• Journal of Advanced Marine Engineering and Technology
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• 제21권1호
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• pp.49-58
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• 1997

The membrane type LNG tank is non self-supporting tank which consists of both primary and secondary membrane supported through the insulation boxes by the adjacent hull struc¬ture. Although the membranes are not structural member. They are subject to periodical cyclic loads due to the thermal expansion and other expansions or contraction of membrane. At the design stage of the tank, an analytical and experimental approach on the fatigue strengths of membrane and its welds is necessary in order to assist the designer and the inpector. In this study the evaluation method of fatigue strength of membrane type LNG tank is pre¬sented with FEM analysis and fatigue test of lap welds and it contains the following:1) The fatigue tests and preparation of design S - N curve for lap welds 2) FEM analysis of test specimens 3) Estimation of cumulative damage factor of lap welds 4) Guideline for inspection of lap welds of membrane type LNG tank As the results of analytical and experimental approaches in this study, the evaluation method of fatigue strengths of membrane type LNG tank is proposed, which is expected to be useful for design and inspection of membrane type LNG tank.

• 청정기술
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• 제13권4호
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• pp.274-280
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• 2007

본 연구에서는 염화 제2철 수용액의 재생 공정에 주로 쓰이고 있는 철환원법을 대체하기 위한 방법으로, 액-액 용매 추출법을 사용하여 수용액 내에 잔존해 있는 중금속인 Fe와 Ni을 분리 회수하는 공정을 개발하였다. Lab 실험을 통해 우선 염화 제2철 수용액으로부터 선택적으로 염화 제2철만을 추출할 수 있는 용매조건을 개발하였고, 그 결과를 사용하여 액-액 추출공정의 상업화 추진을 위한 pilot 공정 및 장치를 개발하였다. 또한 pilot test를 통하여 추출단과 역추출단의 단수를 결정할 수 있었고, 양산 공정에 적용할 수 있는 공정 데이터를 확보하였다.

• 한국정밀공학회지
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• 제26권6호
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• pp.50-58
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• 2009

Micro laser fabrication techniques can potentially be used for the manufacture of microstructures on the thin flat surfaces with large diameter that are frequently used in semiconductor industries. However, the large size of wafers can cause the degraded machining accuracy of the surface because it can be tilted or distorted by geometric errors of machines or the holding fixtures, etc. To overcome these errors the off-line focusing error compensation method is proposed. By using confocal autofocus system, the focusing error profile of machined surface is measured along the pre-determined path and can be compensated at the next machining process by making the corrected motion trajectories. The experimental results for silicon wafers and invar flat surfaces show that the proposed method can compensate the focusing error within the level of below $6.9{\mu}m$ that is the depth of focus required for the laser micromachining process.

• Journal of Welding and Joining
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• 제13권3호
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• pp.18-33
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• 1995

천연가스는 지구상에서 비교적 광범위하게 생산되며 구미 등에서는 대부분 pipe line으로 소비지까지 운송하여 사용하고 있지만 일본 등에서는 액화 천연가스 (LNG)로 저장, 수송하여 사용하고 있다. LNG 저장탱크는 생산측의 액화기지와 사용측 의 수입기지에 설치되며 지금까지 약 240기가 건설되어 있다. 종래 탱크 1기의 용량 은 대부분 6 - 8만m$^{3}$ 규모였지만, 토지의 유효이용 등으로 대형화되고 있으며, 또 지상식에서는 PC(Prestressed Concrete)의 방파제를 외부탱크에 근접시켜 외부탱크 와 일체화시킨 PC LNG 탱크가 개발.설계되었다. 일본에서는 이미 이 방식으로 세계 최대규모인 14만m$^{3}$ 탱크가 건조되어 가동 중이다. LNG의 주성분은 메탄이고 비등점은 -161.5.deg.C로 극저온이다. 이러한 저온에서도 취화되지 않고 사용할 수 있는 재료는 9%Ni강, Al 합금, 스테인레스강 및 Invar 등이 있지만, 탱크의 대형화에 따라 가공성, 용접성 및 경제성을 고려하여 요즈음은 9%Ni강이 주로 사용되고 있다. 한편 9%Ni강용 용접재료는 고Ni계 합금 및 모재와 동일한 성분계의 공금계가 있지만 지금까지 고 Ni계 합급이 주로 사용되고 있다. 본 내용에서는 9%Ni강을 사용한 지상식 평지원통형 LNG 탱크를 예로 들어 탱크의 개요 및 용접재료, 용접시공 등을 포함한 용접기술에 대해서 개괄적으로 설명하고자 한다.

• 대한조선학회논문집
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• 제48권3호
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• pp.200-206
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• 2011

The mechanical properties of the most widely used cryogenic materials, i.e. austenitic stainless steel (ASS), aluminum alloy and invar steel, strongly depend on temperatures and strain rates. These phenomena show very complicated non-linear behaviors and cannot be expressed by general constitutive equation. In this study, an unified constitutive equation was proposed to represent the effect of temperature and strain rate on the materials. The proposed constitutive equation has been based on Tomita/Iwamoto and Bodner/Partom model for the expression of 2nd hardening due to martensite phase transformation of ASS. To simulate ductile fracture, modified Bodner/Chan damage model was additionally applied to the model and the model validity was verified by comparison of experimental and simulation results.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2008년도 하계학술대회 논문집 Vol.9
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• pp.220-220
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• 2008

