• 한국전기전자재료학회논문지
• /
• 제22권3호
• /
• pp.235-238
• /
• 2009

This paper describes the mechanical properties of poly (Polycrystalline) 3C-SiC thin films with $N_2$ in-situ doping. In this work, the poly 3C-SiC film was deposited by APCVD (Atmospheric Pressure Chemical Vapor Deposition) method using single-precursor HMDS (Hexamethyildisilane: $Si_2(CH_3)_6)$ at $1200^{\circ}C$. The mechanical properties of doped poly 3C-SiC thin films were measured by nono-indentation according to the various $N_2$ flow rate. In the case of 0 sccm $N_2$ flow rate, Young's Modulus and hardness were obtained as 285 GPa and 35 GPa, respectively. Young's Modulus and hardness were decreased according to increase of $N_2$ flow rate. The crystallinity and surface roughness was also measured by XRD (X-Ray Diffraction) and AFM (Atomic Force Microscopy), respectively.

• 소성∙가공
• /
• 제6권6호
• /
• pp.508-516
• /
• 1997

Forging process on sintered powder metals has been applied to produce automotive parts which require a high level of strength. In those parts, the measurement of relative density is very important because a low relative density density causes deterioration of strength. In the present study, an indentation force equation was proposed by which the result obtained from the hardness measurement is used to evaluate the relative density. This equation was applied to the prediction of the relative density in cylindrical specimens which were first sintered and then forged at the room temperature and at an elevated temperature. The experimental results were compared with predictions with and without consideration of the workhardening effect on the powder.

• 한국세라믹학회지
• /
• 제43권5호
• /
• pp.320-326
• /
• 2006

Mullite whiskers were synthesized by a vapor-solid reaction with $Al(OH)_3-SiO_2-AlF_3$. The heat treatment temperature did not affect the shape of mullite whisker but the composition change resulted in different sizes. The first one was $30-50{\mu}m$ in size with the aspect ratio of 60 and above, and the second one was $600{\mu}m$ and below in size with the aspect ratio of 15 and below. The $Al_2O_3$ content in formed mullite whisker was 73.57-80.29 wt%, which is high $Al_2O_3$ content composition. The Young's modulus and the hardness measured by nano-indentation method were 136.7 GPa and 19.81 GPa, respectively.

• 자동차안전학회지
• /
• 제7권3호
• /
• pp.19-24
• /
• 2015

Brake pads are a component of disc brake system of automobile and consist of steel backing plates and friction material facing the disk brake rotor. Due to the repeated sliding forces and torque in vehicle braking, friction performance of brake pads are ensured. Futhermore, the brake pad is one of major tuning components in aftermarket, mechanical characteristics of the brake pad are necessary to evaluate for establishing the certification standards of tuning components. This study had performed the five specimen tests for friction coefficients and wear loss rates according to the SAE test specification. Using the instrumented indentation method, yield strength and tensile strength were measured. Friction coefficients, 0.386 - 0.489, and wear loss rates, 1.0% - 3.7% are obtained. The range of yield strength and tensile strength are 21.4 MPa - 105.3 MPa and 39.5 MPa - 176.4 MPa respectively.

• 한국정밀공학회지
• /
• 제21권3호
• /
• pp.139-146
• /
• 2004

In this study, to achieve the optimal conditions for mechanical hyper-fine pattern fabrication process, deformation behavior of the materials during indentation scratch test was studied with numerical method by ABAQUS S/W. Brittle materials (Si, Pyrex glass 7740) were used as specimens, and forming conditions to reduce the elastic recovery and pile-up were proposed. The indenter was modeled as a rigid surface. Minimum mesh sizes of specimens are 1-l0nm. Variables of the nanoindentation scratch test analysis are scratching speed, scratching load, tip radius and tip geometry. The nano-indentation scratch tests were performed by using the Berkovich pyramidal diamond indenter. Comparison between the experimental data and numerical result demonstrated that the FEM approach can be a good model of the nanoindentation scratch test. The result of the investigation will be applied to the fabrication of the hyper-fine pattern.

