• Title/Summary/Keyword: Laboratory test

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Proficiency testing of cadmium and lead in polypropylene resin (폴리프로필렌 수지 중 카드뮴과 납 측정 숙련도시험)

  • Cho, K.H.;Lim, M.C.;Min, H.S.;Han, M.S.;Song, H.J.;Park, C.J.
    • Analytical Science and Technology
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    • v.20 no.3
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    • pp.183-192
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    • 2007
  • The various environmental regulation directives such as RoHS (restriction of hazardous substances in electrical and electronic products) and WEEE (waste from electrical and electronic equipments) are practically used as the technical barrier in international trade (TBT) of vehicles and electrical and electronic products recently. Regarding such an environmental regulation, Korea Research Institute of Standards Science (KRISS) organized a proficiency testing scheme to establish the reliability of measurement results produced by the relevant research institutes and test laboratories in Korea. Participants were 31 laboratories related to production of the electrical and electronic equipments and mobile vehicles. Two polypropylene samples of pellet type were employed as the proficiency testing materials (PTMs). Cadmium and lead were the analytes chosen among six components regulated in European Union (EU) RoHS directive. The PTMs were sent to the participants by post on September $1^{st}$ 2006, and deadline for results submission were October $10^{th}$ 2006. The results of each laboratory were evaluated in comparison with KRISS reference values using Robustic Z-score and Youden plot methods. The results of the various sample digestion methods were also compared. Most of participants reported good agreement within 10 % range of reference values. However, results from several laboratories showed significant biases from reference values. These laboratories should establish the quality assurance system for improvement of the measurement reliability.

Analysis of Solute Transport based on Electrical Resistance Measurements from Laboratory Column Tests (전기저항센서가 부착된 주상실험기에서 측정된 전기저항값을 이용한 용질의 이동해석)

  • Kim, Yong-Sung;Kim, Jae-Jin;Park, Junboum
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.28 no.4C
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    • pp.231-238
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    • 2008
  • A column testing device capable of measuring the electrical resistivity of soil at 3 different locations was developed to verify applicability of bulk electrical conductivity (BEC) breakthrough curves in monitoring contaminant transport. Tracer injection tests were conducted with three different types of saturated sands to obtain average linear velocities and longitudinal hydrodynamic dispersion coefficients based on BEC breakthrough curves and effluent solute breakthrough curves. Comparative analysis of transport parameters obtained from curve fitting the results into the analytical solutions confirmed the validity of resistance measurements in estimating time-continuous resident solute concentration. Under the assumption that a linear relationship exists between ${\sigma}_{sat}-{\sigma}_w-C$, the BEC breakthrough curves are able to effectively reduce the laborious and time-consuming processes involved in the conventional method of sampling and analysis. In order to reduce possible uncertainties in analyzing the BEC breakthrough curves, it was recommended that resistance measurements take place nearby the effluent boundary. In addition, a sufficient electrical contrast or difference in the electrical conductivity of the influent and the saturating solution is required to conduct reliable analysis.

An Estimation on the Applicability of Hollow FRP Soil Nailing System (중공식 FRP쏘일네일링 시스템의 적용성 평가)

  • Lee, Hyuk-Jin;Koh, Hyung-Seon;Han, Yong-Hee;Kim, Hong-Taek
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.26 no.6C
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    • pp.385-393
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    • 2006
  • Soil nailing is a reinforcement method used for stabilizing excavated walls or slopes. Due to its much advantages such as ease of construction and economical efficiency, use of soil nailing is increased. However, the soil nail has much disadvantages for use in urban area. The soil nail needs to be installed inevitably beyond private land boundary, which causes rent for use. For this reason, removable soil nailing system was developed. However, the removal rate of this system is just about 50¢¦70%. To resolve this problem, the Fiber Reinforced Plastic (FRP) soil nailing system which does not need to be removed and allows for the installation beyond private land, is developed. In this paper, through theoretical and experimental studies in laboratory and field such as prototype tests, pullout tests, we evaluate the stability and behavior characteristics of the FRP soil nailing system. And, numerical analyses using FLAC2D were performed with respect to various soil conditions, where prototype test for excavation wall and pullout tests were carried out. As a result of this study, the FRP soil nailing systems show similar behavior characteristics with those of removable soil nailing system. Finally, considering the serviceability and mechanical stability of FRP soil nailing systems, it is enough to be used as a good alternative of general soil nailing system.

