• Fashion & Textile Research Journal
• /
• v.22 no.3
• /
• pp.386-398
• /
• 2020

This study compared dip-coating and in situ polymerization methods for the development of nanofiber-based E-textile using polypyrrole. Nanofiber webs were fabricated by electrospinning an aqueous poly (vinyl alcohol) (PVA) solution. Subsequently, the PVA nanofiber web underwent thermal treatment to improve water resistance. Dip-coating and in situ polymerization methods were used to deposit polypyrrole on the surfaces of the nanofiber web. An FE-SEM analysis was also conducted to examine specimen surface characteristics along with EDS and FT-IR that analyzed the chemical bonding between polypyrrole and specimens. The line resistance and sheet resistance of the treated specimens were measured. Finally, an electrocardiogram (ECG) was measured with textile sensors made of the polypyrrole-deposited PVA nanofiber webs. The polypyrrole-deposited PVA nanofiber webs fabricated by dip-coating dissolved in the dip-coating solution and indicated damage to the nanofibers. However, in the case of in situ polymerization, polypyrrole nanoparticles were deposited on the surface and inter-web structure of the PVA nanofiber web. The resistance measurements indicated that polypyrrole-deposited PVA nanofiber webs fabricated by in situ polymerization with an average sheet resistance of 5.3 k(Ω/□). Polypyrrole-deposited PVA nanofiber webs fabricated by dip-coating showed an average sheet resistance of 57.3 k(Ω/□). Polypyrrole-deposited PVA nanofibers fabricated by in situ polymerization showed a lower line and sheet resistance; in addition, they detected the electrical activity of the heart during ECG measurements. The electrodes made from polypyrrole-deposited PVA nanofiber webs by in situ polymerization showed the best performance for sensing ECG signals among the evaluated specimens.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2008.11a
• /
• pp.264-265
• /
• 2008

While the reliability of bulk insulation has become important particularly in multilayer boards and embedded boards, electronics are to be used under various environments such as at high temperature and in high humidity. We observed internal space charge behavior for two types of epoxy composites under dc electric fields to investigate the influence of water at high temperature. In the case of glass/epoxy specimen, homocharge is observed at water-treated specimen, and spatial oscillations become clearer in the water-treated specimens. Electric field in the vicinity of the electrodes shows the injection of homocharge. In aramid/epoxy specimens, heterocharge is observed at water-treated specimens, i.e. negative charge accumulates near the anode, while positive charge accumulates near the cathode. Electric field is enhanced just before each electrode. In order to further examine the mechanism of space charge formation, we have developed a new system that allows in situ space charge observation during ion migration tests at high temperature and high humidity. Using this in situ system.

• Coupled systems mechanics
• /
• v.12 no.6
• /
• pp.503-517
• /
• 2023

Standard Digital Volume Correlation (DVC) approaches are based on pattern matching between two reconstructed volumes acquired at different stages. Such frameworks are limited by the number of scans (due to acquisition duration), and time-dependent phenomena can generally not be captured. Projection-based Digital Volume Correlation (P-DVC) measures displacement fields from series of 2D radiographs acquired at different angles and loadings, thus resulting in richer temporal sampling (compared to standard DVC). The sought displacement field is decomposed over a basis of separated variables, namely, temporal and spatial modes. This study utilizes an alternative route in which spatial modes are con-structed via scan-wise DVC, and thus only the temporal amplitudes are sought via P-DVC. This meth-od is applied to a glass fiber mat reinforced polymer specimen containing a machined notch, subjected to in-situ cyclic tension, and imaged via X-Ray Computed Tomography. Different temporal interpolations are exploited. It is shown that utilizing only one DVC displacement field (as spatial mode) was sufficient to properly capture the complex kinematics up to specimen failure.

• Journal of the Korean Geotechnical Society
• /
• v.23 no.11
• /
• pp.49-58
• /
• 2007

Numerical experiments using a distinct element code (PFC3D) were carried out for the analysis of grout-material transfer in soil layers and also for the analysis of increase in mechanical strength after permeation grouting. For rapid analysis, up-scaling analysis in length scale was adopted, and the following observations were made from the numerical experiments. Firstly, the relative size of grout material with respect to the in situ soil particles controlled the transfer distance of the grout particles. When the size of grout particle was 0.2 to 0.25 times of the in situ soil particles, clogging of pore spaces among the in situ soil particles occurred, resulting in restricted propagation of grout particles. It was also found that there was a threshold value in the size of grout particle. Below the threshold value, the transfer distance of the grout particle did not increase with the decrease of particle size of the grout material. Secondly, the increase in cohesion and internal friction angle was observed in the numerical specimen with grouting treatment, but not with the untreated specimen.

• Restorative Dentistry and Endodontics
• /
• v.39 no.3
• /
• pp.164-171
• /
• 2014

Objectives: Designing in situ models for caries research is a demanding procedure, as both clinical and laboratory parameters need to be incorporated in a single study. This study aimed to construct an informative guideline for planning in situ models relevant to preexisting caries studies. Materials and Methods: An electronic literature search of the PubMed database was performed. A total 191 of full articles written in English were included and data were extracted from materials and methods. Multiple variables were analyzed in relation to the publication types, participant characteristics, specimen and appliance factors, and other conditions. Frequencies and percentages were displayed to summarize the data and the Pearson's chi-square test was used to assess a statistical significance (p < 0.05). Results: There were many parameters commonly included in the majority of in situ models such as inclusion criteria, sample sizes, sample allocation methods, tooth types, intraoral appliance types, sterilization methods, study periods, outcome measures, experimental interventions, etc. Interrelationships existed between the main research topics and some parameters (outcome measures and sample allocation methods) among the evaluated articles. Conclusions: It will be possible to establish standardized in situ protocols according to the research topics. Furthermore, data collaboration from comparable studies would be enhanced by homogeneous study designs.

