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검색결과 603건 처리시간 0.024초

[Retraction]Characterization of carbon black nanoparticles using asymmetrical flow field-flow fractionation (AsFlFFF)

  • Kim, Kihyun;Lee, Seungho;Kim, Woonjung
    • 분석과학
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    • 제32권3호
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    • pp.77-87
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    • 2019
  • High viscosity carbon black dispersions are used in various industrial fields such as color cosmetics, rubber, tire, plastic and color filter ink. However, carbon black particles are unstable to heat due to inherent characteristics, and it is very difficult to keep the quality of the product constant due to agglomeration of particles. In general, particle size analysis is performed by dynamic light scattering (DLS) during the dispersion process in order to select the optimum dispersant in the carbon black dispersion process. However, the existing low viscosity analysis provides reproducible particle distribution analysis results, but it is difficult to select the optimum dispersant because it is difficult to analyze the reproducible particle distribution at high viscosity. In this study, dynamic light scattering (DLS) and asymmetrical flow field-flow fractionation (AsFlFFF) analysis methods were compared for reproducible particle size analysis of high viscosity carbon black. First, the stability of carbon black dispersion was investigated by particle size analysis by DLS and AsFlFFF according to milling time, and the validity of analytical method for the selection of the optimum dispersant useful for carbon black dispersion was confirmed. The correlation between color and particle size of particles in high viscosity carbon black dispersion was investigated by using colorimeter. The particle size distribution from AsFlFFF was consistent with the colorimetric results. As a result, the correlation between AsFlFFF and colorimetric results confirmed the possibility of a strong analytical method for determining the appropriate dispersant and milling time in high viscosity carbon black dispersions. In addition, for nanoparticles with relatively broad particle size distributions such as carbon black, AsFlFFF has been found to provide a more accurate particle size distribution than DLS. This is because AsFlFFF, unlike DLS, can analyze each fraction by separating particles by size.

Design and Development of a Single-photon Laser and Infrared Common Aperture Optical System

  • Wu, Hongbo;Zhang, Xin;Tan, Shuanglong;Liu, Mingxin;Wang, Lingjie;Yan, Lei;Liu, Yang;Shi, Guangwei
    • Current Optics and Photonics
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    • 제6권2호
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    • pp.171-182
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    • 2022
  • A single-photon laser and mid-wave infrared (MWIR) common aperture optical system was designed and developed to detect and range a long-distance civil aviation aircraft. The secondary mirror of the Ritchey-Chretien (R-C) optical system was chosen as a dichroic lens to realize the design of a common aperture system for the laser and MWIR. Point spread function (PSF) ellipticity was introduced to evaluate the coupling efficiency of the laser receiving system. A small aperture stop and narrow filter were set in the secondary image plane and an afocal light path of the laser system, respectively, and the stray light suppression ability of the small aperture stop was verified by modeling and simulation. With high-precision manufacturing technology by single point diamond turning (SPDT) and a high-efficiency dichroic coating, the laser/MWIR common aperture optical system with a 𝜑300 mm aluminum alloy mirror obtained images of buildings at a distance of 5 km with great quality. A civil aviation aircraft detection experiment was conducted. The results show that the common aperture system could detect and track long-distance civil aviation aircraft effectively, and the coverage was more than 450 km (signal-to-noise ratio = 6.3). It satisfied the application requirements for earlier warning and ranging of long-range targets in the area of aviation, aerospace and ground detection systems.

CCD를 이용한 선형예측기 (Linear Predictor Using Charge-Coupled Devices)

  • 최태영;신철재
    • 한국통신학회논문지
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    • 제12권1호
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    • pp.9-18
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    • 1987
  • DPCM의 선형예측기를 비감광성 원소(dummy pixel)를 가지고 있는 선형 감광성 전하결합소자(CCD)를 광전자 시스템으로 구현하는 방법을 제시하였다. 종래의 시스템과 마찬가지로 이 시스템은 입력광원, 공간여파기(마스크), 선형감광성 CCD의 3부분으로 구성되었다. 비감광성 원소에 의한 시간지연을 고려하여 종래의 마스크를 변형하여 각 예측계수를 하나 이상의 마스크 원소에 분산시킨, 새로운 방식의 분산형 마스크를 제시하고 이 마스크를 사용할 때의 특성을 이론적으로 분석하였으며 실험으로 확인하였다.

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실시간 연소제어를 위한 화염 내 라디칼 계측기법 연구 (An Experimental Study on the Measurement of Radicals in Flame for Real TIme Combustion Control)

  • 권승진;김세원;신명철;류태우;김용모
    • 한국연소학회:학술대회논문집
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    • 한국연소학회 2006년도 제33회 KOSCO SYMPOSIUM 논문집
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    • pp.53-59
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    • 2006
  • This study is measurement of radicals in gas & light oil diffusion flame focused on burner exit. The goal of this study is to analyse the relationship between flame chemiluminescence($OH^{\ast}$, $CH^{\ast}$, $C_2^{\ast}$) intensities and flame conditions. The investigation performed turbulent diffusion flame of commercial burner in varying the excess air ratio from 1.0 to 1.8. The optical emissions were measured by photomultiplier(PMT) using optical band pass filter and spectrometer system. The effects of excess air ratio and NOx emission characteristics on the radical emission intensities were investigated experimentally.

