• Title/Summary/Keyword: Internal pore

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Evaluation Method of Rock Characteristics using X-ray CT images (X-ray CT 이미지를 이용한 암석의 특성 평가 방안)

  • Kim, Kwang Yeom;Yun, Tae Sup
    • Tunnel and Underground Space
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    • v.29 no.6
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    • pp.542-557
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    • 2019
  • The behavior of rock mass is influenced by its microscopic feature of internal structure generating from forming and metamorphic process. This study investigated a new methodology for characterization of rock based on the X-ray CT (computed tomography) images reflecting the spatial distribution characteristics of internal constituent materials. The X-ray image based analysis is capable of quantification of heterogeneity and anisotropy of rock fabric, size distribution and shape parameter analysis of rock mineral grains, fluid flow simulation based on pore geometry image and roughness evaluation of unexposed joint surface which are hardly acquired by conventional rock testing methods.

Development of New Reverse Micellar Microencapsulation Technique to Load Water-Soluble Drug into PLGA Microspheres

  • Kim Hyun Joo;Cho Mi Hyun;Sah Hong Kee
    • Archives of Pharmacal Research
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    • v.28 no.3
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    • pp.370-375
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    • 2005
  • The objective of this study was to develop a new reverse micelle-based microencapsulation technique to load tetracycline hydrochloride into PLGA microspheres. To do so, a reverse micellar system was formulated to dissolve tetracycline hydrochloride and water in ethyl formate with the aid of cetyltrimethylammonium bromide. The resultant micellar solution was used to dissolve 0.3 to 0.75 g of PLGA, and microspheres were prepared following a modified solvent quenching technique. As a control experiment, the drug was encapsulated into PLGA microspheres via a conventional methylene chloride-based emulsion procedure. The micro­spheres were then characterized with regard to drug loading efficiency, their size distribution and morphology. The reverse micellar procedure led to the formation of free-flowing, spherical microspheres with the size mode of 88 ~m. When PLGA microspheres were prepared follow­ing the conventional methylene chloride-based procedure, most of tetracycline hydrochloride leached to the aqueous external phase: A maximal loading efficiency observed our experimental conditions was below $5\%$. Their surfaces had numerous pores, while their internal architecture was honey-combed. In sharp contrast, the new reverse micellar encapsulation technique permitted the attainment of a maximal loading efficiency of 63.19 $\pm$$0.64\%$. Also, the microspheres had smooth and pore-free surfaces, and hollow cavities were absent from their internal matrices. The results of this study demonstrated that PLGA microspheres could be successfully prepared following the new reverse micellar encapsulation technique.

A Study on the Dextran Formation and Inner Structure of Jeung-Pyun during the Fermentation by the Added Chitosan-Oligosaccharide (키토산 올리고당 첨가 증편 발효 중 Dextran 형성과 증편의 내부구조에 관한 연구)

  • 남태희;우경자
    • Journal of the East Asian Society of Dietary Life
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    • v.13 no.2
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    • pp.122-129
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    • 2003
  • This study was carried out in order to investigate the dextran formation and the internal structure of the chitosan-oligisaccharide(COS) Jeung-Pyun during the fermentation. To develop a functional Jeung-Pyun, COS was added to the rice at the level of 0, 2, 4, and 6% to the 2-hour-soaked rice. The pH, dextran and reducing sugar contents of COS batter, specific volume and the internal structure of COS were analyzed as a function of fermentation time. The specific volume of COS peaked at the 3 hour fermentation. The pH values of COS batters reduced with the fermentation time. The dextran content of the control batters peaked at the 7 hour fermentation. In contrast, the dextran contents of COS batters reduced up to 7th hour of fermentation, and then increased slowly until 20th hour of the fermentation process. From the air pore size and distribution of COS observed by SEM, the COS fermented fur 3 hour was judged as the best. It was concluded that COS prevented the fermation of dextran at the early stage of fermentation process.

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Cross-section micrography of burning pulverized coal particles (연소중 미분탄의 단면관측)

  • 한재현;최상민
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.13 no.4
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    • pp.717-725
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    • 1989
  • An experimental investigation on the combustion behavior of pulverized coal particles was performed using the cross-section micrography techniques while sample coal particles were collected in-situ from the flow reactor. The coal particles were representative of pulverized bituminous coal undergoing a raped pyrolysis and combustion, however, quenched at the time when the particles were deposited onto a sample plate. The internal structure of coal was observed to change as deposited. Upon injection into a flow reactor, bituminous coal particles showed many holes which represented internal pore formation during the pyrolysis. The relative portion of the remaining matrix of coal was decreasing as the residence time progressed. This direct observation of cross-section of burning particles enabled better understanding of the coal combustion behavior.

Stress Analysis for Differential Drying Shrinkage of Concrete (콘크리트의 부등건조수축으로 인한 응력의 해석)

  • 김진근;김효범
    • Magazine of the Korea Concrete Institute
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    • v.6 no.4
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    • pp.102-112
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    • 1994
  • The drying shrinkage of concrete has a close relation to the water movement. Since the diffusion process of water in concrete is strongly dependent on the temperature and the pore humidity, the process is highly nonlinear phenomena. This study consists of two parts. The first is the development of a finite element program which is capable of simulating the rnoisture distri- ,bution in concrete, and the other is the estimation of the differential drying shrinkage and stress considering creep by using the modified elastic modulus due to inner temperature change and maturity. It is shown that the analytical results of this study are in good agreement with experlimental data in the literatures, and results calculated by BP-KX model. The internal stress caused by moisture distribution which was resulted from the diffusion process, was calculated :quantitatively. The tensile stress which occured in the drying outer zone mostly exceeded the tensile strength of concrete, and necessarily would result in crack formation.