• Tunnel and Underground Space
• /
• v.21 no.3
• /
• pp.181-191
• /
• 2011

It is very difficult to prepare a lab. test specimen from weak rock masses affected by faults, highly fractured zone or weathered zone. In conventional method of in situ direct shear test a rock block is sheared inside galleries, where reactions for the hydraulic jacks are available. A new in situ direct shear test apparatus has been developed in this study to perform the test inside galleries as well as open pit conditions. The apparatus is composed of normal and shear reaction plates including load transfer plates, hydraulic cylinder systems, load cells, multistage shear boxes with fixing devices, and needle rollers. Maximum size of the test block is $400{\times}400{\times}460$ mm, and procedures of the test block preparation has been suggested. To explore the field applicability of in situ direct shear test apparatus, proper test block site was investigated by extensive geological field survey. In situ direct shear test has been successful in producing most of information related to strength and deformability of the weak rock.

• Geotechnical Engineering
• /
• v.12 no.5
• /
• pp.63-78
• /
• 1996

Various type of in-situ and laboratary tests were performed in order to evaluate the stiffness of sedimentary soft rock. In triaxial compression tests of sedimentary soft rocks, axial strains from the axial displacement of the loading piston or specimen cap conventionally were considerably larger than those measured. tocally on the lateral surfaces of specimen, due to the bedding errors at the top and bottom ends of a specimen. A local deformation transducer was used to measure axial strains free from the bedding error ranging from 0.001% to about 1%. In ultra-sonic wave tests, the elastic modulus of unconfined spec imens was smaller than that of confined specimens, due probably to microfracks. Young's modulus Ed from ultra-sonic wave tests and those at small local strains from triaxial tests were similar, both of which agreed very well with Young's modulus Er from field shear wave velocities. Young'a modulus from the field behaviour was virtually similar to that obtained by reducing Er based on the strain level-dependency of stiffness evaluated by the triaxial tests.

• Journal of the Korean Geotechnical Society
• /
• v.24 no.7
• /
• pp.75-80
• /
• 2008

When a saturated clay is sampled in an undisturbed manner from a bore hole, the sample extends vertically and shrinks horizontally under undrained conditions due to stress release. The conventional consolidation test specimen is trimmed from the expanded sample so that its diameter is equal to the inner diameter of the consolidation test ring, and this test procedure does not reproduce the actual consolidation behavior. The measurement of sample extension was conducted by means of overcoring method showed that the extension strains were 1 to 2%. To simulate the in-situ consolidation behavior, we proposed the consolidation test method that uses a specimen with a slightly smaller diameter than the inside diameter of consolidometer so that the specimen expands laterally to the inside of the ring.

• Journal of the Korean Society for Aeronautical & Space Sciences
• /
• v.31 no.2
• /
• pp.57-62
• /
• 2003

Nano-bending method is presented to measure the Poisson's ratio of thinfilms for MEMS (Micro-Electro-Mechanical Systems) applicaiton. The douvle-ring specimen is designed and fabricated based on the surface micromachining process to facilitate the measurement of the Poisson's ratio. The Poisson's ratio can be obtained through analyzing the linear load-displacement relationship of the double ring specimen subjected to nano-indenter loading. The Present nano-bending mehod is an in-situ measurement approach due to the compatibility to the surface micromachining process. The Poisson's ratio is locally obtained at the location of the double ring specimen with micro dimension. To validate the nano-bending method, the Poisson's ratio of LPCVD (Low Pressure Chemical Vapor Deposition) poly-silicon with thickness of 2.3㎛ is investigated. Experimental results reveal that the Poisson's ratio of the poly-silicon film is 0.2569. The standard deviation of the nano-bending measurement for the stiffness of double ring specimens is 2.66%.

• Mass Spectrometry Letters
• /
• v.14 no.3
• /
• pp.57-78
• /
• 2023

Understanding the chemical composition of the brain helps researchers comprehend various neurological processes effectively. Understanding of the fundamental pathological processes that underpin many neurodegenerative disorders has recently advanced thanks to the advent of innovative bioanalytical techniques that allow high sensitivity and specificity with chemical imaging at high resolution in tissues and cells. Mass spectrometry imaging [MSI] has become more common in biomedical research to map the spatial distribution of biomolecules in situ. The technique enables complete and untargeted delineation of the in-situ distribution characteristics of proteins, metabolites, lipids, and peptides. MSI's superior molecular specificity gives it a significant edge over traditional histochemical methods. Recent years have seen a significant increase in MSI, which is capable of simultaneously mapping the distribution of thousands of biomolecules in the tissue specimen at a high resolution and is otherwise beyond the scope of other molecular imaging techniques. This review aims to acquaint the reader with the MSI experimental workflow, significant recent advancements, and implementations of MSI techniques in visualizing the anatomical distribution of neurochemicals in the human brain in relation to various neurogenerative diseases.