• Title/Summary/Keyword: Low temperature treatment

검색결과 1,963건 처리시간 0.032초

Study for Heat Treatment Optimization of Titanium Hollow Casted Billet (타이타늄 중공마더빌렛 주조재의 열처리공정 최적화 연구)

  • Youn, Chang-Suk;Park, Yang-Kyun;Lee, Hyung-Wook;Lee, Dong-Geun
    • Journal of the Korean Society for Heat Treatment
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    • 제32권2호
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    • pp.68-73
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    • 2019
  • ${\alpha}$-titanium alloy has a relatively low heat treatment characteristic and it is mainly subjected to heat treatment for residual stress, recovery or dynamic recrystallization. In this study, commercially pure titanium hollow castings was fabricated by gravity casting. Heat treatments were carried out at $750^{\circ}C$, $850^{\circ}C$ and $950^{\circ}C$ to investigate the effect of post-heat treatment on microstructure and mechanical properties. Beta-transus temperature ($T_{\beta}$) was about $913^{\circ}C$, and equiaxed microstructure was shown at temperature below $T_{\beta}$ and lath-type microstructure at temperature above $T_{\beta}$. Microstructure and mechanical properties did not show any significant difference in the direction of solidification for titanium hollow billet, so it can be seen that it was a well-made material for extrusion process. The optimum heat treatment condition of hollow billet castings for the seamless tube production was $850^{\circ}C$, 4 hr, FC, indicating a combination of equiaxed microstructure and appropriate mechanical properties.

PL Study on ZnO Thin Films After H-plasma Treatment (수소 플라즈마 처리를 거친 ZnO 박막에 대한 PL 연구)

  • Cho, Jaewon;Rhee, Seuk Joo
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • 제28권1호
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    • pp.17-20
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    • 2015
  • The physical effects of H-plasma treatment on ZnO thin film have been studied using photoluminescence(PL) spectroscopy. Four characteristic peaks have been identified: (i) $D^0X$ peak (neutral donor-bound exciton), showing relatively small integrated intensity after H-plasma treatment, indicates that H-plasma passivates the neutral donors in ZnO at low temperatures. The rapid decrease in the integrated intensity of the peak as the temperature goes up is considered to be due to the ionization of neutral donors. (ii) H-related complex-bound exciton peak appears at the low temperatures (10 K~80 K) after H-plasma treatment, showing the same thermal evolution as $D^0X$ peak. (iii) FX (free exciton) peak starts to show up at 60 K and grows more and more as the temperature goes up, which is considered to be related to the increase in free electron concentration in the film. (iv) violet band is intensified after H-plasma, which means more defects and impurities are generated by H-plasma process.

Morphology control of blue-emitting BAM phosphor particles by the spray pyrolysis (분무열분해법에 의한 푸른색 발광 BAM 형광체 분말의 형태 조절)

  • 강윤찬;노현숙
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 한국전기전자재료학회 1999년도 추계학술대회 논문집
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    • pp.566-569
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    • 1999
  • The blue emitting BAM Phosphor Particles with various compositions were Prepared by the spray Pyrolysis. The effect of composition on the morphology of BAM particles was Investigated. In the case of BaMgAl$_{10}$ /O$_{22}$ : Eu$^{2+}$, the morphology of particles with sphericity and non-aggregation characteristics disappeared after post-treatment at 1400 $^{\circ}C$ for 3 hrs. On the other hand, the ocher composition particles except BaMgAl$_{10}$ /O$_{22}$ : Eu$^{2+}$ maintained their original morphology after post-treatment, even if the particles were prepared at low temperatures in the spray pryrolysis. The BAM particles with MgAl$_{2}$/O$_4$as intermediate material at low post-treatment temperature had high thermal stability and maintained sphericity of particles after post-treatment. All the samples had main omission peak at 450 nm, which corresponds to blue emission. The optimum post-treatment temperature of BAM:Eu$^{2+}$ particles for the maximum PL(photoluminescence) intensity in the spray pylolysis was 1200 $^{\circ}C$ because of high crystallinity, Phase-Purity, and good morphology.ology.