The Comparison of Methods Processing Cells Recovered by Bronchoalveloar Lavage (기관지폐포세척액에서 세포수 측정을 위한 처리방법의 비교)

  • Park, Jae-Seuk;Kim, Jae-Yeal;Lee, Gwi-Lae;Yoo, Chul-Gyu;Han, Sung-Koo;Shim, Young-Soo;Kim, Young-Whan
    • Tuberculosis and Respiratory Diseases
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    • v.45 no.1
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    • pp.176-183
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    • 1998
  • Background: The total and differential cell count of bronchoalveolar lavage(BAL) fluid are useful assessing activity, prognosis and response to therapy in diffuse interstitial lung disease. But controversy exist as to the appropriate method in processing BAL fluid. Therefore we investigated the effect of gauze filtration, centrifugation and different storage time of BAL fluid on the total and differential cell count. Methods: We obtained BAL fluid from 6 persons with no active lung lesion and divided pooled BAL fluid into several siliconized glass tubes and filtered through 0, 1, 2, 4 folds of cotton guaze(pore size: 1mm), and compared total cell count using hemocytometer after trypan blue staining and differential cell count after Wright-Giemsa staining of cytocentrifuged preparations. And we also counted total and differential cell count after centrifugation(400g for 30 min) and various storage time(2hr, 24hr, and 48hr). Results: There was no difference in total and differential cell count according to folds of gauze filtraion. But without gauze filtration, mucus threads that hampered total and differential cell count were found in 2 cases (33%). Centrifugation resulted in loss of total cell count($24{\pm}18%$) without change in differential cell count. There was no change in total cell count after 2hr storage but significant cell loss was found after 24hr storage time(24hr : $28{\pm}21%$, 48hr : $41{\pm}24%$). However there was no change in differential cell count with 48hr storage time. Conclusion: Total and differential cell count of BAL fluid may be best performed after cotton gauze filtration without centrifugation and within 2 hours.

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Geotechnical Characteristics of Crude Oil-Contaminated Sandy Ground (원유로 오염된 지반의 역학적 특성)

  • 신은철;이재범
    • Geotechnical Engineering
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    • v.13 no.6
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    • pp.37-44
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    • 1997
  • In this paper, the effects of crude oil contamination on the geotechnical properties of sand such as compaction characteristics, shear strength, permeability, and bearing capacity are presented. The test results indicate that the compaction characteristics are somewhat influenced by oil contamination. The angle of internal friction of sand based on total stress analysis decreases due to the presence of oil within the pore spaces in Band. The bearing capacity of sand is significantly influenced by oil contamination.

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Membrane contactor and Carbon Dioxide Separation

  • 이규호
    • Proceedings of the Membrane Society of Korea Conference
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    • 2002.07a
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    • pp.59-101
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    • 2002
  • PVDF is good material for a hollow fiber membrane with high porosity and excellent hydrophobicity. Asymmetric PVDF hollow fiber membranes were prepared by the Loeb-Sourirajan phase inversion method. Asymmetric PVDF hollow fiber membranes could be controlled in pore size and porosity using various additives(LiCl, ZnCl$_2$) and internal coagulants (water, EtOH/water, and DMAc/water mixture). $CO_2$removal efficiency of asymmetric PVDF hollow fiber membranes was 1.2 times high than that of commercialized PP hollow fiber membranes at MEA 5wt% solution. $CO_2$flux of asymmetric PVDF hollow fiber membranes was 2.5 times higher than that of commercialized PP hollow fiber membranes. $CO_2$removal efficiency and absorption rate of asymmetric PVDF hollow fiber membranes were 30 times higher than those of packed column at absorbent $H_2O$. $CO_2$flux of asymmetric PVDF hollow fiber membranes at MEA 5wt% solution was 48 times higher than that of pure water. In the case of MEA 5wt% solution used as an absorbent, the $CO_2$absorption rate and removal efficiency of PVDF hollow fiber membrane were 2.3 times higher than that of a packed column.

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Development of geopolymer with pyroclastic flow deposit called Shirasu

  • Katpady, Dhruva Narayana;Takewaka, Koji;Yamaguchi, Toshinobu
    • Advances in materials Research
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    • v.4 no.3
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    • pp.179-192
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    • 2015
  • The study presents a preliminary investigation on the applicability of Shirasu (a pyroclastic flow deposit characterized by high percentage of volcanic glass) in geopolymer. Comparative study on compressive strength and internal pore structure has been done between geopolymers with alkali activated Shirasu and fly ash as aluminosilicates. Mortar mix proportions are selected based on variations in ratio of alkaline activators to aluminosilicate and also on silica to alkali hydroxide ratio. From the experimental study, Shirasu geopolymer exhibited fairly good compressive strength. Mix proportion based on silica to alkali hydroxide ratio is observed to have profound effect on strength development.

GEOTECHNICAL CHARACTERISTICS OF CRUDE OIL-CONTAMINATED GROUND (원유(Crude-Oil)로 오염된 지반의 역학적 특성)

  • 신은철;홍승서;강욱현
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 1997.05a
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    • pp.43-46
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    • 1997
  • The results of an investigation conducted to study the effect of crude oil contamination on the geotechnical properties of sand of presented. The effect of the degree of oil contamination on compaction characteristics, shear strength, and one-dimensional compression characteristics has been investigated. The test results indicate that the compaction characteristics are somewhat influenced by oil contamination. The angle of internal friction of sand (based on total stress basis) decreases due to the presence of oil within the pore spaces in sand. The compression characteristics of sand are significantly-influenced by oil contamination. The details of the tests conducted and the results are presented in the paper.

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