• Title/Summary/Keyword: Large-grain

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Abnormal Grain Growth in Ferrites

  • Ito, Shigeru
    • Proceedings of the Korean Institute of Resources Recycling Conference
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    • 1999.09a
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    • pp.1-63
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    • 1999
  • Generation of abnormally large grains in the microstructure of small grains has been investigated on some ferrites. Some fractions of large grains were observed in the microstructure of sintered ZnFe$_2$O$_4$, Mn-ZnFe$_2$O$_4$, Fe$_3$O$_4$(in N$_2$) and MnFe$_2$O$_4$(in air). On the other hand, the large grains were not observed in NiFe$_2$O$_4$ and CoFe$_2$O$_4$, independent of calcining and sintering conditions. The large grains seem to be generated in such ferrites that are easy to vary their compositions or valencies at high temperatures. As the sintering proceeded, the number of large grains was increasing to form a continuous structure consisting of large grains, while the size of large grains did not increase remarkably. In addition, the growth of small grains was also very slow during the generation of the large grains. The large grains appeared to be suddenly generated after some induction periods. Avrami equation could be applied to the relation between net volume of large grains and sintering time. Thus, the grain boundaries may be strongly stabilized when the large grains are generated. The large grain in generated by the local activation of the stabilized grain boundaries, which is caused by the variation of compositions or valencies during sintering. It is concluded that the essence of the abnormal grain growth is not the generation of abnormally large grains, but the abnormal stabilization and the local activation of the grain boundaries.

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Studies on the Yield Potential Increment by Grain Weight in Rice I. Yield capacity and major agronomic characteristics of rice varieties with large grain (벼의 입중증대에 의한 수량성향상에 관한 연구 -제 1 보 대립 벼품종의 주요특성과 수량성-)

  • 양세준;황흥구;손재근
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.29 no.2
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    • pp.109-113
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    • 1984
  • This study was conducted to get basic information about yield capacity and major agronomic characteristics of rice varieties with large grain. The results obtained are as follows; Between grain weight and grain components such as length, width and thickness showed highly positive correlation. The relationship between grain length and grain shape (Length/Width) was clear (r=0.5707${\ast}\;{\ast}$). 1, 000 grain weight of 14 rice varieties with large grain was negatively correlated with number of spikelets per panicle, number of panicles per hill, ripening ratio, total dry matter, grain yield and harvest index, but less clear. The relationship between grain weight of 14 rice varieties with large grain and growth duration was less clear (r=0.440). 1, 000 grain weight of 20 rice varieties differing in grain size showed a highly positive correlation with chalkiness of rice kernel (r=0.8477${\ast}\;{\ast}$).

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Abnormal Grain Growth in Ferrites (페라이트 이상 입성장)

  • Shigeru Ito
    • Resources Recycling
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    • v.9 no.5
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    • pp.16-21
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    • 2000
  • Generation of abnormally large grains in the microstructure of small grains has been investigated on some ferrites. Some fractions of large grains were observed in the microstructue of sintered ZnFe$_2$O$_4$, Mn-ZnFe$_2$O$_4$, Fe$_3$O$_4$(in $N_2$) and MnFe$_2$O$_4$(in air). On the other hand, the large grains were not observed in $NiFe_2$$O_4$ and $CoFe_2$$O_4$, independent of calcining and sintering conditions. The large grains seem to be generated in such ferrites that are easy to very their compositions or valencies at high temperatures. as the sintering proceeded, the number of large grains was increasing to from a continuous structure consisting of large grains, while the size of large grains did not increase remarkably. In addition, the growth of small grains was also very slow during the generation of the large grains. The large grains appeared be suddenly generated after some induction periods. Avrami equation could be applied to the relation between net volume of large grains and sintering time. Thus, the grain boundaries may be strongly stabilized when the large grains are generated. The large grain is generated y the local activation of the stabilized rain boundaries, which is caused by the variation of composition or valencies during sintering. It is concluded that the essence of the abnormal gain growth is not the generation of abnormally large grains, but the abnormal stabilization and the local activation of he grain boundaries.

