• Restorative Dentistry and Endodontics
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• v.18 no.1
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• pp.205-213
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• 1993

The purpose of the study was to evaluate the degree of the marginal leakage of esthetic restorative materials on root caries restoration. 120 cavities were prepared to $90^{\circ}$ butt joint on all margins on the crown and root portion, and divided into 4 groups. The four groups of cavity were filled with Amalgam(Dongmuyung Dental Alloy Co., Ltd, KOREA), Silux$^{(R)}$(3M Co., USA)-Scotch Bond 2$^{(R)}$(3M Co., USA), Silux$^{(R)}$-All Bond$^{(R)}$(BISCO USA), and GC Fuji II$^{(R)}$(G-C Co., JAPAN) respectively. The apical margin of the preparation was finished to leave a flash of restorative material. The coronal margin of the preparation was finished not to leave a flash of restorative material. All specimens were sectioned longitudinally with Isomet Low speed saw(Buether Ltd, USA). The degree of dye penetration was evaluated as the parameter of marginal leakage under the stereoscope. The results were as follows. 1. At the enamel and dentin/cementum margins, the margin were finished to leave a flash of material showed less marginal leakage than that were finished not to leave a flash of material (P<0.001). 2. The enamel margins showed less marginal leakage than the dentin/cementum margins(P<0.001). 3. There was no significant difference in the degree of the marginal leakage between Silux$^{(R)}$-Scotch Bond 2$^{(R)}$ group and Silux$^{(R)}$-All Bond$^{(R)}$ group.

• Resources Recycling
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• v.14 no.2
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• pp.43-55
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• 2005

As world population increases and the world economy expalds, so does the demand for natural resources especially strategic metals such as cobalt. An accurate assesment of the nation's minerals must include not only the resources available in the ground but also those that become available through recycling. In this paper, data on domestic and international supply of cobalt and its applications by end-user were analyzed for stable security of cobalt resources and effective recycling of cobalt scraps. Also, an initial evaluation of the flow of cobalt-containing materials in the United States was prepared. In 2003, 8,000 metric tons of cobalt were consumed in the United States and an estimated 28% of U.S. cobalt supply was derived from scrap. The superalloy industry and catalyst industries have well-established recycling or cobalt recovery practices. Recycling rates of cobalt scraps from magnet alloy and cemented carbide were relatively low.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
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• v.13 no.5
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• pp.437-443
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• 2000

In this study several lanthanide complexes such as Eu(TTA)$_3$(Phen), Tb(ACAC)$_3$-(Cl-Phen) were synthesized and the white-light electroluminescence(EL) characteristics of their thin films were investigated where the devices having structures of anode/TPD/Tb(ACAC)$_3$(Cl-Phen)/Eu(TTA)$_3$(Phen)/Alq$_3$or Bebq$_2$/cathode and the low work function metal alloy such as Li:Al was used as the electron injecting electrode(cathode). Device structure of glass substrate/ITO/TPD(30nm)/Tb(ACAC)$_3$(Phen)(30nm)/Eu(TTA)$_3$(Phen)(6nm)/DCM doped Alq$_3$(10nm)/Alq$_3$(20nm)/Li:Al(100nm) was also fabricated and their EL characteristics were investigated where Eu(TTA)$_3$(Phen) and DCM doped Alq$_3$were used as red light-emitting materials. It was found that the turn-on voltage of the device with non-doped Alq$_3$was lower than that of the devices with doped Alq$_3$and the blue and red light emission peaks due to TPD and Eu(TTA)$_3$(Phen) with non-doped Alq$_3$were lower than those with DCM doped Alq$_3$Details on the white-light-emitting characteristics of these device structures were explained by the energy and diagrams of various materials used in these structure where the energy levels of new materials such as ionization potential(IP) and electron affinity(EA) were measured by cyclic voltametric method.

