• Title/Summary/Keyword: Low temperature curing

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THERMAL CHANGE AND MICROHARDNESS IN CURING COMPOSITE RESIN ACCORDING TO VARIOUS CURING LIGHT SYSTEM (광중합기에 따른 복합레진 중합시 온도 변화와 미세경도에 관한 연구)

  • Lee, Dong-Jin;Kim, Dae-Eop;Yang, Yong-Sook;Lee, Kwang-Hee
    • Journal of the korean academy of Pediatric Dentistry
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    • v.31 no.3
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    • pp.391-399
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    • 2004
  • The purpose of this study was to compare curing efficiency of newly developed curing units to traditional halogen curing unit by measuring thermal change and surface microhardness according to curing light system. Materials and mathods : The types of curing units were traditional low intensity halogen light(Optilux 360), plasma arc light(Flipo), low heat plasma arc light(Aurys), low intensity LED(Starlight), and high intensity LED(Freelight2). Temperature at the tip of light guide was measured by a digital thermometer using K-type thermocouple. And after resin was filled to 2, 3, 4mm teflon mold, bottom temperature measured during curing. After 24 hours, microhardness of top surface and bottom surface of each resin specimen were measured. Results : The result of this study can be summarized as follows, 1. As measuring temperature of curing unit tips, Flipo is the highest as $52.4^{\circ}C,\;Freelight2(37.86^{\circ}C),\;Optilux360(32.68^{\circ}C),\;Aurys(32.34^{\circ}C),\;and\;Starlight(26.14^{\circ}C)$ were followed. 2. Flipo and Freelight2 were the highest similarly and Optilux360 and Aurys were similarly next and Starlight was lowest in temperature of bottom surface of resin mold. 3. Microhardness of top surface were generally similar, and Aurys was relatively low. 4. Optilux 360 and Freelight2 were the highest, and Flipo, Starlight, and Aurys were followed in microhardness of bottom surface. Conclusions : The results suggest that careful use of Flipo and Freelight2 might be able to cure greater depth of resin composite and do not cause thermal problems than other curing units.

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A Study on Curing Properties and Structures of Phase Separation for UV-Curable Resing and Alkyd Resin Blends (UV중합성 수지와 알키드 수지 혼합물의 경화특성 및 상분리 구조에 관한 연구)

  • 최정병
    • Journal of the Korean Graphic Arts Communication Society
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    • v.18 no.1
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    • pp.13-24
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    • 2000
  • UV-curable resin has the properties of quick-drying, high productivity at low temperature, energy, space saving, solventless, non-polluting and low-stinking, and thus, UV-curing system has been widely used in the fields of printing inks, adhesives, paints and coating agents. This study has been executed to develop a new functionnal material by the polymerization induced phase separation. The results obtained were as follows. As for the curing properties of the monomer/prepolymer/alkyd resin blends, it was found out that there was a peak by the polymerization induced phase separation when measuring the changes of viscosity and elasticity. It was also found out that such polymerization phase separation occurred in case that the alkyd resin contents were 20wt% and 30wt% and not found at the contents of 40wt%. Therefore, it would be desirable to maintain the contents of alkyd resin at less than 30wt% in order to use the polymerization induced phase separation.

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Freeze and Mechanical Properties of Cement Mortar Using Coolant Wastes (폐부동액을 이용한 콘크리트의 동결 및 역학적 특성)

  • 김상우;김정진;홍상희;전충근;한천구
    • Proceedings of the Korea Concrete Institute Conference
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    • 2000.10a
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    • pp.555-558
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    • 2000
  • It has been increasingly proving in interest of environment pollution around the world. so, recycling of waste resources are seriously taken into consideration. Great deal of coolant for the car have been wasted for along time. due to the end of life time of them. Therefore, validities of wasted coolant as an agent for concrete are described in this paper. Mechanical properties of concrete using coolant wastes is investigated. As contents of coolant wastes increase, slump and slump flow decrease, while air content show reverse tendency. setting time shows to be accelerated with increase of waste contents. As for the effect of low curing temperature, low curing temperature increase compressive strength with increase of coolant waste. Application of coolant waste to cold weather concrete is considered to achieve favorable effects.