물 첨가 열화학기상증착을 이용하여 750도에서 길고 수직 성장한 다중벽 탄소나노튜브를 합성하였다. 사용된 기판으로는 우선 실리콘 웨이퍼에 열 증착기로 확산 방지층으로 Ti 50 nm를 입히고 그 위에 Al 15 nm를 입히고 난 후 촉매 층으로 Invar 36 (63 wt% Fe, 37 wt% Ni)을 1 nm 얇게 증착하였다. 탄소나노튜브의 성장에 사용된 가스는 Ar, $C_2H_2$ 이다. Ar은 분위기 가스로 사용되었고, $C_2H_2$는 탄소나노튜브의 성장에 관여하는 가스이다. 또한, 합성중에 약간의 물을 첨가함으로 기존의 탄소나노튜브 성장 길이보다 10배 가량 더 성장 하였다. 이것은 합성 중의 물 첨가로 인해 촉매 입자들의 활동성이 기존에 비해 더 증가했다는 것을 보여준다. 합성된 탄소나노튜브의 길이와 정렬도를 보기 위해 주사전자현미경 (scanning electron microscopy, SEM)을 이용하였고, 탄소나노튜브의 지름과 벽의 개수를 파악하기 위해 투과전자현미경 (transmission electron microscopy)을 이용하였다.

• 대한전기학회:학술대회논문집
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• 대한전기학회 2006년도 추계학술대회 논문집 전기물성,응용부문
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• pp.38-39
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• 2006

We present experimental results that regard the effects of catalyst preparation on the structural and field-emissive properties of CNTs. The CNTs used in this research have been synthesized using the inductively coupled plasma-chemical vapor deposition (ICP-CVD) method. Catalyst materials (such as Ni, Co, and Invar 426) are varied and deposited on buffer films by RF magnetron sputtering. Prior to growth of CNTs, $NH_3$ plasma etching has also been performed with varying plasma etching time and power. For all the CNTs grown, nanostructures and morphologies are analyzed using Raman spectroscopy and FESEM, in terms of buffer films, catalyst materials, and pre-treatment conditions. Furthermore, the field electron-emission of CNTs are measured and characterized in terms of the catalyst preparation environments. The CNTs grown on Nicatalyst layer would be more effectual for enhancing the growth rate and achieving the vertical-alignment of CNTs rather than other buffer materials from results of SEM study. The crystalline graphitic structure of CNTs is improved as the catalyst dot reaches a critical size. Also, the field-emission result shows that the CNTs using Ni catalyst would be more favorable for improving electron-emission capabilities of CNTs compared with other samples.

• 한국전기전자재료학회논문지
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• 제21권2호
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• pp.162-172
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• 2008

We studied the effect of an Al underlayer on the growth of carbon nanotubes (CNTs) and their field emission characteristics, First of all, CNTs were grown on the Invar catalyst layers with different thickness of 1 to 10 nm, showing that the CNT length was saturated for the catalyst 5 nm or thicker. The CNTs grown on the 5-nm-thick catalyst were ${\sim}10{\mu}m$ long and ${\sim}30nm$ in diameter. Second, an Al underlayer was applied between the catalyst layer and the Ti diffusion barrier to reduce the diameters of CNTs for better field emission properties by forming spherical Al oxide particles on which smaller catalyst nanoparticles would occur. The optimal thickness of an Al underlayer underneath the 5-nm-thick catalyst was ${\sim}15nm$, producing the CNTs with the length of ${\sim}15{\mu}m$ and the diameter of ${\sim}15nm$. The field emission measurements, following the tape activation, showed that the thinner and longer CNTs gave rise to better field emission performance with the lower turn-on and threshold electric fields.

• 한국우주과학회:학술대회논문집(한국우주과학회보)
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• 한국우주과학회 2010년도 한국우주과학회보 제19권1호
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• pp.25.3-25.3
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• 2010

Our previous study used a bar-type reference mirror to measure the relative distance to the target surface. The target measurement accuracy was required to $1{\mu}m$ PV for aspheric optical surface up to 1m in diameter. Earlier system suffers from the reference surface deformation when the measuring part moves. In order to reduce the deformation, measuring part and the reference part separated from each order in the new design. This system utilizes a kinematic support assembly using invar flexure to minimize the reference surface deformation under gravity and vibration. The surface deformation requirement of reference mirror is defined as of $0.2{\mu}m$ under gravity and 40Hz vibration. The finite element results, shows reference mirror deformation of $0.164{\mu}m$. The first resonance mode was computed to analysis 46.05Hz for reference part and 43.44Hz for measuring part. Thesis satisfies the frequency requirement.

• Corrosion Science and Technology
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• 제22권6호
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• pp.478-483
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• 2023

This study examined the corrosion behavior of bimetal materials composed of Fe-Ni alloy and Fe-Ni-Mo alloy, both suitable for use in electromagnetic switches. Electrochemical polarization and weight loss measurements revealed that, in contrast to Fe-Ni alloy, which exhibited pseudo-passivity behavior, Fe-Ni-Mo alloy had higher anodic current density, displaying only active dissolution and greater weight loss. This indicated a lower corrosion resistance in the Fe-Ni-Mo alloy. Equilibrium calculations for the phase fraction of precipitates suggested that the addition of 1 wt% Mo may lead to the formation of second-phase precipitates, such as Laves and M₆C, in the γ matrix. These precipitates might degrade the homogeneity of the passive film formed on the surface, leading to localized attacks during the corrosion process. Therefore, considering the differences in corrosion kinetics between these bimetal materials, the early degradation caused by galvanic corrosion should be prevented by designing a new alloy, optimizing heat treatment, or implementing periodic in-service maintenance.