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Fabrication of 6.4 cm single grain $YBa_2$$Cu_3$$O_x$ (6.4cm 크기의 일방향 성장된Y$Ba_2$$Cu_3$$O_x$ 제조)

  • 박병삼;한상철;한영희;정년호;윤희중;김경진;성태현;오제명
    • Progress in Superconductivity
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    • v.5 no.2
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    • pp.114-117
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    • 2004
  • We fabricated large single grain YBa$_2$Cu$_3$O$_{x}$ (Y-123) superconductors. The single grain Y-123 was grown by top seeded melt growth (TSMG) method. In a conventional box furnace with uniform temperature distribution, it was very difficult to grow large single grain Y-123 superconductors due to the size limitation in growth. To overcome the size limitation, we applied a radial thermal gradient (lower temperature at sample center and higher temperature on the sample edge) to the TSMG process. In this case, large single grain Y-123 could be easily grown. This is attributed that the liquid of the sample edge was maintained at the high temperature compared to the growth front. Using this method, we successfully fabricated a large single grain Y-123 of 6.4 cm X6.4 cm

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The Effects of Seed Size on the Early Seedling Growth and Yield of Three Soybean(Glycine max. L.) Cultivars (대두종자(大豆種子)의 대소(大小)가 초기생육(初期生育) 및 수량(收量)에 미치는 영향(影響))

  • Park, Ki Sun;Choi, Chang Yeol;Kang, Jea Chul
    • Korean Journal of Agricultural Science
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    • v.16 no.2
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    • pp.138-151
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    • 1989
  • In order to find the effects of seed size on the early seedling growth and yield of soybean, three soybean cultivars in Korea were investigated. Seed size was classified into large and small according to the weight and planted in pots(1/5000a) and in the field. Three soybean cultivars respresenting large, medium and small grains were Hwangkeum-kong, Kwangkyo and Bangsa-kong respectively. These cultivars were planted on June 20, 1987. 1. The plant height, stem diameter, root length and leaf area index(LAI) of the seed with large size seemed larger than the seed with small size regardless of cultivars. 2. The fresh and dry weight were different depending upon the grain sizes. The large grain had heavier fresh and dry weight than the small grains. 3. The protein consumption rate of the cotyledon of Bangsa-kong with small grain size was faster than the Hwangkeum-kong with large grain size. 4. The stem length, stem diameter and number of main stem node of the seed with large size seemed larger than the seed with small size. Large grains of Hwangkeum-kong were the highest in the number of branch node and number of node. 5. The number of pods and grains per plant of Bangsa-kong with small grain size was larger than the Kwangkyo with large grain size. 6. The yield per 10a for Hwangkeum-kong, Hwangkyo and Bangsa-kong were 226.3kg, 193.0kg and 192.8kg, respectively and they were all statistically different. The yield increases of large grains over small grains in the Hwangkeum-kong, Kwangkyo, and Bangsa-kong were 7.4%, 8.0% and 9.2%, respectively.

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Grain Size Determination of Copper Film by Electron Backscatter Diffraction (EBSD를 이용한 구리박막의 결정립 크기 결정)

  • Kim, Su-Hyeon;Kang, Joo-Hee;Han, Seung Zeon
    • Korean Journal of Metals and Materials
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    • v.48 no.9
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    • pp.847-855
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    • 2010
  • The grain size of a cross-section of $8{\mu}m$-thick copper film was determined by electron backscatter diffraction analysis. Grain size distribution histogram showed the presence of a large fraction of small-sized grains, and the mean grain size was significantly affected by handling of them. A cut-off grain size, below which all grains are ignored as noise and eliminated for the calculation of the mean value, should be three or four times as large as the step size. Due to the presence of small grains, the linear intercept method derived larger mean grain size, which depends less sensitively on the cut-off grain size than the equivalent circle diameter method.