• Proceedings of the KIEE Conference
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• 2002.11a
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• pp.82-84
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• 2002

Dimensionally stable anode(DSA) can be used for the electrowinning of non-ferrous metal like as a Zn, and electrolysis of sea water. $MnO_2$ electrode satisfies the requirements of DSA, and has a good cycle life and a low overpotential for oxygen evolution. $MnO_2$ electrodes coated with DMF and PVDF based on Pb alloy produced at several compositions and dry temperatures. The viscosity of solvent used as a binder of $MnO_2$ powder increased with the increasing PVDF contents. When the ratio of PVDF to BMF with the 5 times dipping at the solution mixed with PVDF and DMF was 1/9, the coating thickness was $150{\mu}m$. When the ratio of PVDF to $MnO_2$ was lower than 1/6, the electrode didn't show any reaction irrespective of the concentrations of DMF. However, When the ratio of PVDF to $MnO_2$ was higher than 1/6, the electrode showed a constant current reactions and homogeneous cyclic voltammetry even though at a high cycle. The reason for the high current and homogeneous cyclic voltammetry is the good catalytic reactions of $MnO_2$ powder in electrode. The reactions of Pb electrode coated with $MnO_2$ and PVDF based on the pure Pb electrode.

• Journal of the Korean Vacuum Society
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• v.9 no.3
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• pp.237-241
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• 2000

The structural, electrical and etching characteristics of Al alloy thin film with low impurity concentrations AlNd deposited by using do magnetron sputtering deposition are investigated for the applications as gate bus line in the TFt-LCD panel. And ITO thin film was deposited on AlNd, then the contact resistance was measured by Kelvin resistor. The deposited thin films show the decrease of resistivity and the increase of grain size after the RTA at $300^{\circ}C$ for 20 min. Moreover, the resistivity of AlNd does not show appreciable grain size dependence after RTA. It is concluded that the decrease of resistivity after RTA is due to the increase of grain size. The annealed AlNd is found to be hillock free. The etching profiles of AlNd was good and the minimun contact resistance was about $110\;{\mu\Omega}cm$. Calculation results reveal that the AlNd (2wt.%) thin film can be applicable to 25" SXGA class TFT-LCD panels.

• Radiation Oncology Journal
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• v.4 no.2
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• pp.165-172
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• 1986

In electron therapy, lead cutout or low-melting alloy block is used for shaping the field. Material for shaping electron field affects the output factor as wet 1 as the collimation system. The authors measured the output factors of electron beams for shaped fields from Clinac-18 using ionization chamber of Farmer type in polystyrene phantom. They analyzed the parameters that affect the output factors. The output factors of electron beams depend on the incident energy, collimation system and size of shaped field. For shaped field the variation of output factor for the field size (A/P) has appearence of a smooth curve for all energy and all applicator collimator combination. The output factors for open field deviate from the curves for shaped fields. An output factor for a given field can be calculated by equivalent field method such as A/P method, if a combination of applicator and collimator is fixed.

• Journal of Welding and Joining
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• v.1 no.2
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• pp.45-52
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• 1983

Many pressure vessels for the hot H$\sub$2//H$\sub$2/S service are made of 2+1/4Cr-1Mo steel with austenitic stainless steel overlay to combat agressive corrosion due to hydrogen sulfide. Hydrogen dissolves in to materials during operation, and sometimes gives rise to unfore-seeable damages. Appropriate precautions must, therefore, be taken to avoid the hydrogen induced damages in the design, fabrication and operation stage of such reactor vessels. Recently, hydrogeninduced cracking (or Disbonding) was found at the interface between base metal and stainless weld overlay of a desulfurizing reactor. Since the stainless steel overlay weld metal is subjected to thermal and internal-pressure loads in reactor operation, it is desirable for the overlay weld metal to have high strength and ductility from the stand point of structural safety. In section III of ASME Boiler and Pressure Vessel Code, Post-Weld Heat Treatment(PWHT) of more than one hour per inch at over 1100.deg. F(593.deg. C) is required for the weld joints of low alloy pressure vessel steels. This heat treatment to relieve stresses in the welded joint during construction of the pressure vessel is considered to cause sensitization of the overlay weld metal. The present study was carried out to make clear the diffusion of carbon migration by PWHT in dissimilar metal welded joint. The main conclusion reached from this study are as follows: 1) The theoretical analysis for diffusion of carbon in stainless steel overlay weld metal does not agree with Fick's 2nd law but the general law of molecular diffusion phenomenon by thermodynamic chemical potential. 2) In the stainless steel overlay welded joint, the PWHT at 720.deg. C for 10 hours causes a diffusion of carbon atoms from ferritic steel into austenitic steel according to the theoretical analysis for carbon migration and its experiment. 3) In case of PWHT at 720.deg. C for 10 hours, the micro-hardness of stainless steel weld metal in bonded zone increase very highly in the carburized layer with remarkable hardening than that of weld metal.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.36 no.9
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• pp.997-1002
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• 2012