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Oxidative Etching of Imprinted Nanopatterns by Combination of Vacuum Annealing and Plasma Treatment

  • Park, Dae Keun;Kang, Aeyeon;Jeong, Mira;Lee, Jae-Jong;Yun, Wan Soo
    • Proceedings of the Korean Vacuum Society Conference
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    • 한국진공학회 2013년도 제45회 하계 정기학술대회 초록집
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    • pp.251.1-251.1
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    • 2013
  • Combination of oxidative vacuum annealing and oxygen plasma treatment can serve as a simple and efficient method of line-width modification of imprinted nanopatterns. Since the vacuum annealing and oxygen plasma could lead mass loss of polymeric materials, either one of the process can yield a narrowed patterns. However, the vacuum annealing process usually demands quite high temperatures (${\geq}300^{\circ}C$) and extended annealing time to get appreciable line-width reduction. Although the plasma treatment may be considered as an effective low temperature rapid process for the line-width reduction, it is also suffering for the lowered controllability on application to very fine patterns. We have found that the vacuum annealing temperature can be lowered by introducing the oxygen in the vacuum process and that the combination of oxygen plasma treatment with the vacuum annealing could yield the best result in the line-with reduction of the imprinted polymeric nanopatterns. Well-defined line width reduction by more than 50% was successfully demonstrated at relatively low temperatures. Furthermore, it was verified that this process was applicable to the nanopatterns of different shapes and materials.

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Comparison of Hardness and Damping Capacities of Mg-Al Alloy Subjected to T6 Heat Treatment and Low Temperature Long Term Isothermal Aging (T6 열처리 및 저온 장시간 등온 시효한 Mg-Al 합금의 경도 및 진동감쇠능 비교)

  • Joong-Hwan Jun
    • Journal of the Korean Society for Heat Treatment
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    • 제36권5호
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    • pp.277-284
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    • 2023
  • Hardness and damping characteristics of fine discontinuous precipitates (DPs) microstructure generated by low temperature long term isothermal aging were investigated in comparison with those of T6 heat-treated microstructure composed of DPs and continuous precipitates (CPs) in Mg-9%Al alloy. In this study, T6 and fine DPs microstructures were obtained by isothermal aging at 453 K for 24 h and at 413 K for 336 h, respectively, after solution treatment at 693 K for 24 h. The DPs microstructure exhibited higher hardness than the T6 microstructure, which is related to the lower (α + β) interlamellar spacing of the DPs. The DPs microstructure possessed better damping capacity than the T6 microstructure in the strain-amplitude independent region, whereas in the strain-amplitude dependent region, the reverse behavior was observed. The damping tendencies depending on strain-amplitude were discussed based on the microstructural features of the T6 and DPs microstructures.

Comparison of Brood Productions in the Cold-Treated Pairing vs. Not Cold-Treated Pairing in a Stenochronous Spider

  • Kim, Kil-Won
    • Journal of Ecology and Environment
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    • 제32권3호
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    • pp.145-148
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    • 2009
  • To understand whether experience of cold season in reproductive behaviors in the adults of Amaurobius ferox, the paired adults of a female and a male were exposed under 'cold-treated environment' and 'not cold-treated environment', respectively. I investigated effects of the cold treatment on the brood production of A. ferox. In not cold treatment in which male-female pairs were formed in October at a temperature of $20^{\circ}C$ (${\pm}2^{\circ}C$) and continuously kept under not cold-treated environment, only 3 of 50 pairs successfully reproduced (reproduction was defined as the emergence of spiderlings). In cold treatment where individuals were kept in cold conditions for 3 months prior to pair formation, 57 out of 60 couples succeeded in reproducing. Females which did not experience the low temperature displayed strong aggressiveness toward males. This behavioral inhibition might the primary barrier to copulation of A. ferox that decrease following a period of low temperature. The reproductive inhibition might help the females to allocate the maximum amount of energy in a given environment to reaching the adult stage and to delay reproduction in unfavorable wintering conditions.

The Physical Properties and Dyeability of KOH Treated Cotton Fabrics (KOH 처리 면직물의 물성 및 염색성)