Evaluation of bonding state of shotcrete lining using nondestructive testing methods - experimental analysis (비파괴 시험 기법을 이용한 숏크리트 배면 접착상태 평가에 관한 실험적 연구)

  • Song, Ki-Il;Cho, Gye-Chun;Chang, Seok-Bue;Hong, Eun-Soo
    • Journal of Korean Tunnelling and Underground Space Association
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    • v.11 no.1
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    • pp.71-83
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    • 2009
  • Shotcrete is an important primary support for tunnelling in rock. The quality control of shotcrete is a core issue in the safe construction and maintenance of tunnels. Although shotcrete may be applied well initially onto excavated rock surfaces, it is affected by blasting, rock deformation and shrinkage and can debond from the excavated surface, causing problems such as corrosion, buckling, fracturing and the creation of internal voids. This study suggests an effective non-destructive evaluation method of the tunnel shotcrete bonding state applied onto hard rocks using the impact-echo (IE) method and ground penetration radar (GPR). To verify previous numerical simulation results, experimental study carried out. Generally, the bonding state of shotcrete can be classified into void, debonded, and fully bonded. In the laboratory, three different bonding conditions were modeled. The signals obtained from the experimental IE tests were analyzed at the time domain, frequency domain, and time-frequency domain (i.e., the Short- Time Fourier transform). For all cases in the analyses, the experimental test results were in good agreement with the previous numerical simulation results, verifying this approach. Both the numerical and experimental results suggest that the bonding state of shotcrete can be evaluated through changes in the resonance frequency and geometric damping ratio in a frequency domain analysis, and through changes in the contour shape and correlation coefficient in a time-frequency analysis: as the bonding state worsens in hard rock condition, the autospectral density increases, the geometric damping ratio decreases, and the contour shape in the time-frequency domain has a long tail parallel to the time axis. The correlation coefficient can be effectively applied for a quantitative evaluation of bonding state of tunnel shotcrete. Finally, the bonding state of shotcrete can be successfully evaluated based on the process suggested in this study.

Calcium-doped zinc oxide nanocrystals as an innovative intracanal medicament: a pilot study

  • Gabriela Leite de Souza;Thamara Eduarda Alves Magalhaes;Gabrielle Alves Nunes Freitas;Nelly Xiomara Alvarado Lemus;Gabriella Lopes de Rezende Barbosa;Anielle Christine Almeida Silva;Camilla Christian Gomes Moura
    • Restorative Dentistry and Endodontics
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    • v.47 no.4
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    • pp.38.1-38.15
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    • 2022
  • Objectives: This study investigated the cytotoxicity, radiopacity, pH, and dentinal tubule penetration of a paste of 1.0% calcium-doped zinc oxide nanocrystals (ZnO:1.0Ca) combined with propylene glycol (PRG) or polyethylene glycol and propylene glycol (PEG-PRG). Materials and Methods: The pastes were prepared by mixing calcium hydroxide [Ca(OH)2] or ZnO:1.0Ca with PRG or a PEG-PRG mixture. The pH was evaluated after 24 and 96 hours of storage in deionized water. Digital radiographs were acquired for radiopacity analysis and bubble counting of each material. The materials were labeled with 0.1% fluorescein and applied to root canals, and images of their dentinal tubule penetration were obtained using confocal laser scanning microscopy. RAW264.7 macrophages were placed in different dilutions of culture media previously exposed to the materials for 24 and 96 hours and tested for cell viability using the MTT assay. Analysis of variance and the Tukey test (α = 0.05) were performed. Results: ZnO:1.0Ca materials showed lower viability at 1:1 and 1:2 dilutions than Ca(OH)2 materials (p < 0.0001). Ca(OH)2 had higher pH values than ZnO:1.0Ca at 24 and 96 hours, regardless of the vehicle (p < 0.05). ZnO:1.0Ca pastes showed higher radiopacity than Ca(OH)2 pastes (p < 0.01). No between-material differences were found in bubble counting (p = 0.0902). The ZnO:1.0Ca pastes had a greater penetration depth than Ca(OH)2 in the apical third (p < 0.0001). Conclusions: ZnO:1.0Ca medicaments presented higher penetrability, cell viability, and radiopacity than Ca(OH)2. Higher values of cell viability and pH were present in Ca(OH)2 than in ZnO:1.0Ca.