Bi-layer channel large grain TFT의 channel width의 변화에 따른 전기적 특성 비교 분석

  • Lee, Won-Baek;Park, Hyeong-Sik;Park, Seung-Man;Lee, Jun-Sin
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.430-430
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    • 2010
  • MICC 방법으로 제작된 TFT는 large grain과 그에 따른 grain boundary의 감소로 인하여여, 소자의 전기적 특성을 좋게 할 수 있다. 본 연구에서는 bi-layer channel의 large grain size TFT를 제작하여 소자의 전기적 특성을 비교하였다. Channel의 width / length의 크기는 각 각의 경우 $7/5{\times}2$, $10/5{\times}2$, $15/5{\times}2$ (${\mu}m$)로 하였다. 소자의 성능 측정 결과 Field-effect mobility의 경우에는 channel width가 증가할 수록 감소하는 경향성을 나타내었으며, Threshold voltage의 경우에는 조금 감소하는 경향성은 있었으나 변화의 폭이 매우 작았다. Output characteristics 의 경우에는 모든 set에서 좋은 saturation 특성을 보였다. 이것은 current croding이 없었다는 것을 의미하는데, 큰 grain size로 인한 효과로 해석 할 수 있다. 본 연구에서는 bi-layer channel에서 corner effect에 중점을 두어 소자의 전기적 특성 변화에 대하여 논하였다.

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Electrical characteristics of Large-grain TFT induced with Ni (Ni로 유도된 Large-grain TFT의 전기적 특성)

  • Lee, Jin-Hyuk;Lee, Won-Baek;Yi, Jun-Sin
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2010.06a
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    • pp.367-367
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    • 2010
  • Electrical characteristics of Large-grain silicon with Ni-induced crystallization which gate insulator is made of 80 nm $SiO_2$ and 20 nm SiNx was fabricated and measured with different channel widths, channel length fixed $10{\mu}m$. Focusing on the changes of channel widths from $4{\mu}m$ to $40{\mu}m$. Field-effect mobility decreased from 111.30 to $94.10\;cm^2/V_s$ when the channel widths increased. Still threshold voltage was almost similar with -1.06V.

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Variation of Dielectric Constnat with Grain Size of Pyrochlore Phase in the PMN-Pyrochlore Diphasic Mixtrues (Pyrochlore상의 입자크기에 따른 PMN-Pyrochlore 2상 혼합체의 유전율 변화)

  • 허강일;김정주;조상희
    • Journal of the Korean Ceramic Society
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    • v.30 no.5
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    • pp.365-372
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    • 1993
  • Variation of dielectric constant in PMN-Pyrochlore diphasic mixtures were investigated with grain size of pyrochlore phase. Size of pyrochlore phase was controlled by the numbers of calcining and sedimentation method during powder processing. When grain size of pyrochlore phase is large in the sintered specimen, dielectric constant slowly decreased with increase of amount of pyrochlore phase. On the contary, grain size of pyrochlore phase is small, dielectric constant drastically decreased. It was thought that small sized pyrochlore grains more easily surrounded high dielectric phase (perovskite PMN) than large ones with addition of pyrochlore phase.

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The Influence of Grain Size on the Fatigue Crack Propagation Behavior in the Low Carbon Steel (SM26C) (저탄소강재(SM25C)의 피로크랙 전파거동에 미치는 결정립 크기의 영향)

  • 김건호
    • Journal of Advanced Marine Engineering and Technology
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    • v.26 no.1
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    • pp.76-82
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    • 2002
  • In this study, the rotary bending fatigue test was carried out with low carbon steel(SM25C). The specimens were heat-treated in order to change the grain size, and investigated items are fatigue limit, small crack initiation, fatigue crack propagation behavior and possibility of fatigue life prediction according to the different grain size. The summarized result are as follows ; Fatigue limit of the smooth specimen was dependent upon the grain size. The fatigue crack initiation of the small grain size specimen was delayed more than that of the large grain size specimen. And the small cracks of small grain size specimen were distributed in the narrow region of the main crack circumference contrary to the large grain size specimen. The main crack was grown along the grain boundary having co-alliance with small cracks. The experiment material has quantitatively disclosed the possibility of fatigue life prediction because the fatigue crack propagation behavior is dependent upon the grain size.