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Study on the Quality Properties of Anti Freeze Agent manufactured in Korea (국내 시판 방동제의 품질 특성에 관한 조사)

  • Lee, Gun-Cheol;Noh, Sang-Kyun;Cho, Byoung-Young;Kim, Young-Geun
    • Proceedings of the Korea Concrete Institute Conference
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    • 2010.05a
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    • pp.333-334
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    • 2010
  • In this paper, quality variations of commercially available anti-freezers manufactured in Korea are studied. This study is focused on the effect of the use of anti freezer on strength recovery of cement mortar under low curing temperature. As expected, regardless of types of anti freezer, the use of antifreezer protects the water from freezing under low curing temperature.

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Application of Insulation Curing Method with Double Bubble Sheets Subjected to Cold Weather (이중 버블시트를 이용한 단열양생공법의 한중시공 적용 사례)

  • Hong, Seak-Min;Lee, Chung-Sub;Kim, Jong;Jeon, Chung-Kun;Han, Min-Cheol;Han, Cheon-Goo
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.04a
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    • pp.1001-1004
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    • 2008
  • This study reviewed the results of utilization of insulation heat curing method using double layer bubble sheet in slab concrete and mass concrete in cold weather environment. First of all, when double layer bubble sheets are applied, it was shown that slab concrete was protected from early freezing by remaining between 6 and $10^{\circ}C$ even in case outside temperature drops $10^{\circ}C$ below zero until the 2nd day from piling, and in the case of mass concrete, with the maximum temperature difference between the center and surface less than $6^{\circ}C$, crack occurrence index was close to 2 and no hydration heat crack occurred by internal constraint. The insulation heat preservation curing method using the double bubble sheet applied in this field prevented early freezing owing to stable curing temperature management, deterring concrete strength development delay at low temperature, and obtained the needed strength. Also, it was proven that the method is highly effective and economic for cold weather concrete quality maintenance through curing cost reduction like construction period shortening and labor cost reduction, etc by reducing the process of temporary equipment installation and disassembling.

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A Experimental Study on Early Age Compressive Strength of Cement Mortar Using Anti Freezer and Hardening Accelerator at low temperature (방동제와 경화촉진제를 사용한 저온환경하 모르타르의 초기압축강도에 관한 실험적 연구)

  • Kim, Mok-Kyu;Lee, Han-Seung
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2014.11a
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    • pp.135-136
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    • 2014
  • In this study, the experimental study on the early age compressive strength of cement mortar using anti freezer and hardening accelerator at low temperature was conducted. For this study, all of materials for experiment were kept in a low temperature for 24 hours before mortar mixing. After mortar curing at low temperature, compressive strength was measured at the early ages. Furthermore, properties of hardened cement material was analysed using TG-DTA and MIP.

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Thermal and Humidity Sensing Properties of Heat Resistant Polyimide Thin Film Manufactured by Dry Process (건식법에 의해 제조된 내열성 폴리이미드박막의 열적특성 및 습도감지특성)

  • Lim, Kyung-Bum;Kim, Ki-Hwan;Hwang, Sun-Yang;Kim, Jong-Yoon;Hwang, Myung-Hwan
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.56 no.6
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    • pp.1080-1086
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    • 2007
  • The aim of this paper is to establish the optimum fabrication condition of specimens, using the Vapor Deposition Polymerization Method(VDPM), which is one of modesto prepare functional organic thin films using a dry process, and to develop a thin film type humidity sensor which has good humidity sensitive characteristics. The inner part of the film became denser and roughness of the film surface eased as curing temperature increased so that thickness of the film could be made uniform. This also shows the appropriate curing temperature was $250^{\circ}C$. The basic structure of the humidity sensor is a parallel capacitor which consists of three layers of Aluminum/Polyimide/Aluminum. The result of SEM and AFM measurement shows that the thickness of PI thin films decreased and the refraction increased as curing temperature increased, which indicates that a capacitance-type humidity sensor utilizing polyimide thin film is fabricated on a glass substrate. The characteristics of fabricated samples were measured under various conditions, and the samples had linear characteristics in the range of 20-80 %RH, independent of temperature change, and low hysteresis characteristic.

