• Carbon letters
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• v.3 no.1
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• pp.33-38
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• 2002

Petroleum based isotropic pitch was spun into short fiber by melt-blown spinning technology. The processing parameters chosen were air velocity, die temperature, and throughput rate of the pitch within the ranges of experimental tolerances. The fiber diameter was reduced to $6{\mu}m$ by increases of hot air velocity, and spin die temperature. Also, the fiber diameter was strongly dependent on the throughput rate of the pitch and jet speed of hot air through the spinnerets. Even fibers with $10{\mu}m$ diameter were produced at throughput rate of $0.17g/min{\cdot}hole$ and at die temperature of $290^{\circ}C$.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2005.11a
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• pp.422-425
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• 2005

In an transversely isotropic composite laminates, the velocities, the particle directions and the amplitudes of reflected and transmitted waves were obtained using the equation of motion, the constitutive equation, and the displacement equation expressed by wave number and frequency Eigenvalue problem involving a velocity was solved by Snell's law. Finally, the results were confirmed by T300 Carbon fiber/5208 Epoxy materials. This approach could be applied to the detection of flaws in a transversely isotropic composite laminates by the water immersion C-scan procedure.

• Journal of the Korean Society of Propulsion Engineers
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• v.10 no.2
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• pp.62-69
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• 2006

In transversely isotropic composite laminates, the velocities, the particle directions and the amplitudes of reflected and transmitted waves were obtained using the equation of motion, the constitutive equation, and the displacement equation expressed by wave number and frequency. Eigenvalue problem involving a velocity was solved by Snell's law. Finally, the results were confirmed by 7300 Carbon fiber/5208 Epoxy materials. This approach could be applied to the detection of flaws in transversely isotropic composite laminates by the water immersion C-scan procedure.

• Carbon letters
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• v.3 no.2
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• pp.80-84
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• 2002

The surface treatment of C-type isotropic pitch-based carbon fiber was carried out by anodic oxidation in 5 wt% $NH_4NO_3$ electrolyte. The changes of fiber surface and carbon fiber/ABS resin composites were characterized by SEM, XPS and mechanical properties test. The oxygen functional groups on the surface, such as hydroxyl (-C-OH), carboxyl (-COOH) groups etc., increased after oxidation. Tensile strength, flexural strength and modulus of carbon fiber/ABS composites were also enhanced. However, the impact strength decreased with the improvement of the surface adhesion between CF and matrix.

• Carbon letters
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• v.7 no.2
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• pp.114-118
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• 2006

Isotropic pitch-based carbon fiber has been activated by steam diluted in nitrogen in order to characterize the microporosity. Especially, 40 wt% burn-off ACFs were prepared from different conditions to compare the pore structure and size. The ACFs were thinly sliced to investigate the inside pores by TEM and image analyzer. As expected, the adsorption characteristics of these ACFs were quite different from one another because of different pore structure and size. Most pores are not slit-shaped but rather round. Small round micropores become broad and irregular as increasing the activation time and temperature.

• Carbon letters
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• v.10 no.3
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• pp.202-207
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• 2009

Pitch-based carbon fiber tows were prepared from naphtha cracking bottom oil by reforming and carbonization. The relationship between exothermic heat and carbon contents of the fiber was investigated by changing the carbonization conditions. The carbon contents and the crystallinities of isotropic pitch-based carbon fibers were 86.8~93.8 wt% and 33.7~40.1%, respectively, which were linearly proportional to the increase of carbonization temperature from 700 to $1000^{\circ}C$. The exothermic heat (temperature increase) of fiber tows was measured in a short time, which was also linearly proportional to the increase of carbon contents due to the increase of crystallinity, even though the crystallinity was low. Therefore, the carbon contents or carbonization degree of fibers can rapidly and indirectly be estimated by measuring the surface temperature increase of fibers.

• Journal of Industrial and Engineering Chemistry
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• v.67
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• pp.276-283
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• 2018

For the first time, polyvinyl chloride (PVC) was used as an easily-handled chlorine source for preparation of isotropic pitch-based carbon fiber (IPCF) incorporating ethylene bottom oil (EO) as a raw material. Pitch precursors were prepared by the chlorination-dehydrochlorination triggered by chlorine radicals originated from PVC; aromatization and poly-condensation reactions occurred by polyene-type radicals from PVC. Radical production and co-carbonization were facilitated by pretreatments of EO through vacuum distillation, bromination, and additional heat treatment. Pitches were prepared by the co-carbonization of pretreated EO and EO containing 20 wt% PVC, and had higher yields and better spinnability than those by simple distillation.

• Journal of the Korean Applied Science and Technology
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• v.22 no.2
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• pp.91-95
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• 2005

Carbon composites were prepared with pitch-based round, C, hollow-type carbon fibers and pitch matrix. The thermal conductivities parallel and perpendicular to the fiber axis were measured by steady-state method. It was found that the thermal conductivities depended on the cross-sectional forms of the reinforcing fibers as well as the reinforcing orientation and carbon fiber precusors. Especially, mesophase pitch-based hollow carbon fiber-carbon composites had the most excellent thermal anisotropy, which was above 100.

• Proceedings of the Korea Concrete Institute Conference
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• 2002.10a
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• pp.313-318
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• 2002

The use of carbon fiber rods is a promising technology of increasing flexural and shear strength of deficient reinforced concrete members. The purpose of this experimental study is to investigate the fatigue behavior and strengthening effects of the strengthened bridge deck with isotropic and othortropic carbon fiber rod. This study shows a fatigue loading, compliance and S-N Curve between strengthened isotropically and othortropically. Then estimate the effective fatigue behavior of RC slab using composite rods that are inserted in high special purposed polymer mortar.

• Proceedings of the Korea Concrete Institute Conference
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• 2001.11a
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• pp.757-762
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• 2001

This study was performed experiment for strengthened bridge decks with isotropic carbon fiber sheets received fatigue loading, and compared with fatigue behavior of unstrengthened bridge decks. By the results, this study was examined effect of increasing strengthened to phase life cycles of bridge deck for fatigue loading and application of the punching shear theory of bridge deck strengthened by carbon fiber sheet.