• Transactions of the Korean Society of Mechanical Engineers A
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• v.32 no.1
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• pp.35-42
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• 2008

Instrumented sharp indentation test is a well-directed method to measure hardness and elastic modulus. The sharp indenter such as Berkovich and conical indenters have a geometrical self-similarity in theory, but the self-similarity ceases to work in practice due to inevitable indenter tip-blunting. In this study we analyzed the load-depth curves of conical indenter with finite tip-radius via finite element method. Using the numerical regression data obtained from Kick's law, we first confirmed that loading curvature is significantly affected by tip radius as well as material properties. We then established a new method to evaluate Young's modulus, which successfully provides the value of elastic modulus with an average error of less than 2%, regardless of tip-radius and material properties of both indenter and specimen.

• Journal of the Korean Ceramic Society
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• v.44 no.7
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• pp.368-374
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• 2007

CVD-SiC coating has been introduced as a protective layer in TRISO nuclear fuel particle of high temperature gas cooled reactor (HTGR) due to its excellent mechanical stability at high temperature. In order to prevent the failure of the TRISO particles, it is important to evaluate the fracture strength of the SiC coating layer. It is needed to develop a new simple characterization technique to evaluate the mechanical properties of the coating layer as a pre-irradiation step. In present work, direct strength measurement method with the specimen of hem i-spherical shell configuration was suggested. The indentation experiment on a hemisphere shell with a plate indenter was conducted. The fracture strength of the coating layer is related with the critical load for radial cracking of the shell. The finite element analysis was used to drive the semi-empirical equation for the strength measurement. The SiC hemispherical shells were successfully recovered from the section-grinding of TRISO coated particle and successive heat treatment in air. The strength of CVD-SiC coating layer was evaluated from the experimentally measured critical load during the indentation on SiC hemisphere shell. Weibull diagram of fracture strength was also constructed. This study suggested a new strength equation and experimental method to measure the fracture strength of CVD-SiC coating of TRISO coated fuel particles.

• Journal of the Korea Academia-Industrial cooperation Society
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• v.15 no.10
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• pp.5974-5979
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• 2014

Lightweight parts with very uniform precision are manufactured by an indent method and the press technique has been improved. Upon assembly with an indent method, a deformation force due to the compressive force occurs between the pin and hole and the contact surface is affected by damage. Therefore, a 3 dimensional model was made using the CATIA program and the damage on the surface contacted with indent was estimated through the ANSYS program in this study. In the analysis result, the maximum load applied at the PCB plate was 21.3 N when the pin goes through the PCB plate. When PCB plate came out of the pin, the maximum load was 19.24 N. As the structural analysis result, the maximum equivalent stress of Pin 1 was 192.96MPa because the maximum stress occurs at Pin 1 among all parts of this study model. By examining the damage property of the contacted indent and applying this study result to the design of real indentation, the damage can be prevented and the durability can be estimated.

• Structural Engineering and Mechanics
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• v.7 no.6
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• pp.575-588
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• 1999

A boundary element method is applied to the analysis of crack trajectory in materials with complex microstructure, such as discontinuously reinforced composite materials, and systems subjected to complex loading, such as indentation. The path followed by the crack(s) has non-trivial geometry. A study of the stress intensity factors and fracture toughness of such systems must therefore be accompanied by an analysis of crack trajectory. The simulation is achieved using a dual boundary integral method in planar problems, and a single boundary integral method coupled with substructuring in axisymmetric problems. The direction of crack propagation is determined using the maximum mechanical energy release rate criterion. The method is demonstrated by application to (i) a composite material composed of components having the elastic properties of aluminium (matrix) and silicon carbide (reinforcement), and (ii) analysis of contact damage induced by the action of an indenter on brittle materials. The chief advantage of the method is the ease with which problems having complex geometry or loading (giving rise to complex crack trajectories) can be treated.

• Journal of the Korean Ceramic Society
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• v.24 no.4
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• pp.357-363
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• 1987

This study consists of two powder preparation process. One is that the synthesized Forsterite at 1400$^{\circ}C$ mixed with Zirconia powder. Another, theoretical Forsterite composition mixed with Zirconia. These two Forsterite bodies were heat-treated at 1400$^{\circ}C$, 1450$^{\circ}C$. Synthesized Foresterite composition showed higher density, strength than Forsterite composite which was directly mixed with Zirconia KIC value was measured by Microhardness Indentation method. It shows the highest value when 15 weight percent Zirconia dispersed.

• Journal of the Korean institute of surface engineering
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• v.30 no.5
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• pp.347-354
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• 1997

Composite plating is a method of co-depositing fine particles of metallic, non-metallic compound or polymers in the plated layer to improve material properties such as were-resistance, lubrication, or corrosion resistance. Graded Ni-Sic composite coating were produced in this research. Prior to produce Graded Ni-SiC composite coatings, effects of particle size, particle content, pH of electrolyte, temperature, current density, stirring rate on the amount of SiC deposited in the Ni layer were investigated. By manipulating current density and plating time properties of these coating were evaluated by micro-indentation hardness test.

• Proceedings of the Materials Research Society of Korea Conference
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• 2008.05a
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• pp.42.2-42.2
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• 2008

• Journal of the Korean institute of surface engineering
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• v.53 no.1
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• pp.36-42
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• 2020

In this study, two novel methods to measure the surface hardness of anodic oxide films on aluminum alloys are reported. The first method is to impregnate oil-based ink into pores in the anodic oxide film and then to clean the ink on the surface using ethanol, resulting in an impregnation of inks only inside of the pores in anodic oxide film. The second method is to coat the anodic oxide film surface with thin Au layer less than 0.1 ?. Both the ink-impregnating method and Au-coating method provided clear indentation marks on the anodic oxide film surface when it was indented using a pyramidal-diamond penetrator. Thus, Vickers hardness of anodic oxide films on aluminium alloy could be measured successfully and precisely from the anodic film surface. In addition, advantages and disadvantages of the ink-impregnating method and Au-coating method for the measurement of surface hardness of anodic oxide films are discussed.

• Journal of the Korean Ceramic Society
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• v.29 no.8
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• pp.651-659
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• 1992

Fracture toughness of alumina was determined by IF, IS, DT, SEPB methods, and the data were inter-compared. Round robin test on IF and IS methods was also conducted under the participitation of 4∼5 domestic institutes. Fracture toughness data determined by IF, IS, DT methods were similar, while those by SEPB method were smaller. Variation of toughness data determined by IS method using 98N of indentation load was significantly small compared to those determined by any other methods. Round robin test results showed that toughness data determined by IF method at various institutes do not coincide each other, while those by IS method do well coincide. Thus, it was concluded that inter-confidence on fracture toughness data, if determined by IS method at all institute, can be established between institutes.

• Journal of the Microelectronics and Packaging Society
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• v.27 no.3
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• pp.83-88
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• 2020

The evolution of smartphones has led to numerous researches in the mechanical behavior of flexible devices. Due to the nano-size of the thin flexible film, nanoindentation is widely used to evaluate its mechanical behaviors, such as elastic modulus, and hardness. However, the commonly used Oliver-Pharr method is not suited for analyzing the indentation force-depth curves of hard films on soft substrates, as the effects of soft substrate is not considered theoretically. In this study, the elastic modulus of the thin film was evaluated with references to other reported models which include the substrate effect, and with calibration of the indentation depth for the pile-ups between the indenter and test surface. We fabricated test samples by deposition of amorphous metal film on polyimide and silicon wafers for verification of modified models.