• Title/Summary/Keyword: In Situ Composite

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The Effect of Cold Working and Heat Treatment on the Magnetic Properties of in-situ Formed Cu-Fe Composites (In-situ 법(法)에 의한 Cu-Fe 복합조직(複合組織)의 자기적(磁氣的) 특성(特性)에 미치는 가공(加工) 및 열처리(熱處理)의 영향(影響))

  • Shur, S.J.;Park, H.S.
    • Journal of the Korean Society for Heat Treatment
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    • v.2 no.2
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    • pp.38-45
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    • 1989
  • The Cu-Fe permanent magnet were prepared in situ process, which has economic and mass productive merits in producing multi filamentary composites. The purpose of this research was to study the effect of reduction ratio and heat treatment on magnetic property. As the reduction ratio of Cu-Fe wire increased, the filament structure became finer and interfilament distances decreased and the morphology of filament cross section became ribbon shape. As Fe content increased significantly. The coercivity and squareness of Cu-55 wt%Fe composite increased as a reduction ratio became higher, whereas they increased to maximum values at 0.09 mm ${\phi}$ for Cu-30 wt%Fe, and 0.066 mm ${\phi}$ for CU-45 wt%Fe respectively, and decreased for further reduction. The magnetic properties of Cu-Fe composites can be more enhanced by intermediate heat treatment. The best magnetic properties were obtained from Cu-55 wt%Fe composite deformed to 0.054 mm ${\phi}$ and annealed.

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Enhanced Low-field Magnetoresistance of La0.7Sr0.3Mn1+dO3-Mn3O4 Composite Films Prepared by ex-situ Solid Phase Crystallization

  • Kang, Young-Min;Kim, Hyo-Jin;Yoo, Sang-Im
    • Journal of Magnetics
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    • v.17 no.4
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    • pp.265-270
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    • 2012
  • We report improved low-field magnetoresistance (LFMR) effects of the $La_{0.7}Sr_{0.3}Mn_{1+d}O_3-Mn_3O_4$ composite films with the nominal composition of $La_{0.7}Sr_{0.3}MnO_3$(LSMO)-50 mol% $Mn_3O_4$. The composite films were fabricated by ex-situ solid phase crystallization (SPC) of amorphous films at the annealing temperature region of $900-1100^{\circ}C$ for 2 h in a pure oxygen atmosphere. The amorphous films were deposited on polycrystalline $BaZrO_3$ (poly-BZO) substrates by dc-magnetron sputtering at room temperature. The Curie temperatures ($T_C$) of all composite films were insignificantly altered in the range of 368-372 K. The highest LFMR value of 1.29 % in 0.5 kOe with the maximum dMR/dH value of $37.4%kOe^{-1}$ at 300 K was obtained from 900 nm-thick composite film annealed at $1100^{\circ}C$. The improved LFMR properties of the composite films are attributed to effective spin-dependent scattering at the $La_{0.7}Sr_{0.3}Mn_{1+d}O_3$ grain boundaries sharpened by adjacent chemically compatible $Mn_3O_4$ grains.

Modelling and integrity assessment of shear connectors in precast cast-in-situ concrete bridges

  • Moyo, Pilate;Sibanda, Bongani;Beushausen, Hans
    • Structural Engineering and Mechanics
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    • v.42 no.1
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    • pp.55-72
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    • 2012
  • Precast-cast insitu concrete bridge construction is widely practiced for small to medium span structures. These bridges consist of precast pre-stressed concrete beams of various cross-sections with a cast in-situ reinforced concrete slab. The connection between the beams and the slab is via shear links often included during the manufacturing process of the beams. This form of construction is attractive as it provides for standardisation, reduced formwork and construction time. The assessment of the integrity of shear connectors in existing bridges is a major challenge. A procedure for assessment of shear connectors based on vibration testing and finite element model updating is proposed. The technique is applied successfully to a scaled model bridge model and an existing bridge structure.