• 한국가스학회:학술대회논문집
• /
• 한국가스학회 2002년도 춘계학술발표회 논문집
• /
• pp.78-85
• /
• 2002

• Journal of Welding and Joining
• /
• 제20권2호
• /
• pp.42-49
• /
• 2002

• 한국재료학회지
• /
• 제10권8호
• /
• pp.575-580
• /
• 2000

Ta(TaC) 필라멘트를 이용한 HF-CVD 법에 의하여 $Si_3N_4$, SiC, WC, $Al_2O_3$를 기판으로 다이아몬드 박막을 증착하고, 그 밀착특성을 평가하였다. 로내의 $CH_4$농도를 10%로 높게 하였을 경우에는 막중에 graphitic(amorphous) carbon이 생성됨을 확인할 수 있었다. 박막을 $12\mu\textrm{m}$ 정도까지 두껍게 하면, WC기판에서는 부분적 박리형상이 관찰되었으나, $Si_3N_4$를 기판으로 하였을 경우에는 안정한 박막을 얻을 수 있었다. Indentation test 결과로부터 grainding에 의한 기판표 처리가 밀착성 향상에 효과적이라는 것을 알 수 있었다. 또 compression topple test에서는 박막의 두께는 밀착성과 반비례의 관계를 가지는 것을 알 수 있었다. 수 있었다.

• 한국재료학회지
• /
• 제10권10호
• /
• pp.677-683
• /
• 2000

3Y-TZP/12Ce-TZP 의 3층 5층 복합체를 슬립주입법으로 제조하고, 그 기계적 성질을 검토하였다. 지름-원반압축시험법으로 구한 다층복합체의 파괴강도는 327~534MPa이었다. Vickers압입하중의 증가(~300N)와 더불어 압입강도는 전반적으로 감소하였으나, 다층물질은 단상물질에 비하여 우수한 손상저항을 나타내었다. 49N의 하중으로 압입후 다층물질의 4점 꺽임강도는 620~674MPa 인데 반하여 단상 물질의 경우는 129~339MPa을 나타내었다. 압자압입에 의한 다층물질의 인서은 $7.7~13.1\;MPa{\cdot}m^{1/2}$ 정도를 나타내었다.

• 한국결정성장학회지
• /
• 제15권1호
• /
• pp.39-44
• /
• 2005

적점토 60 wt%, 석탄회 20 wt%, 석분오니 20 wt%를 혼합하여 제작한 sheet 형태의 소지에 인덴트(indent)를 주고 건조방법, 파쇄방법, 성형방법을 변화시켜 1～5 mm 골재의 파쇄율을 알아보았다. 소지를 건조할 때 실내와 실외에서의 자연건조, 건조기건조, 마이크로웨이브(microwave)건조, 급속건조로 분류하여 비교실험 하였고, 파쇄방법은 볼밀 Ⅰ 파쇄, 볼밀 Ⅱ 파쇄, 낙하파쇄, 기계식 파쇄(롤러밀사용)법으로 변화를 주었다. 성형방법은 인덴트의 간격과 깊이를 변화시키면서 동시에 소지의 두께를 변화시켜 실험하였다. 건조방법에 의한 비교실험 결과는 210초까지 건조시킨 마이크로웨이브건조가 약 42%로. 파쇄방법에서는 볼밀 Ⅱ 파쇄법이 약 65 %로 가장 높은 파쇄율을 보였고, 성형방법에서는 인덴트의 깊이가 깊어질수록(3mm의 소지에서만), 소지의 두께가 증가할수록 크기가 Ф=5 mm보다 큰 골재의 수율은 감소했고 Ф=5 mm 이하인 골재의 수율은 증가했다. 각각의 실험 후 파쇄 된 1～5mm 골재의 aspect ratio를 비교해본 결과 3mm 두께의 소지를 급속건조법에 의해 건조하고 볼밀 Ⅱ법을 이용해 파쇄 한 경우 가장 균일한 골재의 모양으로 파쇄 되었음을 알 수 있었다.