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MEASURING CROWN PROJECTION AREA AND TREE HEIGHT USINGLIDAR

  • Kwak Doo-Ahn;Lee Woo-Kyun;Son Min-Ho
    • 대한원격탐사학회:학술대회논문집
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    • 대한원격탐사학회 2005년도 Proceedings of ISRS 2005
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    • pp.515-518
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    • 2005
  • LiDAR(Light Detection and Ranging) with digital aerial photograph can be used to measure tree growth factors like total height, height of clear-length, dbh(diameter at breast height) and crown projection area. Delineating crown is an important process for identifying and numbering individual trees. Crown delineation can be done by watershed method to segment basin according to elevation values of DSMmax produced by LiDAR. Digital aerial photograph can be used to validate the crown projection area using LiDAR. And tree height can be acquired by image processing using window filter$(3cell\times3cell\;or\;5cell\times5cell)$ that compares grid elevation values of individual crown segmented by watershed.

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PSD의 신호 처리를 위한 AM 변조 및 복조 회로 (Signal Processing Algorithm for a PSD Sensor using Amplitude Modulation/Demodulation)

  • 라종필;신명관;박기환
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2003년도 학술회의 논문집 정보 및 제어부문 A
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    • pp.71-74
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    • 2003
  • The signal processing algorithm for a PSD(Position Sensitive Detector) using amplitude modulation/demodulation is addressed in this paper. Dark currents and external noises such as daylight and fluorescent lights are eliminated by using amplitude modulation/demodulation and a low pass filter. The proposed amplitude modulation/demodulation method for a PSD sensor is compared with pulse amplitude modulation method. The proposed amplitude modulation is proved to be more accurate and robust than PAM method by analysis and experiments. Multiple measurements using one PSD sensor by amplitude modulation/demodulation is also addressed. The Power variation of light source is compensated by normalization process using a divider.

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Production of Cellulase by Trichoderma reesei Rut C30 in a Batch Fermenter

  • Yu, Xiao-Bin;Yun, Hyun-Shik;Koo, Yoon-Mo
    • Journal of Microbiology and Biotechnology
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    • 제8권6호
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    • pp.575-580
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    • 1998
  • Cellulase production by batch culture using the Trichoderma reesei Rut C30 strain with various concentrations of Solka Floc with 1 % wheat bran was studied in a 2.5 I fermenter. The cellulase activity increased with Solka Floc concentration up to 5%. When 5% Solka Floc and 1% wheat bran were contained in the medium, carboxymethyl cellulose (CMC) and filter paper (FP) activities were 232.4 U/$m\ell$ and 21.25 U/$m\ell$, respectively. The productivity was 143.6 FPU $1^{-l}h^{-1}$ and the yield was 425 FPU/g. The colonial morphology of T. reesei Rut C30 grown on Avicel agar plates and the changes in mycelial morphology of T. reesei Rut C30 with culture time are also presented.

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실시간 연소제어를 위한 화염 내 라디칼 계측기법 연구 (An Experimental Study on the Measurement of Radicals in Flame for Real Time Combustion Control)

  • 신명철;김세원;류태우;권승진
    • 한국연소학회지
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    • 제11권3호
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    • pp.18-25
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    • 2006
  • The present studying is aimed to establish the relationship between flame chemiluminescence$(OH^*,\;CH^*,\;C_2^*)$ intensities and combustion conditions such as $NO_x$ emission characteristics. Measurements are made for $OH^*,\;CH^*,\;C_2^*$ radicals in gas & light oil diffusion flames. At turbulent nonpremixed combustion mode, the equivalence ratio is varied. The optical emissions were measured by photomultiplier(PMT) using optical band pass filter and spectrometer system. The experimental results showed that the ratio of radicals and $NO_x$ emission characteristics have exponential correlations and equivalence ratio characteristics have linear correlations at this experimental conditions.

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A Photometric Study of the W UMa-type Contact Binary GX Aurigae

  • Park, Jang-Ho;Kim, Chun-Hwey;Lee, Jae-Woo
    • 한국우주과학회:학술대회논문집(한국우주과학회보)
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    • 한국우주과학회 2008년도 한국우주과학회보 제17권2호
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    • pp.29.2-29.2
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    • 2008
  • The CCD photometric observations of the W UMa type contact binary GX Aur were performed for 33 nights from 2004 to 2008 using a 2K CCD camera and Johnson BVRI filter system attached to the 61cm reflector at Sobaeksan Optical Astronomy Observatory (SOAO). From our observations, the first BVRI light curves of GX Aur were completed and eight new times of minima (primary: 4, secondary: 4) were obtained. All the times of minima including our timings were collected and analyzed to see the dynamical behavior of GX Aur system. Intensive analysis of our BVRI lightcurves with the recent Wilson-Devinney binary model shows that GX Aur is an over-contact binary whose component stars have equal mass and time-variable spots.

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Cellulase Production in Fed-Batch Culture by Trichoderma reesei Rut C30

  • Yu, Xiao-Bin;Yun, Hyun-Shik;Koo, Yoon-Mo
    • Journal of Microbiology and Biotechnology
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    • 제9권1호
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    • pp.44-49
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    • 1999
  • Cellulase production by fed-batch cultivation of Trichoderma reesei Rut C30 with various initial concentrations of Solka Floc in 1 % wheat bran-containing medium was investigated. The cellulase activity and productivity increased with initial Solka Floc concentration up to 5%. When a total Solka Floc concentration of 90 g/l was used for cellulase production, CMC (carboxymethyl cellulose) and FP (filter paper) activities, productivity, and yield were 359.7 U/ml, 30.61 U/ml, 161 FPU $L^{-1}$ $h^{-1}$, and 340 FPU $g^{-1}$, respectively. It was important to maintain a high cell concentration during cellulase production to obtain high cellulase activity and productivity. Cellulase powder was prepared by ammonium sulfate precipitation: FP activity was 396.7 U/g and CMC activity was 6481 U/g.

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