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Partisil/Partisphere 이온 교환 컬럼 재생 가이드 (Column regeneration for Partisil/Partisphere ion-exchange columns)

  • Mark Fever;Gemma Howse
    • FOCUS: LIFE SCIENCE
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    • 제1호
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    • pp.5.1-5.3
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    • 2024
  • The document discusses the regeneration of Partisil/Partisphere ion-exchange columns in chromatography. It mentions that column efficiency can diminish with use due to the accumulation of sample and/or mobile phase impurities at the head of the column. This can lead to a change in back pressure, lower column efficiency, and sometimes a change in selectivity. The document outlines a procedure that may restore column performance. The document also provides everyday practices to enhance the lifetime of a column. These include using only high-purity HPLC solvents and buffers, using freshly prepared mobile phases and buffers, filtering mobile phases to remove particulates, using appropriate sample clean-up procedures, using a guard column or pre-column filter, and working within the pressure and flow rate limitations of the column. For the regeneration of Partisil/Partisphere SAX, SCX, WAX, and WCX columns, the document suggests passing 20 column volumes of various mobile phases through the column. These include a buffer wash, distilled water, an acid wash, a chelating wash, a methanol wash, and a buffer for separation. The document emphasizes that not all of these wash steps are required for every column clean-up and that some chromatographers require only a combination of certain steps.

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119구조·구급대원의 직업만족도에 관한 연구 -전국을 대상으로- (A study on 119 Rescue and First aids' satisfaction level of Occupation)

  • 김순심;권혜란
    • 한국응급구조학회지
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    • 제6권1호
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    • pp.169-184
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    • 2002
  • The purpose of this study was to find out the 119 rescue and first aid's satisfaction level for their occupations, understand the influential factors of the satisfaction level and also analyze the level of each working districts. Therefore to provide basic information of policy decisions to increase the satisfaction level. Date were collected from 400 national the 119 rescue and first aids by questionnaire and using the tools, which has developed by Slavitt, from August 2 to September 30, 2002. The data were analyzed by percentage, mean t-test and ANOVA. Divided 39 items into 7 provinces to find out the satisfaction level of each province, follow as the influential factors of the satisfaction level. 1. The most of the 119 rescue and first aids were satisfying about their occupations as they got 3.02 marks out of 5, which is the full mark. 2. As the results after analyzed the relation ship between the satisfaction level and the general characteristics of analyzed the relation ship between the satisfaction level and the general characteristics of the 119 rescue and first aids, there were not statistically significant differences of sex distinction, age, scholarship, not married and has or have married, grade and qualification. There were statistically significant differences follow as working period, applying motive, moving, seeking a job, working place, an adviser, work overtime and compensation follow as work overtime. 3. It appeared that all the 119 rescue and first aids were satisfying enough about duty itself but were dissatisfying about working condition. As the results; job itself got 4.00, reciprocal action got 3.74, business demand got 3.28, autonomy got 3.06, organization demand got 2.96, pay got 2.43 and working condition got 1.72, each out of 5 full marks. As you see the results, most of the 119 rescue and first aids are satisfying about a job itself but they are dissatisfying about their working condition. Therefore we should formulate a plan that can increase the satisfaction level by improving duty system for 24 working hours per week.

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대전지역 주부의 친환경농산물 구매행동 (The Housewives' Purchase Behaviors on Environment-friendly Agricultural Products in Daejeon Area)

  • 김인정;이준호
    • 대한지역사회영양학회지
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    • 제16권3호
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    • pp.386-397
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    • 2011
  • This study was to investigate the housewives' purchase behaviors on the environment-friendly agricultural products (EFAP) by survey in Daejeon area housewives. 390 questionnaires were used and analysed. Most of the subjects were female (92.6%) distributed evenly in their 40's (55.4%), and graduated from high school (43.6%) or college (36.4%). Subjects' occupation was most housewives (64.1%) and 77.4% of the subjects had monthly family income of 2 million won or more. 76.9% of the subjects had purchased EFAP already. The reason of purchasing EFAP was mainly "good for health" (80.3%), and reason for non-purchasing was "high prices" (28%) or "not so trustworthy" (25.6%). The most purchasing frequency was "once a week" (29%). 46.7% of the subjects spent 20% of their agricultural product cost for EFAP and 38.7% of them spent less than 30,000 won per month for EFAP. On checking of EFAP labeling, the housewives scored 3.59 for the validate date, 3.25 for the place of origin, 2.8 for the quality certification mark by 4-point Likert scale. 65.1% of the subject had intention to increase purchasing of EFAP in future. To promote the consumption of EFAP, the improvement factors were price-cutting (47.9%), trust on producers (18.2%) and quality betterment (17.7%). Accordingly, the consumers prefer EFAP for wellbeing health of families; however, they hesitate to buy due to their high price and the low reliability on producers of EFAP. Thus the producers and the related organization of EFAP should contrive proper countermeasures to increase consumer's satisfaction level on their credibility and price of EFAP.

