• 한국진공학회:학술대회논문집
• /
• 한국진공학회 2011년도 제41회 하계 정기 학술대회 초록집
• /
• pp.110-110
• /
• 2011

The nanomechanical properties of fully lithiated and unlithiated silicon nanowire deposited on silicon substrate have been studied with atomic force microscopy. Silicon nanowires were synthesized using the vapor-liquid-solid process on stainless steel substrates using Au catalyst. Fully lithiated silicon nanowires were obtained by using the electrochemical method, followed by drop-casting on the silicon substrate. The roughness, derived from a line profile of the surface measured in contact mode atomic force microscopy, has a smaller value for lithiated silicon nanowire and a higher value for unlithiated silicon nanowire. Force spectroscopy was utilitzed to study the influence of lithiation on the tip-surface adhesion force. Lithiated silicon nanowire revealed a smaller value than that of the Si nanowire substrate by a factor of two, while the adhesion force of the silicon nanowire is similar to that of the silicon substrate. The Young's modulus obtained from the force-distance curve, also shows that the unlithiated silicon nanowire has a relatively higher value than lithiated silicon nanowire due to the elastically soft amorphous structures. The frictional forces acting on the tip sliding on the surface of lithiated and unlithiated silicon nanowire were obtained within the range of 0.5-4.0 Hz and 0.01-200 nN for velocity and load dependency, respectively. We explain the trend of adhesion and modulus in light of the materials properties of silicon and lithiated silicon. The results suggest a useful method for chemical identification of the lithiated region during the charging and discharging process.

• 대한환경공학회지
• /
• 제22권4호
• /
• pp.713-722
• /
• 2000

본 연구는 입자크기를 분석하기 위한 장치인 레이저회절 분광계의 측정오차 및 재현성을 분석한 것이다. 레이저회절 spectrometers는 입자크기를 분석하기 위한 장치 중에서 가장 대표적이고 중요성을 가진다. 이 측정장치는 운전이 간단하며, 입자분석에 있어서 재현성이 우수하고, 빠른 속도로 분석이 가능한 형태이다. 입자크기를 분석하는 과정에 있어서 공급되는 분산형태와 흐름율에 따라서 측정오차가 미세하게 발생되었고, 흐름율은 분산형태가 건식인 경우 0.1~23 g/min로 공급하였고, 습식인 경우는 분산되는 용매에 따라서 1.4~35 %가 되도록 조절하여 측정결과에 따라서 발생되는 측정오차를 분석하였다. 흐름을 변화에 따라서 발생되는 측정 오차는 측정 cell 내의 입자에 입사되는 레이저 회절패턴이 변화함으로서 측정오차가 다양하게 발생하였다. 본 연구에서 측정오차를 분석하기 위해서는 입자모양, 크기, 분산형태와 용매, 흐름율과 농도의 변화에 따라서 실험을 실행하였고, 분석장치의 시스템에 따른 측정오차를 나타내기 위해서는 장치내의 역학적인 공정, 측정시간, 초점거리, 주입압력, 전처리과정인 ultrasonic이나 혼합에 의한 분산효과에 따라 측정오차 및 재현성을 분석하였다.

• 한국환경과학회지
• /
• 제26권7호
• /
• pp.827-836
• /
• 2017

Freezing rain is a phenomenon when precipitation falls as a liquid rain drop, but freezes when it comes into contact with surfaces or objects. In this study, we investigated the predictability of freezing rain and its characteristics, which are strongly related with the occurrence of black ice using synoptic scale meteorological observation data. Two different cases occurred at 2012 were analyzed and in the presented cases, freezing rain often occurs in the low-level low pressure with the warm front. The warm front due to the lower cyclone make suitable environment in which snow falling from the upper layer can change into supercooled water. The $0^{\circ}C$ temperature line to generate supercooling water is located at an altitude of 850 hPa in the vertical temperature distribution. And the ground temperature remained below zero, as is commonly known as a condition for black ice formation. It is confirmed that the formation rate of freezing rain is higher when the thickness after 1000-850 hPa is 1290-1310 m and the thickness of 850-700 hPa layer is larger than 1540 m in both cases. It can also be used to predict and estimate the generation of freezing rain by detecting and analyzing bright bands in radar observation.

