• 한국분말재료학회지
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• 제25권3호
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• pp.251-256
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• 2018

We report the feasibility of TaC production via self-propagating high temperature synthesis, and the influence of the initial green compact density on the final composite particle size. Experiments are carried out from a minimum pressure of 0.3 MPa, the pressure at which the initial green body becomes self-standing, up to 3 MPa, the point at which no further combustion occurs. The green density of the pellets varies from 29.99% to 42.97%, as compared with the theoretical density. The increase in green density decreases the powder size of TaC, and the smallest particle size is observed with 1.5 MPa, at $10.36{\mu}m$. Phase analysis results confirm the presence of the TaC phase only. In the range of 0.3-0.5 MPa, traces of unreacted Ta and C residues are detected. However, results also show the presence of only C residue in the matrix within the pressure range of 0.6-3.0 MPa.

• 한국산업융합학회 논문집
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• 제21권6호
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• pp.273-284
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• 2018

3D printing technology in the construction field is currently being developed and commercialized actively in foreign countries, but the development of material and equipment is underway as an initial research stage in Korea. It is necessary to implement commercialization through the introduction of 3D printing technology in the construction field as soon as possible in Korea, but there is no guideline for suitable equipment and materials in Korea at present. Therefore, in order to help prepare for commercialization, it is necessary to provide data such as equipment size and materials suitable for commercialization at the initial stage. This study investigates the types, specifications, and applications of equipment that are being used overseas to provide the equipment type and material cost required in the initial stage of commercialization in Korea. Using the surveyed data, it was possible to calculate the advantages and disadvantages of the equipment type and specification, and the cost of materials used. As a result of the analysis, Gantry type is suitable for the domestic commercialization, and the standard of the output area is $100m^2$ and the extrusion amount of $250m^3/sec$ is proposed, and the material cost of the commercial product is 20thousand won. The suggestions in this study will help to plan the construction of products and equipments to commercialize 3D printing technology in construction field in the future.

• Structural Engineering and Mechanics
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• 제70권5호
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• pp.623-637
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• 2019

This paper analyzes the non-stationary vibration and super-harmonic resonances in nonlinear dynamic motion of viscoelastic nano-resonators. For this purpose, a new coupled size-dependent model is developed for a plate-shape nano-resonator made of nonlinear viscoelastic material based on modified coupled stress theory. The virtual work induced by viscous forces obtained in the framework of the Leaderman integral for the size-independent and size-dependent stress tensors. With incorporating the size-dependent potential energy, kinetic energy, and an external excitation force work based on Hamilton's principle, the viscous work equation is balanced. The resulting size-dependent viscoelastically coupled equations are solved using the expansion theory, Galerkin method and the fourth-order Runge-Kutta technique. The Hilbert-Huang transform is performed to examine the effects of the viscoelastic parameter and initial excitation values on the nanosystem free vibration. Furthermore, the secondary resonance due to the super-harmonic motions are examined in the form of frequency response, force response, Poincare map, phase portrait and fast Fourier transforms. The results show that the vibration of viscoelastic nanosystem is non-stationary at higher excitation values unlike the elastic ones. In addition, ignoring the small-size effects shifts the secondary resonance, significantly.

• 한국광물학회지
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• 제9권2호
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• pp.71-81
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• 1996

Dissolution experiments were conducted to understand chemical nature of weathering of anorthosite from the Hadong area. Anorthosite and plagioclase from it were reacted with HCl or KOH solutions under various conditions concerning such as grain size, initial pH of solutions, and shaking Average composition of plagioclase used in the experiment was Na0.32Ca0.71Al1.71Si2.28O8.Under acidic conditions, solution pH increases rapidly in the initial stage and then gradually to reach palteau. Shaking agitates the reaction rate in the initial stage but does not affect after the system reached steady state. Ca and si concentrations show rapid increase and then gradual increase. Al concentration increases rapidly in the early stage and then decreases. Later decrease was interpreted as the precipitation of an Al-bearing material. Different dissolution rates of different constituents of plagioclase together the with precipitation of al-bearing material might be responsible for the non-stoichiometric dissolution of plagioclase.X-ray diffraction analyses on anorthosite before and after dissolution experiment show dissolution rates differ with different lattice planes of plagioclase. It suggests the crystallographic control on dissolution reaction. X-ray photoelectron spectroscopic result shows that the average composition of plagioclase surface reacted with HCL of initial pH 1.97 for 2000 hours is Na0.20Ca0.26Al1.7Si2.3O8. It means that Na- and Ca-depleted H-feldspar is developed without Al-depleted layer on the surface of plagioclase by reaction with HCl and that dissolution reaction takes place sparsely on the surface of plagioclase. Al and Si are dissolved preferentially over Ca from anorthosite powder in KHO solution. Reaction of acid-reacted anorthosite with KOH solution shows the same Si dissolution behavior as in the fresh anorthosite. This indicates that the Al-depleted and Si-enriched layer does not build up on the acid-reacted surface.

