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Effect of Isothermal Transformation Heat-treatment Time on Cold Workability of STS 430 Stainless Steel after High Temperature Gas Nitriding

고온 가스질화 된 STS 430 스테인리스강의 냉간 가공성에 미치는 항온변태 열처리 시간 변화의 영향

  • Kim, J.M. (Korea Institute of Materials Science (KIMS)) ;
  • Hyun, Y.K. (Korea Institute of Materials Science (KIMS)) ;
  • Song, S.W. (Korea Institute of Materials Science (KIMS)) ;
  • Kim, G.D. (Korea Institute of Materials Science (KIMS)) ;
  • Son, Y.H. (Korea Institute of Materials Science (KIMS)) ;
  • Sung, J.H. (Center for Advanced Net Shape Manufacturing and Clean Process, Dong-A University)
  • 김정민 (한국기계연구원 부설 재료연구소) ;
  • 현양기 (한국기계연구원 부설 재료연구소) ;
  • 송상우 (한국기계연구원 부설 재료연구소) ;
  • 김기동 (한국기계연구원 부설 재료연구소) ;
  • 손영호 (한국기계연구원 부설 재료연구소) ;
  • 성장현 (동아대학교 신소형재가공청정공정개발 연구센터)
  • Received : 2013.11.07
  • Accepted : 2013.12.05
  • Published : 2014.01.30

Abstract

This study is to investigate the phase changes and cold workability after isothermal transformation at $780^{\circ}C$ by using the high temperature gas nitrided (HTGN) STS 430 ferritic stainless steel specimens. The phase diagram of STS 430 steel obtained by calculation showed that the phase appeared at $1100^{\circ}C$ showed as ${\alpha}+{\gamma}{\rightarrow}{\gamma}{\rightarrow}{\gamma}+Cr_2N{\rightarrow}{\gamma}+Cr_2N+CrN$ with increasing nitrogen concentration. Also, the transformation of ${\gamma}{\rightarrow}Cr_2N$ during heat treatment isothermally at $780^{\circ}C$, nitrogen pearlite with lamellar type was fully formed at the nitrogen permated surface layer for 10 hrs. However, this transformation was not completed for 1 hr, resulting nitrogen pearlite plus martensite. The cold rolled specimen of isothermally transformed at $780^{\circ}C$ for 10 hrs after high temperature gas nitriding decreased the layer thickness of nitrogen pearlite inducing the deformation of hard $Cr_2N$ phase. the dissolution rate of $Cr_2N$ phase increased rapidly with increasing cold rolling ratio. Specimens with the microstructure of nitrogen pearlite (isothermally transformed at $780^{\circ}C$ for 10 hrs) were possible to cold rolling without crack formation. However, the mixed structures of nitrogen pearlite + martensite (isothermally transformed at $780^{\circ}C$ for 1 hr) were impossible to cold deformation without cracking.

Keywords

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