• 한국추진공학회:학술대회논문집
• /
• 한국추진공학회 2017년도 제48회 춘계학술대회논문집
• /
• pp.892-895
• /
• 2017

대형 가스터빈 연소기 구성품인 단일 압력선회식 연료분사기(Pressure swirl simplex liquid injector)를 설계, 분무특성 및 성능을 시험을 통해 평가하였다. 공급 압력 대비 분무 유량을 측정하여 설계점 기준 분무유량과 비교하였으며 섀도우그래프(Shadowgraph)를 통해 분무가시화이미지를 기록, 분무의 형상을 정성적으로 파악하고 분무각을 측정하였다. 시험 결과 동일한 공급압력 대비 측정된 분무유량은 설계점 기준 유량과 거의 일치하여 설계 및 제작의 정합성이 확인되었으며 섀도우그래프 이미지를 통해 연료분사기의 분무형상을 파악하고 설계 의도된 분무각이 나타남을 확인할 수 있었다. 이를 기반으로 향후 PDA(Phase Doppler Anemometry)를 통한 분무측정을 통해 보다 구체적인 연료 분사기의 분무 성능 및 특성을 파악할 수 있을 것으로 기대된다.

• 한국토양비료학회지
• /
• 제28권3호
• /
• pp.278-286
• /
• 1995

토양(土壤)에 축적(蓄積)되어 있는 난용성(難溶性) 인산염(燐酸鹽)을 이용(利用)하고자 인산염(燐酸鹽) 가용화능(可溶化能)을 가지고 있는 Pseudomonas putida, Penicillium속(屬) 및 Aspergillus niger를 우리 나라 주요(主要) 경작지(耕作地) 토양(土壤)에서 분리(分離)하여 이들 균(菌)의 용해능(溶解能)을 측정(測定)하였다. 인산염(燐酸鹽) 용해량(溶解量)은 배지내(培地內)의 pH 저하(低下)와 밀접(密接)한 관계(關係)를 가지고 있었다. Pseudomonas putida, Penicillium속(屬)에 비(比)해 Aspergillus niger의 인산염(燐酸鹽) 가용화능(可溶化能)이 높았다. Aspergillus niger에 의한 인산염(燐酸鹽) 종류별(種類別) 최대(最大) 가용화량(可溶化量)은 질소원(窒素源)이 $KNO_3$일 때는 aluminium phosphate 776ppm, hydroxyapatite 665ppm, tai-calcium phosphate 593ppm이었으며 인광석(燐鑛石)은 질소원(窒素源)이 $(NH_4)_2SO_4$일 때 411ppm이었다.

• 대한금속재료학회지
• /
• 제48권10호
• /
• pp.893-900
• /
• 2010

In the present work, the impact loads and their effects on the surface damage under the simultaneous cavitation bubble and solid particle collapses in the sea water have been quantitatively investigated for the austenitic 304 stainless steel by using a vibratory cavitation test device. To do this, angular $SiO_2$ solid particles with an average size of $150{\mu}m$ were dispersed into the test liquid, and the measured impact amplitudes were converted into the impact loads by a steel ball drop test. The maximum impact load was determined to be 28.2 N in the absence of solid particles, but increased to 33.7 N in the presence of solid particles. In addition, the critical impact loads, $L_{crit}$, required to generate pits with sizes greater than $3{\mu}m$ were measured to be 19.6 N and 16.6 N, respectively, for the cavitation bubble collapse and solid particle collapse. As a result of the cavitation erosion test, the incubation time and erosion rate were 1.2 times lower and 1.5 times higher, respectively, by a solid particle collapse compared to those only by the cavitation bubble collapse, indicating a drastic decrease in a resistance to cavitation erosion by the solid particle collapse.

• 한국추진공학회:학술대회논문집
• /
• 한국추진공학회 2012년도 제38회 춘계학술대회논문집
• /
• pp.457-460
• /
• 2012

본 연구는 7톤급 연소기용 분사기 검증을 위한 축소형 연소기의 설계 및 제작에 관한 것이다. 7톤급 연소기의 헤드부는 90개의 동축 와류형 분사기로 구성되며, 연소실은 케로신 재생냉각 일체형 연소기이다. 7톤급 연소기에 적용할 분사기로 차압 및 리세스 수를 달리한 분사기를 설계하였다. 설계된 분사기를 실물형 연소기에 적용하기 전 축소형 연소기에 먼저 적용하여 분사기 작동성 및 성능검증을 하고자 한다. 축소형 연소기는 분사기 19개로 구성되며, 연소압력 70 bar, 총 추진제 유량은 4.3 kg/s, 혼합비는 2.45이다.