Formation of $Fe_3AlC$ Base Alloy by Mechanical Alloying and Vacuum Hot Pressing

  • Isonishi, Kazuo
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.1290-1291
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    • 2006
  • Fabrication of $Fe_3AlC$ matrix in-situ composite, reinforced by a FeAl phase, was studied by using the powder metallurgical processing route. Especially, in order to disperse the second phase more finely, we chose the mechanical alloying process. We investigated the microstructural and mechanical properties of the consolidated material. After consolidation by vacuum hot pressing, the compact showed almost full density and consisted of a $Fe_3AlC$ matrix and FeAl second phase (average particle size was less than 1m). The compact showed HV746, which was higher than that of the arc melted $Fe_3AlC$ monolithic material, HV603.

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Organic-Inorganic nani-Composite of PMMA-Forsterite Doped with $Eu^{+3}$

  • Park, Dong Gon;Gang, Jin;Gwon, Hae Yeong
    • Bulletin of the Korean Chemical Society
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    • v.21 no.6
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    • pp.604-610
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    • 2000
  • Drying-step in sol-gel processing was bypassed by exchanging alcoholic solvent in forsterite alcogel directly with MMA. By in-situ polymerization of the MMA, organic-inorganic nano-composite of PMMA-forsterite was prepared. As porous nature of inorganic networks in the gel was preserved and fixated in the composite, spherical morphology of PMMA was resulted. The PMMA-forsterite composite was optically transparent, machinable,mechanically sustainable, and thermally more stable than pristine PMMA. When doped with $Eu^{+3}$, inorganic moiety in the composite provided site environment that is very different from that in pristine PMMA. Prominent $^{5}D_0$$^{7}F_0$ transition at 578 nm, broken degeneracy in $^{5}D_0$$^{7}F_1$ and $^{5}D_0$$^{7}F_2$ transitions suggested that $Eu^{+3}$ was exclusively doped in the inorganic moiety of the composite, which had lower symmetry than the organic counterpart.

Microstructure and Mechanical Properties of Ni3Al Matrix Composites with Fine Aluminum Oxide by PM Method

  • Han, Chang-Suk;Choi, Dong-Nyeok
    • Korean Journal of Materials Research
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    • v.28 no.9
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    • pp.495-498
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    • 2018
  • Intermetallic compound matrix composites have been expected to be established as high temperature structural components. $Ni_3Al$ is a representative intermetallic alloy, which has excellent ductility even at room temperature by adding certain alloying elements. $Ni_3Al$ matrix composites with aluminum oxide particles, which are formed by the in-situ reaction between the alloy and aluminum borate whiskers, are fabricated by a powder metallurgical method. The addition of aluminum borate whiskers disperses the synthetic aluminum oxide particles during sintering and dramatically increases the strength of the composite. The uniform dispersion of reaction synthesized aluminum oxide particles and the uniform solution of boron in the matrix seem to play an important role in the improvement in strength. There is a dramatic increase in strength with the addition of the whisker, and the maximum value is obtained at a 10 vol% addition of whisker. The $Ni_3Al$ composite with 10 vol% aluminum oxide particles $0.3{\mu}m$ in size and with 0.1 wt% boron powder fabricated by the conventional powder metallurgical process does not have such high strength because of inhomogeneous distribution of aluminum oxide particles and of boron. The tensile strength of the $Ni_3Al$ with a 10 vol% aluminum borate whisker reaches more than twice the value, 930 MPa, of the parent alloy. No third phase is observed between the aluminum oxide and the matrix.