Application of Near-Infrared Spectroscopy in Neurological Disorders: Especially in Orthostatic Intolerance (신경계 질환에서 근적외선분광분석법의 적용: 기립불내증을 중심으로)

  • Kim, Yoo Hwan;Paik, Seung-ho;Phillips V, Zephaniah;Seok, Hung Youl;Jeon, Nam-Joon;Kim, Beop-Min;Kim, Byung-Jo
    • Journal of the Korean neurological association
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    • v.35 no.1
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    • pp.8-15
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    • 2017
  • Near-infrared spectroscopy (NIRS), a noninvasive optical method, utilizes the characteristic absorption spectra of hemoglobin in the near-infrared range to provide information on cerebral hemodynamic changes in various clinical situations. NIRS monitoring have been used mainly to detect reduced perfusion of the brain during orthostatic stress for three common forms of orthostatic intolerance (OI); orthostatic hypotension, neurally mediated syncope, and postural orthostatic tachycardia syndrome. Autonomic function testing is an important diagnostic test to assess their autonomic nervous systems for patients with symptom of OI. However, these techniques cannot measure dynamic changes in cerebral blood flow. There are many experimentations about study of NIRS to reveal the pathophysiology of patients with OI. Research using NIRS in other neurologic diseases (stroke, epilepsy and migraine) are ongoing. NIRS have been experimentally used in all stages of stroke and may complement the established diagnostic and monitoring tools. NIRS also provide pathophysiological approach during rehabilitation and secondary prevention of stroke. The hemodynamic response to seizure has long been a topic for discussion in association with the neuronal damage resulting from convulsion. One critical issue when unpredictable events are to be detected is how continuous NIRS data are analyzed. Besides, NIRS studies targeting pathophysiological aspects of migraine may contribute to a deeper understanding of mechanisms relating to aura of migraine. NIRS monitoring may play an important role to trend regional hemodynamic distribution of flow in real time and also highlights the pathophysiology and management of not only patients with OI symptoms but also those with various neurologic diseases.

Rice (Oryza sativa L.) Growth Promotion by Various Plant Extracts Produced Using Different Extraction Methods

  • Ei Ei;Hyun Hwa Park;Yong In Kuk
    • Proceedings of the Korean Society of Crop Science Conference
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    • 2022.10a
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    • pp.53-53
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    • 2022
  • Modem agricultural production needs to provide sustainable management practices that are eco-friendly and low cost. Plant extracts are a cost-effective and environmentally friendly alternative to synthetic plant growth regulators. This study was therefore carried out to investigate the effects of various plant extracts produced using different extraction methods on the vegetative growth of rice under laboratory and greenhouse conditions. For this study, seventeen plant extracts were made from plant species such as leaves of M. arvense, C. asiatica, M. oleifera, V. radiata, V. unguiculate, P. guajava, A. vera, and A. tuberosum, aboveground plant parts of C. rotundus, M. sativa, and P. frutescens, roots of R. undulatum, tubers of A. sativum, leaves and stems of G. max (cv. Taegwang) as well as rice straw and hulls (cv. Hopyeong). As a test crop, we applied these extracts to rice plants. For the purpose of making our extracts, some plant materials and species were collected in fields and others were purchased from Chonnam Hanyaknonghyup Cooperation (South Korea). Leaves, roots, and aboveground plant parts of plant species were dried, ground, extracted (water, boiling water and ethanol) and fermented. Rice growth promotion effects were determined using plant extracts at 0, 0.05, 0.1, 0.5, and 1% concentrations under petri dish conditions. Seven selected plant extracts were applied to rice seeds with soil drench application or seedling at 3-4 leaf stages with soil and foliar applications under greenhouse conditions. For comparison with extracts, we used urea at 0.6%. Of the 17 water extracts used in this study, 10 extracts reduced rice growth, but the other 7 extracts (P. guajava, A. vera, A. tuberosum, M. sativa, A. sativum, and G. max) increased growth by 40-60% on compared to the control in Petri dish bioassay. Thus, these 7 extracts were selected for further study. Under greenhouse conditions, rice growth also increased by 20-40% when the same 7 extracts were applied to rice seeds using soil drench application. Furthermore, at the 3-4 leaf stage rice growth also increased 30-80% or 30-60% when the same 7 extracts were applied using soil and foliar applications. Overall, the 7 extracts produced higher rates of growth promotion when soil drench application was used than when foliar application was used. In the case of boiling water and ethanol extracts, rice growth increased only 20% in response to both soil drench and foliar application of the same 7 extracts. Rice growth promotion was greater when extracts were produced using water extraction method than boiling water and ethanol extraction methods. Most notably, the 7 water extracts used in this study produced higher rates of growth promotion than urea at 0.6% which is typically used for crop growth promotion. Overall, the 7 water extracts when applied using soil drenching method can be used as effective growth promotors of rice in organic agriculture.