• Advances in materials Research
• /
• 제8권1호
• /
• pp.37-46
• /
• 2019

Electrochemical double layer capacitors (EDLCs) which are fabricated using carbon based electrodes have been emerging at an alarming rate to fulfill the energy demand in the present day world. Activated charcoal has been accepted as a very suitable candidate for electrodes but its cost is higher than natural graphite. Present study is about fabrication of EDLCs using composite electrodes with activated charcoal and Sri Lankan natural graphite as well as a gel polymer electrolyte which is identified as a suitable substitute for liquid electrolytes. Electrochemical Impedance Spectroscopy, Cyclic Voltammetry and Galvanostatic Charge Discharge test were done to evaluate the performance of the fabricated EDLCs. Amount of activated charcoal and natural graphite plays a noticeable role on the capacity. 50 graphite : 40 AC : 10 PVdF showed the optimum single electrode specific capacity value of 15 F/g. Capacity is determined by the cycling rate as well as the potential window within which cycling is being done. Continuous cycling resulted an average single electrode specific capacity variation of 48 F/g - 16 F/g. Capacity fading was higher at the beginning. Later, it dropped noticeably. Initial discharge capacity drop under Galvanostatic Charge Discharge test was slightly fast but reached near stable upon continuous charge discharge process. It can be concluded that initially some agitation is required to reach the maturity. However, the results can be considered as encouraging to initiate studies on EDLCs using Sri Lankan natural graphite.

• International Journal of Naval Architecture and Ocean Engineering
• /
• 제13권1호
• /
• pp.554-565
• /
• 2021

Air bubble entrainment is a phenomenon that can significantly reduce the efficiency of liquid motion in piping systems. In the present study, the bubble formation mechanism in a globe valve with 90% water fraction flow is explained by visualization study and pressure oscillation analysis. The shadowgraph imaging technique is applied to illustrate the unsteady flow inside the transparent valve. This helps to study the effect of bubbles induced by the globe valve on pressure distribution and valve flow coefficient. International Society of Automation (ISA) recommends locations for measuring pressure drop of the valve to determine its flow coefficient. This paper presents the comparison of the pressures at different locations along with the upstream and the downstream of the valve with the values at recommended positions by the ISA standard. The results show that in partially filled pipe flow, the discrepancies in pressure between different measurement locations in the valve downstream are significant at valve openings less than 30%. The aerated flow induces the oscillation in pressure and flow rate, which leads to the fluctuation in the flow coefficient of the valve. The flow coefficients have a linear relationship with the Reynolds number. For the same increase of Reynolds number, the flow coefficients grow faster with larger valve openings and level off at the opening of 50%.

• 한방안이비인후피부과학회지
• /
• 제35권1호
• /
• pp.24-37
• /
• 2022

Objectives : The purpose of this literature review is to analyze process of manufacture and formulation and toxicity of Geumgweyoryak(金匱要略)'s external applicants for modern and safe using. Methods : This study used the Geumgweyoryak(金匱要略) reprinted by Zhao Kaimei(趙開美) as basic data for a understanding of the manufacture and formulation and toxicity for external applicants. Among the 25 chapters, the 22 chapters were studied except for the last three chapters, which are known to be written by later writers. Based on the above, Geumgweyoryeok(金匱要略)'s external applicants was analyzed the process of manufacture, formulation and the toxicity. Results : There are 11 types of external applicants of Geumgweyoryak(金匱要略). Washing method(洗法) was used 2 times, Drop method(瀝法) was used 1 time, Smoke method(熏法) was used 2 times, Rubbing method(摩法) was used 1 time, Plaster method(敷法) was used 2 times, Invading method(浸法) was used 1 time, Suppository method (坐法) was used 2 times, Flatiron method(烙法) was used 1 time. According to classified the modern formulation, there are 4 types of powder formulation, 4 types of liquid formulation, 2 types of suppository, and 1 type of Semi-solid formulation. Especially toxic drugs, such as Realgar(雄黃) or Hydrocerussite(鉛粉), should be careful. When Realgar(雄黃) smokes, a toxic substance called AS2O3 can come out. Hydrocerussite(鉛粉) can cause lead poisoning. Lead increases the risk of anemia, dehydration, and lead neuropathy when chronically exposed. Conclusion : We supposed that this study can serve as a basic data to help clinical Korean doctors to use the prescription for external applicants more safely and to easily apply it in the form of external applicants.