임플란트 식립 초기 의원성 동요가 최종 골결합에 미치는 영향 (The influence of iatrogenic mobilization in the initial stage of implant installation on final osteointegration)

  • 곽명배;조진현;이두형;이청희
    • 대한치과보철학회지
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    • 제52권2호
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    • pp.105-112
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    • 2014
  • 연구 목적: 이 연구의 목적은 임플란트 식립 초기 수회의 의원성 동요가 최종 골결합에 미치는 영향을 확인하는 것이다. 연구 재료 및 방법: 순수한 티타늄(Grade IV) 으로 직경 3.75 mm, 길이 8 mm의 실험용 임플란트를 제작한 후, 하방 4 mm에 RBM 표면처리($MegaGen^{(R)}$: Ca-P)를 하였다. 임플란트의 하부만 골에 식립되었으며 비침하시켰다. 수술은 3.5 kg이상의 토끼의 좌우 경골의 단층 치밀골에 각각 2개씩 130개를 통상적인 방법으로 식립하였다(Female, New Zealand White). 비틀림 제거 간격에 따라, 다음과 같은 13개의 군으로 나누었다; Group I (1일), Group II (1일 + 2일), Group III (1일 + 2일 + 3일), Group IV (1일 + 2일 + 3일 + 4일), Group V (2일), Group VI (2일 + 4일), Group VII (2일 + 4일 + 6일), Group VIII (2일 + 4일 + 6일 + 8일), Group IX (4일), Group X (4일 + 7일), Group XI (4일 + 7일 + 10일), Group XII (4일 + 7일 + 10일 + 14일), 그리고 대조군. 대조군은 식립 후 8주의 치유기간을 준 후 최종 비틀림 제거력을 측정하였다(Mark-10, USA). 실험군은 각각의 조건에 맞추어 1회에서 4회에 걸쳐 비틀림 제거력을 측정하였다. 비틀림 제거력을 측정한 이후에 대체적으로 임플란트를 측정 전의 위치로 재위치시켰다. 모든 실험군에서 임플란트 식립 후 8주간의 치유기간을 준 다음 최종 비틀림 제거력을 측정하여 대조군, 각 실험군의 1, 2, 3, 4번째 비틀림 제거력과 비교하였다. 결과: 실험군 간에 최종 비틀림 제거력을 비교한 결과에서, XII군을 제외한 실험군의 비틀림 제거력은 대조군과 유의할만한 차이를 보이지는 않았다. 그리고 실험 I군과 II군의 값은 VI, VIII, X, XI, XII군의 값보다 유의하게 높게 나타났다. 그리고 III, IV, V군은 XI, XII군의 값보다 유의하게 높게 나타났다. 각 실험군간 비틀림 제거력 비교에서, 최종 비틀림 제거력은 VIII, X, XI, XII군을 제외한 모든 군에서 높게 나타났다. 결론: 충분한 치유기간이 주어진다면, 토끼에게 임플란트 식립 후 매우 이른 초기에 지대주에 가해지는 약간의 동요는 임플란트 골결합에 영향을 미치지 않았다.