Mock-up Test of Low Heat Concrete Using High Volume Mineral Admixture (혼화재를 다량 사용한 저발열 콘크리트의 모의부재실험)

  • Kim, Yong-Ro;Song, Young-Chan;Kim, Hyo-Rak;Park, Jong-Ho;Yoo, Jung-Hoon;Jeong, Yong
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2011.05b
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    • pp.31-34
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    • 2011
  • In this study, for the evaluation of field application of low heat concrete using high volume mineral admixture, the characteristics of hydration heat generation and engineering properties of low heat concrete was investigated by mock-up test according to the replacement ratio of mineral admixture. Also, it was evaluated the compressive strength of low heat concrete with curing temperatures and ages for effective concrete mix design considering seasonal change.

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Effects of Curing Temperature on Autogenous Shrinkage, Relative Humidity, Pore Structure of Cement Pastes

  • Park Ki-Bong
    • Journal of the Korea Concrete Institute
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    • v.17 no.5 s.89
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    • pp.853-856
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    • 2005
  • A low water/cement ratio leads to autogenous shrinkage of cement paste at an early age. This autogenous shrinkage is related to the change of relative humidity in the pore structure that is formed during the hydration process. The relationship between autogenous shrinkage and relative humidity change are relatively well defined today, but the effects of temperature on autogenous shrinkage, relative humidity, and pore structures have been studied less systematically. This study focused on correlating alterations of these properties of cement paste hydrated at constant temperatures of 20, 40, and $60^{\circ}C$. The test results clearly indicate that increasing curing temperature resulted in increased porosity, particularly for pores between 5 to 50 nm as measured by MIP, and increased autogenous shrinkages, as a consequence of a reduction of relative humidity at early ages.

AN EXPERIMENTAL STUDY ON THE DIMENSIONAL CHANGES OF RELINED DENTURES AND MECHANICAL PROPERTIES AND SURFACE TEXTURES OF SEVERAL RESINS USED IN DENTURE RELINING (수종 레진으로 의치상 조직면 개조시 의치상의 크기변화와 물리적 성질 및 표면상태 비교 연구)

  • Lee, Chang-Han;Kim, Yung-Soo
    • The Journal of Korean Academy of Prosthodontics
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    • v.28 no.1
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    • pp.25-41
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    • 1990
  • The purpose of this study was to evaluate and compare the dimensional changes of relined dentures with a light-curing resin, a heat-curing resin, and a direct, hard reline resin. And also to measure the transverse strength, impact strength, surface hardness of the three resins used in relining. The surface textures of three resins also of evaluated by using scanning electron microscope. Through analyses on the data from this study, the following conclusions were obtained. 1. Impact strength of heat-curing resin was highest, and direct, hard reline resin higher, light-curing resin lowest. 2. Transverse strength of heat-curing resin was highest, and direct, hard reline resin and light-curing resin was lower and not signiicantly different. 3. Surface hardness of light-curing resin was lighest, heat-curing resin higher, and direct, hard reline resin was lowest. 4. After storage of the relined dentures for 1 day and 1 week in water at room temperature, linear shrinkage of distance between the reference points in the maxillary base relined with direct, hard reline resin was lowest, and those relined with light-curing resin and heat-curing resin were lower and were not significantly different. 5. After storage for 4 weeks in orator at room tempeature, linear shrinkage of distance between ridge crests of dentures relined with heat-curing resin was highest and that of distance between denture borders was not significantly different. 6. The dimensional changes of relined dentures during storage in water was not significant except those of distance between denture borders relined with light-curing resin at 1 day and 1 week storage in water. 7. At low magnification (x40) of SEM examination, the surface textures of three resins were similar except light-curing resin which had some defects. At high magnification (x200), the surface textures of hard, direct reline resin were smooth with little defects, but those of heat-curing resin and light-curing resin w ere irregular.

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