  • Song, Hyun-Joo;Kim, Su-Mi;Song, Wha-Soon
    • Fashion & Textile Research Journal
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    • 제7권1호
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    • pp.91-95
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    • 2005
  • The purpose of this study is to investigate the improvement of fiber surface, physical properties and research the physical properties and dyeability of cotton fabrics treated with KOH solution at low and high temperature. The treatment conditions for mercerization with KOH were changed various temperatures(25, $90^{\circ}C$), concentrations(15, 20, 25, 30%. w/v) and times(30, 60, 180, 300sec). The effects of mercerization after KOH treatment estimated with tensile strength, tearing strength, shrinkage, drape stiffness, moisture regain, fiber surface, and dyeability. The optimal conditions were concentration of KOH 20%, time 180sec in low temperature and concentration of KOH 20%, time 60sec in high temperature. The results are as follows; Tensile strength, tearing strength and moisture regain were much improved than those of untreated cotton fabric. Shrinkage and drape stiffness of KOH treated cotton were more increased at $25^{\circ}C$ than $90^{\circ}C$. Fiber surface showed more rounded shape at $25^{\circ}C$ than $90^{\circ}C$. Dyeability of cotton fabrics improved by KOH treatment.

Chemical and Micro-Structural Changes in Glass-Like Carbon during High Temperature Heat Treatment

  • Lim, Yun-Soo;Kim, Hee-Seok;Kim, Myung-Soo;Cho, Nam-Hee;Sahn Nahm
    • Macromolecular Research
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    • 제11권2호
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    • pp.122-127
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    • 2003
  • A glass-like carbon was fabricated using furan resin. The influence of heat treatment temperature during fabrication process on the chemical and micro-structural changes was studied by various analytical and spectroscopic methods including TGA, FT-IR, CHN, TEM and XRD. The chemical resistance properties of the fabricated glass-like carbon were also investigated. It has been found that the heat-treated samples at higher temperature up to 2600 $^{\circ}C$ in $N_2$ atmosphere had little weight loss, small amounts of functional groups, and high carbon content. The fabricated glass-like carbons upon heat treatment at 2600 $^{\circ}C$ showed an amorphous stage without any grain growth and/or reconstruction of structure. The glass-like carbon had much better chemical resistance than the artificial graphite, and exhibited a high chemical resistance due to its low surface areas, minimum impurities, and low graphite crystallites.

Photosynthesis, Chlorophyll Contents and Leaf Characteristics of Illicium anisatum under Different Shading Treatments (비음처리에 따른 붓순나무의 광합성, 엽록소 함량 및 엽 특성)

  • Son, Seog-Gu;Han, Jin-Gyu;Kim, Chan-Soo;Hwang, Suk-In;Jeong, Jin-Heon;Lee, Sung-Gie
    • Journal of Environmental Science International
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    • 제16권11호
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    • pp.1313-1318
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    • 2007
  • Illicium anisatum was bred under four different light intensity. Those condition were full sunlight(PPFD $1600{\mu} mol\;m^{-2}s^{-1}$), 30% treatment(PPFD $400{\mu} mol\;m^{-2}s^{-1}$), 50% treatment(PPFD $250{\mu} mol\;m^{-2}s^{-1}$) and 70% treatment(PPFD $100{\mu} mol\;m^{-2}s^{-1}$), respectively. Chlorophyll a and b were increased according to decrease of light intensity. Thirty percent and 50% treatment had not significant different in chlorophyll a and b. Thirty percent treatment was shown the best photosynthetic activity through invested photosynthetic rate, intercellular $CO_2$ concentration and water use efficiency. Photosynthetic activity trend of 50% treatment was similar to 30% treatment. Seventy percent treatment was shown the best photosynthetic activity at low light intensity but that was decreased to lower value than 30% and 50% treatment under high intensity. Control, bred full sunlight, was shown the worst photosynthetic activity at measured all light intensity. That result could imply that was caused by photo-inhibition because of long term exposed of shade tolerant plant at high light intensity. Leaf characteristics had not significant different in leaf length, width and area but leaf dry weight had similar trend to photosynthetic activity.

Effect of annealing treatment on gelatinization of upland and lowland waxy brown rice starches (아닐링 처리가 밭벼와 논벼 찹쌀 전분의 호화에 미치는 영향)

  • Kim, Sung-Kon
    • Applied Biological Chemistry
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    • 제34권2호
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    • pp.187-189
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    • 1991
  • Gelatinization temperatures of upland and lowland waxy brown rice starches annealed at $25^{\circ}C$ and $60^{\circ}C$ for 24hr were investigated with differential scanning calorimetry No annealing effect was observed at low temperature. The upland rice starch showed narrower range of gelatinization temperature upon annealing treatment at $60\circ}C$ compared with the lowland rice starch. The enthalpy of gelatinization was not changed in case of the upland rice starch but was increased in case of the lowland one upon annealing.

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