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Effects of Functional Improvement of Multiaxis Flat Continuous Soil Cement Earth Retaining Wall (다축 평면 연속형 SCW 흙막이 벽체의 개선 효과)

  • Chung, Choong-Sub;Yoo, Chan Ho;Nam, Ho Seong;Choi, In Gyu;Baek, Seung Cheol
    • Journal of the Korean Geotechnical Society
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    • v.39 no.11
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    • pp.7-22
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    • 2023
  • In January 2022, a new legislation was enforced to enhance the safety of underground construction. Consequently, a comprehensive assessment of underground safety is now an integral part of the planning process, including an evaluation of its impact. Ensuring the stability of temporary retaining walls during underground excavation has become paramount, prompting a heightened focus on the assessment of underground safety. This study delves into the analysis of the Multi-axis Flat Continuous Soil Cement Wall retaining wall (MFS) construction method. This method facilitates the expansion of wall thickness in the ground and provides flexibility in selecting and spacing H-piles. Through laboratory model tests, we scrutinized the load-displacement behavior of the wall, varying the H-pile installation intervals using the MFS method. Additionally, a 3-dimensional numerical analysis was conducted to explore the influence of H-pile installation intervals and sizes on the load for different thicknesses of the MFS retaining wall. The displacement analysis yielded the calculation of the height of the arching effect acting on the wall. To further our understanding, a design method was introduced, quantitatively analyzing the results of axial force and shear force acting on the wall. This involved applying the maximum arching height, calculated by the MFS method, to the existing member force review method. The axial force and shear force, contingent on the H-pile installation interval and size applied to the MFS retaining wall, demonstrated a reduction effect ranging from 24.6% to 62.9%.

The Quality Control Method in the Laboratory Analysis of Aquatic Ecosystem Health Monitoring and Assessment: Permanent Mounting Slides Tool Development Using Benthic Attached Diatoms. (수생태계 건강성 조사·평가를 위한 실내분석 정도관리 방법: 부착돌말류 영구표본 분석도구 개발)

  • Jae-Ki Shin;Nan-Young Kim;Yongeun Park;Kyung-Lak Lee;Baik-Ho Kim;Yong-Jae Kim;Han-Soon Kim;Jung Ho Lee;Hak Young Lee;Soon-Jin Hwang
    • Korean Journal of Ecology and Environment
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    • v.56 no.3
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    • pp.196-206
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    • 2023
  • Benthic attached diatoms (BADs), a major primary producer in lotic stream and river ecosystems are micro-sized organisms and require a highly magnified microscopic technique in the observation work. Thus, it is often not easy to ensure accuracy and precision in both qualitative and quantitative analyses. This study proposed a new technique applicable to improve quality control of aquatic ecosystem monitoring and assessment using BADs. In order to meet the purpose of quality control, we developed a permanent mounting slide technique which can be used for both qualitative and quantitative analyses simultaneously. We designed specimens with the combination of grid on both cover and slide glasses and compared their efficiency. As a result of observation and counting of BADs, the slide glass designed with the color-lined grid showed the highest efficiency compared to other test conditions. We expect that the method developed in this study could be effectively used to analyze BADs and contributed to improve the quality control in aquatic ecosystem health monitoring and assessment.

Correlation Analysis of Cutter Acting Force and Temperature During the Linear Cutting Test Accompanied by Infrared Thermography (선형절삭시험과 적외선 열화상 측정을 통한 픽커터 작용력과 발생 온도의 상관관계 분석)

  • Soo-Ho Chang;Tae-Ho Kang;Chulho Lee;Hoyoung Jeong;Soon-Wook Choi
    • Tunnel and Underground Space
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    • v.33 no.6
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    • pp.519-533
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    • 2023
  • In this study, the linear cutting tests of pick cutters were carried out on a granitic rock with the average compressive strength over 100 MPa. From the tests, the correlation between the cutter acting force and the temperature measured by infrared thermal imaging camera during rock cutting was analyzed. In every experimental condition, the maximum temperature was measured at the rock surface where the chipping occurred, and the temperature generated in the rock was closely correlated with the cutter acting force. On the other hand, the temperature of a pick cutter increased up to only 36℃ above the ambient temperature, and the correlation with the cutter force was not obvious. This can be attributed to the short cutting distance under laboratory conditions and the high thermal conductivity of the tungsten carbide inserts. However, the relatively high temperature of the tungsten carbide inserts was found to be maintained. Therefore, it is recommended that a reinforcement between the insert and the head of a pick cutter or the quality improvement of silvering brazing in the production of a cutter is necessary to maintain the high cutting performance of a pick cutter.