• 한국산업융합학회 논문집
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• 제5권4호
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• pp.361-366
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• 2002

The change of mechanical properties of drawn PP filaments which was treated by isothermally annealed after elevated heating. Measurements were carried out with UTM for mechanical properties. Isothermally heat treatment were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min, in silicon oil bath. And isothermally heat treatment after elevated heating from $20^{\circ}C$ were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min., with heating rate of $1^{\circ}C/min$., $5^{\circ}C/min$., $10^{\circ}C/min$. From the results of this study, it found the following facts. Initial modulus and tensile strength were increased with increasing of annealed temperature and time. Also initial modulus of tensile strength of samples which were isothermally annealed after elevated heating from $20^{\circ}C$ were higher than those of isothermally annealed samples.

• 한국산업융합학회 논문집
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• 제6권4호
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• pp.387-392
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• 2003

The change of crystalline structure and mechanical properties of PET filaments were investigated. Samples were treated by isothermally annealed after elevated heating. Measurements were carried out of density gradient tube for crystallinity and UTM for initial modulus and yield stress. Isothermally heat treatment were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min, in silicon oil bath. And isothermally heat treatment after elevated heating from $20^{\circ}C$ were carried out $100^{\circ}C$, $120^{\circ}C$, $140^{\circ}C$ for 10min., 30min., 60min., with heating rate of $5^{\circ}C/min$., $10^{\circ}C/min$. From the results of this study, it found the following facts. It was found that the crystallinity, initial modulus and yield stress of samples were increased with increasing of annealed temperature and time. Also crystallinity, initial modulus and yield stress of samples which were isothermally annealed after elevated heating from $20^{\circ}C$ were larger than those of isohtermally annealed samples.

• 한국산업융합학회 논문집
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• 제3권4호
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• pp.345-351
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• 2000

The change of crystalline structure of drawn PP filaments were investigated. Samples were treated by isothermally annealed after elevated heating from $20^{\circ}C$. Measurements were carried out with XRD for crystallite size and density gradient tube for crystallinity. Isothermally heat treatment were carried out at the temperature of $100^{\circ}C$, $120^{\circ}C$ and $140^{\circ}C$ for 10min., 30min. and 60min. in dry oven. The isothermal heat treatment after elevated heating from $20^{\circ}C$ were carried out at the temperature of $100^{\circ}C$, $120^{\circ}C$ and $140^{\circ}C$ for 10min., 30min. and 60min. with heating rate of $1^{\circ}C$/min., $5^{\circ}C$/min. and $10^{\circ}C$/min. From the results of this study, it found the following facts. It was found that the crystallinity and crystallite size of (110) plane of sample were increased with increasing of annealed temperature and time. Also crystallinity and crystallite size of samples which were isothermally annealed after elevated heating from $20^{\circ}C$ were higher than those of isohtermally annealed samples.

• 열처리공학회지
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• 제9권1호
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• pp.27-33
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• 1996

Metallographic observation was carried out by scanning and transmission electron microscopy to evaluate microstructural characteristics of partially austenitized and isothermally transformed 1.0C-1.5Cr bearing steel. It was observed that lower bainite formed in the local region of specimen partially austenitized and isothermally held at $250^{\circ}C$ for 1/3 hr and formed in almost all area of the specimen isothermally held at $250^{\circ}C$ for 2 hrs. Lower bainitic carbides with midrib was also observed in the specimen partially austenitized and isothermally held at $250^{\circ}C$ for 4 hrs. Midrib was nearly carbide-free region and thicker in the vicinity of spherical carbides than the other region. Lengthening speed of lower bainitic carbides was remarkabey increased at isothermal holding time ranging from 2 hrs to 4 hrs.

• 열처리공학회지
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• 제27권1호
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• pp.15-22
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• 2014

This study is to investigate the phase changes and cold workability after isothermal transformation at $780^{\circ}C$ by using the high temperature gas nitrided (HTGN) STS 430 ferritic stainless steel specimens. The phase diagram of STS 430 steel obtained by calculation showed that the phase appeared at $1100^{\circ}C$ showed as ${\alpha}+{\gamma}{\rightarrow}{\gamma}{\rightarrow}{\gamma}+Cr_2N{\rightarrow}{\gamma}+Cr_2N+CrN$ with increasing nitrogen concentration. Also, the transformation of ${\gamma}{\rightarrow}Cr_2N$ during heat treatment isothermally at $780^{\circ}C$, nitrogen pearlite with lamellar type was fully formed at the nitrogen permated surface layer for 10 hrs. However, this transformation was not completed for 1 hr, resulting nitrogen pearlite plus martensite. The cold rolled specimen of isothermally transformed at $780^{\circ}C$ for 10 hrs after high temperature gas nitriding decreased the layer thickness of nitrogen pearlite inducing the deformation of hard $Cr_2N$ phase. the dissolution rate of $Cr_2N$ phase increased rapidly with increasing cold rolling ratio. Specimens with the microstructure of nitrogen pearlite (isothermally transformed at $780^{\circ}C$ for 10 hrs) were possible to cold rolling without crack formation. However, the mixed structures of nitrogen pearlite + martensite (isothermally transformed at $780^{\circ}C$ for 1 hr) were impossible to cold deformation without cracking.