• 대한기계학회논문집B
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• 제34권12호
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• pp.1051-1060
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• 2010

고화 입자 크기의 관점에서 TROI 용융물-냉각수 반응 실험의 결과에 대한 물질 효과를 분석하였다. 고화 입자 크기를 분석하면 용융물-냉각수 반응에서 초기 조건, 혼합, 폭발을 기적으로 해석할 수 있다. 증기 폭발이 발생한 경우와 폭발이 발생하지 않는 경우의 고화 입자 크기를 분석한 결과 증기 폭발이 발생한 경우에는 미세 입자가 많고 비교적 큰 입자는 적은 것으로 나타났다. 또한, 혼합 과정에 대한 정보를 보존할 수 있는 증기 폭발이 발생하지 않은 용융물-냉각수 반응을 이용하여 용융물 입자 크기에 대한 물질 효과를 분석하였다. 증기 폭발이 잘 발생하는 용융물은 증기 폭발에 참여할 수 있는 큰 입자를 많이 포함하고 있었고, 증기 폭발이 잘 발생하지 않는 용융물은 증기 폭발보다는 냉각되기 쉬운 작은 입자 혹은 미세 입자를 많이 포함하고 있었다.

• 한국재료학회지
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• 제22권6호
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• pp.303-308
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• 2012

This study evaluated the enhancement of microstructural and mechanical properties of a cross rolled Ni-10Cr alloy, comparing with conventionally rolled material. Cold rolling was carried out to 90% thickness reduction and the specimens were subsequently annealed at $700^{\circ}C$ for 30 min to obtain a fully recrystallized microstructure. Cross roll rolling was carried out at a tilted roll mill condition of $5^{\circ}$ from the transverse direction in the RD-TD plane. In order to observe the deformed microstructures of the cold rolled materials, transmission electron microscopy was employed. For annealed materials after rolling, in order to investigate the grain boundary characteristic distributions, an electron back-scattering diffraction technique was applied. Application of cold rolling to the Ni-10Cr alloy contributed to notable grain refinement, and consequently the average grain size was refined from 135 ${\mu}m$ in the initial material to 9.4 and 4.2 ${\mu}m$ in conventionally rolled and cross rolled materials, respectively, thus showing more significantly refined grains in the cross rolled material. This refined grain size led to enhanced mechanical properties such as yield and tensile strengths, with slightly higher values in the cross rolled material. Furthermore, the <111>//ND texture in the CRR material was better developed compared to that of the CR material, which contributed to enhanced mechanical properties and formability.

• 대한금속재료학회지
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• 제49권8호
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• pp.649-656
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• 2011

The present study evaluated the microstructures and mechanical properties of severely deformed Ni-30Cr alloys. Cross-roll rolling (CRR) process was introduced as a severe plastic deformation (SPD), and Ni-30Cr alloy sheets were cold rolled to 90% thickness reduction and subsequently annealed at $700^{\circ}C$ for 30 min to obtain the recrystallized microstructure. Electron back-scattering diffraction (EBSD) was introduced to analyze grain boundary character distributions (GBCDs). The application of CRR to the Ni-30Cr alloy was effective in enhancing the grain refinement through heat treatment; consequently, the average grain size was significantly refined from $33{\mu}m$ in the initial material to $0.6{\mu}m$. This grain refinement directly improved the mechanical properties, in which yield and tensile strengths significantly increased relative to those of the initial material. We systematically discuss the grain refinement and accompanying improvement of the mechanical properties, in terms of the effective strain imposed by CRR relative to conventional rolling (CR).

• 한국진공학회지
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• 제4권S1호
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• pp.113-117
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• 1995

MOCVD of Cu films were carried out on gold-TiN(1000$\AA$)/Ti/Si wafers from hexafluoroacetylacetonate-Cu(l) vinyltrimethylsilane, Cu(l)(hafac)(vtms), in a small cold-wall type reactor. Effects of the substrate and bubbler temperatures on the film growth rate were studied, and a film with $\rho$=1.8$\pm$0.1$\mu$$\Omega$.cm could be deposited 150nm/min at Ts=200 and Tb=$30^{\circ}C$, respectively. The initial stage of the film formation was also investigated by in-situ laser reflectivity monitoring combined with SEM observations, based on which variations in the film properties depending on the growth conditions were discussed in terms of the nucleation rate and grain size.

• 한국소성가공학회:학술대회논문집
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• 한국소성가공학회 1994년도 추계학술대회 논문집
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• pp.141-148
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• 1994

In order to improve the productivity of cold forging at low production cost, an integrated system's approach is necessary in handling the material preparation and the optimum process design, considering the forming machines, tooling, and operation including quality control. As the first step toward this approach, an expert system for multi-stage cold forging process design for fasteners with various head geometries is developed using Prolog language on IBM 486 PC. For effective representation of the complex part geometries, the system uses the multiple element input, and the forward inference scheme in determination of the initial billet size and intermediate forging steps. In order to determine intermediate steps, the basic empirical rules for extrusion, heading, and trimming were applied. The required forming loads and global strain distributions at each forging step were calculated and displayed on the PC monitor. The designed process sequence drawing can be obtained by AutoCAD. The developed system will be useful in reducing trial and error of design engineers in determining the diameter and height of the initial cylindrical billet from the final product geometry and the intermediate necessary sequences.

• 한국안전학회지
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• 제29권3호
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• pp.136-142
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• 2014

Recently a new version of PRO-LOCA program was released. Using the program, failure probability of pipes can be evaluated considering fatigue and/or stress corrosion crack growth and the effects of various parameters on the integrity of pipes in nuclear power plants can be evaluated quantitatively. The analysis results can be used to establish an inspection plan and to examine the effects of important parameters in a maintenance plan. In this study, sensitivity analyses were performed using the program for several important parameters including sampling method, initial crack size, number of initial fabrication flaws, operation temperature, inspection interval, operation temperature and nominal applied bending stress. The effect of parameters on the leak and rupture probability of pipes was evaluated due to fatigue or stress corrosion crack growth.