countries. Typically motors consume 60∼80 % of the electricity for those used In the industrial sector and about 20∼35 % of the electricity for those used in the commercial sector. For that is important to know their participation to the noise pollution of the environment and the efficient ways of their noise reduction. Each step in determining the ways for TPIM electromagnetic noise reduction including the methods that highlight their efficiency, are presented and explained.

Analysis of Agrochemical Residues in Tobacco Using QuEChERS Method by GC-MS/MS

  • Lee, Jeong-Min;Jang, Gi-Chul;Hwang, Keon-Joong
    • Journal of the Korean Society of Tobacco Science
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    • v.29 no.2
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    • pp.132-139
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    • 2007
  • This study was performed to apply the more rapid and accurate sample preparation, and the high selectivity and sensitivity of the analyte detection by gas chromatography-triple quadrupole mass spectrometry (GC-MS/MS). QuEChERS (quick, easy, cheap, effective, rugged and safe) method was validated for 49 agrochemicals in the CORESTA Agrochemical Advisory Committee guide and amenable to GC-MS/MS determination. In QuEChERS method, the effects of sorbents (PSA, $C_{18}$ and GCB) and matrix of the analytes in tobacco types (flue-cured, burley and oriental) were investigated. MS/MS acquisition provided high specificity and selectivity for agrochemicals and low limit of quantification. QuEChERS by using PSA alone and the matrix-matched standards gave good recoveries and RSD values in three types of tobaccos. QuEChERS method was no needed to be complex clean-up procedure and would be used as the fast and easy method for agrochemical residue analysis in tobacco.