• 열처리공학회지
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• 제8권4호
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• pp.302-317
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• 1995

After initial structure of AISI 9260 steel is changed into pearlite and martensite, one is isothermally annealed at $700^{\circ}C$ below of $A_1$ transformation point and the other is isothermally annealed at the same condition after 3 cycles of heating and cooling between $680^{\circ}C$ and $780^{\circ}C$ of $A_1$ transformation point. Analyzing the changes of microstructure, mechanical properties and fractography of tension test, we obtained result as follows. The fastest spheroidization rate by changes of initial structure and heat treatment cycles is appeared at the heat treatment cycle which is isothermally annealed after 3 cycles of heating and cooling at below and above $A_1$ transformation point for martensite. At the above condition, the perfect spheroidization structure is appeared after 60hrs and after then, globular carbide is being coarsened. The mean diameter of globular carbide is $2.4{\times}10^{-3}mm$ after 90hrs. The changes of tension strength during spheroidization heat treatment follows Orwan function, ${\sigma}_o={\sigma}_i+Gb/l$, where l is interspacing of carbide particles and at the above condition, ${\sigma}_o=70.48+2.5{\times}10^{-3}/l(kg/mm^2)$. Fractography of fracture of spheroidization structure in tension test is appeared as dimple which is ductile rupture type by nucleation and growth of void, size of dimple is larger and deeper with increasing of heat treatment time.

• 열처리공학회지
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• 제14권3호
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• pp.167-178
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• 2001

• 한국재료학회지
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• 제28권9호
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• pp.522-527
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• 2018

This study investigates the effects of isothermal holding temperature and time on the microstructure, hardness and Charpy impact properties of medium-carbon bainitic steel specimens. Medium-carbon steel specimens with different bainitic microstructures are fabricated by varying the isothermal conditions and their microstructures are characterized using OM, SEM and EBSD analysis. Hardness and Charpy impact tests are also performed to examine the correlation of microstructure and mechanical properties. The microstructural analysis results reveal that granular bainite, bainitic ferrite, lath martensite and retained austenite form differently in the specimens. The volume fraction of granular bainite and bainitic ferrite increases as the isothermal holding temperature increases, which decreases the hardness of specimens isothermally heat-treated at $300^{\circ}C$ or higher. The specimens isothermally heat-treated at $250^{\circ}C$ exhibit the highest hardness due to the formation of lath martensite, irrespective of isothermal holding time. The Charpy impact test results indicate that increasing isothermal holding time improves the impact toughness because of the increase in volume fraction of granular bainite and bainitic ferrite, which have a relatively soft microstructure compared to lath martensite for specimens isothermally heat-treated at $250^{\circ}C$ and $300^{\circ}C$.

• 열처리공학회지
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• 제15권1호
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• pp.3-8
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• 2002

The effect of ADI heat treatment conditions on the core microstructures and mechanical properties of GCD 45 has been investigated. In the case of $25{\ss}{\AE}$ in diameter, it has been found that pearlite structure is not obtained, and the matrix is consisted of graphite, bainite and retained austenite. Upon cooling isothermally from $900^{\circ}C$, the core structure of 35 mm in diameter is converted to pearlite. However, the structure is transformed to bainite after slow cooling from $900^{\circ}C$ to $800^{\circ}C$.

• 열처리공학회지
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• 제21권1호
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• pp.3-9
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• 2008

Al-Co-N thin films, Al-Co-N/Al-N and Al-Co-N/Al-Co multilayers containing various amounts of Co content were deposited by using a two-facing targets type dc sputtering (TFTS) system. The films were also annealed successively and isothermally at different annealing temperatures. Irrespective of Co content and preparation methods, all the as-deposited films were observed non-magnetized. It was found that annealing conditions can control the magnetic and electrical properties as well as the microstructure of the films.