• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2016년도 추계학술대회 논문집
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• pp.195-195
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• 2016

Titanium and its alloys are widely used as implants in orthopedics, dentistry and cardiology due to their outstanding properties, such as high strength, high level of hemocompatibility and enhanced biocompatibility. Hence, recent works showed that the synthesis of new Ti-based alloys for implant application involves more biocompatible metallic alloying element, such as, Nb, Hf, Zr and Mo. In particular, Nb and Hf are one of the most effective Ti ${\beta}-stabilizer$ and reducing the elastic modulus. Plasma electrolyte oxidation (PEO) is known as excellent method in the biocompatibility of biomaterial due to quickly coating time and controlled coating condition. The anodized oxide layer and diameter modulation of Ti alloys can be obtained function of improvement of cell adhesion. Silicon (Si) and magnesium (Mg) has a beneficial effect on bone. Si in particular has been found to be essential for normal bone and cartilage growth and development. In vitro studies have shown that Mg plays very important roles in essential for normal growth and metabolism of skeletal tissue in vertebrates and can be detected as minor constituents in teeth and bone. The aim of this study is to research Si and Mg doped hydroxyapatite film formation by plasma electrolytic oxidation. Ti-29Nb-xHf (x= 0, 3, 7 and 15wt%, mass fraction) alloys were prepared Ti-29Nb-xHf alloys of containing Hf up from 0 wt% to 15 wt% were melted by using a vacuum furnace. Ti-29Nb-xHf alloys were homogenized for 2 hr at $1050^{\circ}C$. Each alloy was anodized in solution containing typically 0.15 M calcium acetate monohydrate + 0.02 M calcium glycerophosphate at room temperature. A direct current power source was used for the process of anodization. Anodized alloys was prepared using 270V~300V anodization voltage at room. A Si and Mg coating was produced by RF-magnetron sputtering system. RF power of 100W was applied to the target for 1h at room temperature. The microstructure, phase and composition of Si and Mg coated oxide surface of Ti-29Nb-xHf alloys were examined by FE-SEM, EDS, and XRD.

• 한국산학기술학회논문지
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• 제20권12호
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• pp.513-518
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• 2019

마찰교반용접(Friction Stir Welding) 기술은 금속 소재를 대상으로 하는 용접기술 중의 하나로 용접대상이 되는 소재와 고속으로 회전하는 용접툴 사이의 마찰로 인한 열을 활용하여 소재의 융점 이하 온도에서 접합하는 기술이다. 이번 연구에서는 마찰교반용접을 진행할 때, 용접 대상물의 내부 온도 변화를 분석하기 위한 방법으로 수치해석기법을 사용하였다. 용접소재로는 마그네슘 합금인 AZ31을 고려하였으며, 용접현상을 멜팅풀(melting-pool)이 생성되는 유동특성으로 간주하고 유동해석을 수행하기 위해 유동특성 수치해석 툴인 FLUENT를 이용하였다. 용접과정의 유동해석을 진행하기 위해 용접소재는 고점도 뉴턴 유체로 가정하였고, 용접툴과 용접대상 소재의 경계면은 마찰 및 미끄러짐이 동시에 발생하는 조건으로 경계조건을 선정하였다. 그리고 용접툴의 회전속도 및 용접속도를 변수로 하여 다양한 해석을 진행하였다. 해석 결과로부터 용접툴의 회전속도가 높을수록, 용접속도가 느릴수록 소재 내 최고온도가 증가함을 확인할 수 있었으며, 그 중 용접툴의 회전속도 차이가 온도 변화에 더 큰 영향을 보임을 확인하였다.