Modelling of headed stud in steel-precast composite beams

  • El-Lobody, Ehab;Lam, Dennis
    • Steel and Composite Structures
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    • v.2 no.5
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    • pp.355-378
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    • 2002
  • Use of composite steel construction with precast hollow core slabs is now popular in the UK, but the present knowledge in shear capacity of the headed shear studs for this type of composite construction is very limited. Currently, all the information is based on the results obtained from experimental push-off tests. A finite element model to simulate the behaviour of headed stud shear connection in composite beam with precast hollow core slabs is described. The model is based on finite element method and takes into account the linear and non-linear behaviour of all the materials. The model has been validated against the test results, for which the accuracy of the model used is demonstrated. Parametric studies showing the effect of the change in transverse gap size, transverse reinforcement diameter and in-situ concrete strength on the shear connection capacity are presented.

Nano-Composite Solder Technology for the Improvement of Solder Joint Properties (무연솔더 접합부 특성향상을 위한 나노복합솔더 기술)

  • Ki, Won-Myoung;Lee, Young-Kyu;Lee, Chang-Woo;Yoo, Se-Hoon
    • Journal of the Microelectronics and Packaging Society
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    • v.18 no.3
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    • pp.9-17
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    • 2011
  • Nano-composite solders have been studied to improve the properties of Pb-free solder joints. The nanoparticles in the composite solders were carbon nanotubes(CNTs), metals (Ag, Ni, Cr, etc.), ceramics (SiC, $ZrO_2$, $TiB_2$, etc.). To fabricate the nano-composite solders, mechanical mixing methods and in-situ fabrication method has been used for well-dispersed nano phase. The characteristic properties of the nano-composite solders were high creep resistance, low undercooling, low IMC growth rate and fine microstructures. More researches on the nano-composite solders are required to improve the processibility and the reliability of the nano-composite solder joints.

Formation of TiC Composite Layer on Ductile Iron by Laser Surface Modification (레이저 처리에 의한 구상흑연주철의 TiC 복합화에 관한 연구)

  • Kim, Woo-Yeol;Park, Heung-Il
    • Journal of Korea Foundry Society
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    • v.18 no.6
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    • pp.593-603
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    • 1998
  • Commercial ductile iron was coated with titanium and aluminum powders by low pressure plasma spraying and then irradiated with a $CO_2$ laser to produce anti-corrosive TiC composite layer. TiC carbides were precipitated homogeneously in a laser alloyed layer by in-situ reaction between carbon existed in the base metal and titanium with thermal sprayed coating. The formation of gas pores and brittle limited mixing zone with ledeburite microstructure in TiC composite layer were surpressed by the complementary alloying of aluminum. The hardness of TiC composite layer obtained by addition of titanium and aluminum was between 600 and 660 Hv, which was three times as high as the hardness of ferritic ductile iron. From the results of isothermal oxidation at 1123k for 24 hours in air, high temperature oxidation resistance of the TiC composite layer with aluminum was improved and doubled when compared with the TiC composite layer without aluminum.

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Novel OLED structure allowing for the in-situ ohmic contact and reduction of charge accumulation in the device

  • Song, Won-Jun;Kristal, Boris;Lee, Chong-Hoon;Sung, Yeun-Joo;Koh, Sung-Soo;Kim, Mu-Hyun;Lee, Seong-Taek;Kim, Hye-Dong;Lee, Chang-Hee;Chung, Ho-Kyoon
    • 한국정보디스플레이학회:학술대회논문집
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    • 2007.08a
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    • pp.1014-1018
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    • 2007
  • We have demonstrated the enhancement of the power efficiency and device lifetime of organic light-emitting diodes (OLEDs) by introducing the ETL 1 / ETL2 (composite ETL) structure between EML and cathode and the HIL1 (composite HIL) / HIL2 between anode and HTL. Compared to reference devices retaining conventional architecture, novel OLED structure shows an outstanding EL efficiency that is 1.6 times higher (${\sim}4.5$ lm/w versus ${\sim}$ 2.71 lm/w for the reference device) and lower driving voltage $({\bigtriangleup}V>1V)$, but also a longer lifetime and smaller operating voltage drift over time. It is suggested in this work that the device performance can be improved by in-situ ohmic contact through novel electron controlled structure and reduction of charge accumulation in the interface through composite HIL

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