With the increasing demand for lightweight materials to reduce fuel consumption, especially in the transportation industry, magnesium alloys are being widely studied. However, there are several limitations to the large-scale application of magnesium alloys in a structure because of their low formability and strong anisotropy. In order to take into account both the strong anisotropy and tension-compression asymmetry of AZ31 sheet alloy, the Cazacu-Plunkett-Barlat yield criterion (Cazacu, 2006) was adopted in material modeling. The variation of the anisotropic coefficients that describe the yield surface evolution of AZ31 is optimized using an interpolation function based on specific calibration results. It generates continuous yield surfaces, which makes it possible to describe different hardening rates in tension and compression as well as the tension-compression asymmetry of magnesium alloys. The performance of the CPB06 yield criterion for simulating an axial crushing test was tested and compared with that of the Hill (1948) yield criterion.

• Transactions of Materials Processing
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• v.13 no.5
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• pp.422-428
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• 2004

At present, the design of extrusion dies and operation in extrusion companies are primarily based on trial and error. The experience of the die designer, the press operator and the die corrector determine the performance of the extrusion die and the efficiency of the process. In order to produce defect-free products of desirable quality in terms of strength, surface quality and geometrical dimensions, it is important to obtain more knowledge of the processes that occur during extrusion. Recently, to reduce the costs of designing and manufacturing of extrusion dies, and to ensure the quality of the extruded products, numerical simulation for extrusion processes such as FEM (finite element method) is applied increasingly and becomes a very important tool for the design and development of new products. However, most of the studies about FE simulation have been accomplished for simple geometry and low extrusion ratio in the filed of steady metal flow conditions. The extruded products of AI alloy in industrial practice involve complicated sectional geometry. This study was designed to reduce the time of die design and manufacturing in the extrusion process using FEM simulation. FEM simulations of extrusion process were performed in non-steady states conditions by changing weld plate included in extrusion die set. Product which was employed in this study is heat sink that has been used in the parts of heat exchanger of electric circuits. It is generally applied for aluminum or its alloys due to heat efficiency and easy production of complicated shapes, and manufactured by extrusion process. The simulated results showed that weld plate shape in extrusion dies influences meta] flow and dimensional accuracy of products.

• Transactions of the Korean Society of Mechanical Engineers
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• v.11 no.2
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• pp.314-321
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• 1987

Post weld heat treatment (PWHT) of weldment of the low alloy Cr-Mo steel, in general, is carried out not only to remove residual stress and hydrogen existing in weldment but to improve fracture toughness of weld heat affected zone (HAZ). There occur some problems such as toughness decrement and stress relief cracking (SRC) in the coarse grained region of weld HAZ when PWHT is practiced. Especially, embrittlement of structure directly relates to the mode of fracture and is appeared as the difference of fracture surface such as grain boundary failure. Therefore, in this paper, the effect of heating rate on PWHT embrittlement under the various kinds of stresses simulated residual stress in weld HAZ was evaluated by COD fracture toughness test and observation of fracture surface. Fracture toughness of weld HAZ decreased with increment of heating rate under no stress, but it was improved to increment of heating rate under the stress. Grain boundary failure didn't almost appear at the heating rate of 600.deg.C/hr but it appeared from being the applied stress of 294 MPa at 220.deg.C/hr and 196 MPa at 60.deg.C/hr.