A Modified, Direct Neck Lift Technique: The Cervical Wave-Plasty

  • Parsa, Fereydoun Don;Castel, Nikki;Parsa, Natalie Niloufar
    • Archives of Plastic Surgery
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    • 제43권2호
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    • pp.181-188
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    • 2016
  • Background Major problems with cervicoplasty by direct skin excision include the subjective nature of skin markings preoperatively and the confusing array of procedures offered. This technique incorporates curved incisions, resulting in a wave-like scar, which is why the procedure is called a "wave-plasty". Methods This prospective study includes 37 patients who underwent wave-plasty procedures from 2004 to 2015. Skin pinching technique was used to mark the anterior neck preoperatively in a reproducible fashion. Intra-operatively, redundant skin was excised, along with excess fat when necessary, and closed to form a wave-shaped scar. Patients were asked to follow up at 1 week, 6 weeks, and 6 months after surgery. Results The mean operation time was 70.8 minutes. The majority (81.3%) was satisfied with their progress. On a scale of 1 to 10 (1 being the worst, and 10 being the best), the scars were objectively graded on average 5.5 when viewed from the front and 7.3 when seen from the side 6 months after surgery. Complications consisted of one partial wound dehiscence (2.3%), one incidence of hypertrophic scarring (2.3%), and two cases of under-resection requiring revision (5.4%). Conclusions In select patients, surgical rejuvenation of the neck may be obtained through wave-like incisions to remove redundant cervical skin when other options are not available. The technique is reproducible, easily teachable and carries low morbidity and high patient satisfaction in carefully chosen patients.

FASTENER HOLE 모델의 대한 예비압입 적용 연구 (A Study on the Application of Pre-Indentation Technique for Fastener Hole Model)

  • 황정선;조환기
    • 한국항공우주학회지
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    • 제31권9호
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    • pp.26-31
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    • 2003
  • 노후 항공기는 일반적으로 다중손상(MSD)이라고 하는 폭넓게 분포된 피로손상을 내포하고 있다. 2024-T3 알루미늄합금과 같은 연성재료에 있어서 다중손상은 전통적인 파괴역학에서 예측할 수 있는 것보다 낮은 운용수명을 예측하게 만드는 것으로 알려져 있다. 본 논문에서는 다중손상을 갖는 평판 구조물을 모델링한 Fastener Hole을 갖는 2024-T3 알루미늄합금 판재로 제작된 Hole/Slot type M(T) 시편에 예입압입을 적용한 후 피로시험을 수행하여 피로균열 성장지연에 의한 운용수명 증가에 대한 효과를 연구하였다. 예비압입을 적용한 시편은 파단에 이르는 사이클수가 최소 10배에서 최대 40배까지 증가하였으며, 일정진폭 하중의 최대값을 증가시킴에 따라서 그 효과가 감소함을 보여주었다. 또한, 압입에 의한 균열성장지연 메커니즘은 균열진전경로가 압입자국에 들어서면서 균열성장률이 감소하기 시작하며 압입자국의 중심을 지나면서 최소균열성장률 상태로 일정한 시간동안 균열성장이 정체됨으로써 피로수명이 연장됨을 밝혔다.

Optimizing and Modeling Brightness Development in Peroxide Bleaching of Thermomechanical Pulp

  • Yoon, Byung-Ho;Wang, Li-Jun;Park, Soo-Kyoung;Kim, Dong-Yoon
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 1999년도 추계학술발표논문집
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    • pp.180-186
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    • 1999
  • Alkaline peroxide bleaching of (chemi) mechanical pulp is a very complicated system where various process factors affect the bleaching performance and pulp properties. Traditional on-factor-at a time method is ineffective and costly in finding the optimal bleaching conditions. In this study statistical experimental methods which include three steps. I. e. screening, response surface modeling and optimization, were used to find the conditions for maximal brightness development during one stage alkaline peroxide bleaching of TMP which had an initial brightness of 54.5% Elerpho. The TMP was pretreated with EDTA(0.5% on O. D. pulp. consistency, $30^{\circ}C$ for 60 minutes) and bleached in a 2L Mark V Quantum Reactor at 750rpm, 7.5% of bleaching consistency and with 0.05% magnesium sulfate addition. The ranges of other factors studied were 1~5% hydrogen peroxide on O. D plup, 1~4% sodium hydroxide on O. D pulp and 1~4% sodium silicate on O. D pulp, reaction temperature 50~$90^{\circ}C$ and reaction time 40~180minutes. A models with good predictability was established and the maximal brightness after one stage bleaching was found to be 70% Elerpho at $50^{\circ}C$, 50 minutes 5% hydrogen peroxide on O. D. pulp 3.2~3.4% sodium hydroxide on O. D. pulp 3.2~3.4% sodium hydroxide on O. D pulp and 4% silicate on O. D pulp. However further studies on other pulp properties such as strength and brightness stability shall be carried out in order to find out the optimal bleaching conditions.

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Crosserase와 crosstalk이 DVD 재생 신호에 미치는 영향 (Crosserase and Crosstalk Effects on Readout Signal of Digital Versatile Disks)

  • 박연수;김지원;조순철
    • 전자공학회논문지CI
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    • 제38권4호
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    • pp.33-38
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    • 2001
  • 고밀도 기록매체인 DVD RAM 시스템에서 단면 기록밀도 4.7 GB, 15 GB 매체 개발 실현에 가장 큰 걸림돌로 작용하고 있는 crosserase 및 crosstalk 현상이 재생 신호에 미치는 영향을 분석하기 위해 4.7 GB 및 15 GB 규격으로 재생 신호를 시뮬레이션 하였다. 디스크에 조사된 빔의 강도는 Gaussian으로 근사화하고 기록된 마크는 타원형 마크로 가정하였으며, 재생신호는 Gaussian 빔 패턴과 마크 패턴의 이중 적분으로 계산되었다. Crosserase 정도를 변하여 얻어진 재생 신호로부터 주파수 분석을 통하여 3T-11T 마크의 carrier level의 크기를 구하여 비교하였다. 1,000개의 3T-11T 랜덤 마크로 부터 crosserase 및 crosstalk 에 의한 지터를 계산하여 비교한 결과, crosserase에 의한 지터가 crosstalk에 의한 지터 보다 상대적으로 작음을 확인할 수 있었다.

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Studies on Anopheles sinensis, the vector species of vivax malaria in Korea

  • REE Han-Il
    • Parasites, Hosts and Diseases
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    • 제43권3호
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    • pp.75-92
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    • 2005
  • Extensive previous studies on taxonomy, behavior/bionomics and control of Anopheles sinensis are reviewed and summarized. Recent molecular identification revealed that the population of An. sinensis complex includes An. sinensis, An. pullus, An. lesteri and at least two new species, and An. yatsushiroensis is synonmy of An. pullus. An. sinensis is the main vector specie of vivax malaria in Korea. Larvae of An. sinensis breed in wide range of habitats which are naturally-made clean water, stagnant or flowing; main habitats include rice fields, ditches, streams, irrigation cannals, marshes, ponds, ground pools, etc. Their host preferences are highly zoophilic. Human blood rate is very low ($0.7-1.7\%$); nevertheless An. sinensis readily feeds on man when domestic animals are not found near by. They feed on hosts throughout the night from dusk to dawn with a peak period of 02:00-04:00 hours; they are slightly more exophagic (biting outdoors); much larger numbers come into the room when light is on. Main resting places are outdoors such as grasses, vegetable fields and rice fields. A mark-release-recapture study resulted that $37.1\%$ was recaptured within 1 km, $29.4\%$ at 1-3 km, $21.1\%$ at 3-6 km, $10.3\%$ at 6-9 km and $2.1\%$ at 9-12 km distance. An. sinensis hibernate outdoors (mostly under part of dense grasses) during October-March. At the end of the hibernation period (March-April) they feed on cows at daytime. Until today any single measure to effectively control An. sinensis population has not been found. Indoor residual spray with a long-lasting insecticide can not reduce vector population densities, but shorten their life spans in some degree, so contributes to malaria control.

제주도의 GPS/Levelling 지오이드와 PNU95 지오이드 (Comparison of GPS/Levelling Geoid with PNU95 Geoid in Cheju Island)

  • 최광선;박재희;홍순헌
    • 지구물리
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    • 제3권1호
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    • pp.13-24
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    • 2000
  • 제주도 내의 13개의 수준점에서 GPS를 측정하였으며, 이에 의한 GPS/Levelling 지오이드와 PNU95 지오이드를 비교, 분석하여 보았다. GPS의 측정결과 각. 수준점의 타원체 높이를 ${\pm}3\;cm$ 이내의 정밀도로 측정하였다. 계산된 GPS/Levelling 지오이드는 제주도의 지형 변화를 잘 나타내고 있으며, 제주도에서 지오이드와 지형의 상관식은 다음과 같다. $$N\;=\;0.001082\;{\times}\;h\;+\;25.458\;{\pm}\;0.227\;s.d.$$ 계산된 GPS/Levelling 지오이드와 PNU95 지오이드는 잘 일치하고 있으며 두 지오이드의 RMS 차이는 0.14 m이다.

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