• 제목/요약/키워드: Hot Forming

검색결과 448건 처리시간 0.025초

산업 설비 재료에 CCO박막의 적용을 위한 부식성 분석 (Corrosion analysis for application of CCO thin films to industrial equipment materials)

  • 백민숙
    • 한국산학기술학회논문지
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    • 제19권6호
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    • pp.98-103
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    • 2018
  • 산업의 발전에 따라 설비 및 재료 등 따라서 재료 표면의 특성을 내식성 및 고강도, 내마모성 등을 향상 시키기 위하여 지금까지 많은 코팅 기술들이 발전해 왔다. 그 중 CCO(CaCoO, 이후 CCO) 박막 형성은 전자재료 영역에서 연구, 사용이 되어오고 있는데, 이 CCO 박막의 특징 중 하나가 고온의 열에 강하다는 것이 있다. 특히 CCO 박막을 형성 시키는 방법 또한 비교적 간단하여 고온의 산화 분위기에 도입이 가능 할 것으로 판단되었다. 따라서 본 연구에서는 이 CCO 박막의 코팅이 용융 아연 도금 설비에 적용을 하기 전에, 고온 및 Zn fume에 대한 부식성을 파악하여 용융 아연 도금 설비에 적용이 가능한지를 파악하기 위한 실험 및 분석을 실시 하였다. 우선 기본 소재 STS304 표면에 CCO 박막을 형성 시키고, 650도의 대기로에서 Zn fume의 분위기 내에서 산화 시킨 후 CCO 박막의 부식 정도를 확인 및 측정 하였다. 산화는 30일간 진행되었고, 30일 후 SEM을 이용하여 CCO박막의 형상을 확인 하였으며 동전위분극 실험을 통하여 부식성을 분석하였다.

액상소결에 의한 $\beta-SiC-TiB_2$ 복합체의 제조와 특성 (Manufacture of $\beta-SiC-TiB_2$ Composites Densified by Liquid-Phase Sintering)

  • 신용덕;주진영;박미림;소병문;임승혁;송준태
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2000년도 추계학술대회 논문집 학회본부 C
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    • pp.479-481
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    • 2000
  • The effect of $Al_{2}O_{3}+Y_{2}O_{3}$ additives on fracture toughness of $\beta-SiC-TiB_2$ composites by hot-pressed sintering were investigated. The f$\beta-SiC-TiB_2$ ceramic composites were hot-presse sintered and annealed by adding 16, 20, 24wt% $Al_{2}O_{3}+Y_{2}O_{3}$(6 : 4wt%) powder as a liquid forming additives at low temperature($1800^{\circ}C$) for 4h. In this microstructures, the relative density is over 95.88% of the theoretical density and the porosity increased with increasing $Al_{2}O_{3}+Y_{2}O_{3}$ contents because of the increasing tendency of pore formation. The fracture toughness showed the highest of $5.88MPa{\cdot}m^{1/2}$ for composites added with 20wt% $Al_{2}O_{3}+Y_{2}O_{3}$ additives at room temperature. The electrical resistivity showed the lowest of $5.22{\times}10^{-4}\Omega{\cdot}cm$ for composite added with 20wt% $Al_{2}O_{3}+Y_{2}O_{3}$ additives at room temperature and is all positive temperature coefficient resistance (PTCR) against temperature up to $700^{\circ}C$.

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$\beta-SiC-ZrB_2$ 복합체의 파괴인성 증진연구 (A Study on Improvement of Fracture Toughness of $\beta-SiC-ZrB_2$Composites)

  • 신용덕;주진영;윤세원;황철;송준태
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1999년도 춘계학술대회 논문집
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    • pp.291-294
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    • 1999
  • The effect of AI$_2$O$_3$+Y$_2$O$_3$additives on fracture toughness of $\beta$-SiC-ZrB$_2$composites by hot-pressed sintering were Investigated. The $\beta$-SiC-ZrB$_2$ ceramic composites were hot-presse sintered and annealed by adding 1, 2, 3wt% AI$_2$O$_3$+Y$_2$O$_3$(6:4wt%) powder as a liquid forming additives at 195$0^{\circ}C$ for 4h. In this microstructures, no reactions were observed between $\beta$-SiC and ZrB$_2$, and the relative density Is over 90.79% of the theoretical density and the porosity decreased with increasing AI$_2$O$_3$+Y$_2$O$_3$ contents. Owing to crack deflection and crack bridging of fracture toughness mechanism, the fracture toughness showed the highest of 5.5328MPa . m$^{1}$2/ for composites added with 2wt% AI$_2$O$_3$+Y$_2$O$_3$ additives at room temperature. But the standard deviation of fracture toughness of specimens decreased with increasing AI$_2$O$_3$+Y$_2$O$_3$ contents and showed the highest of 0.8624 for composite tilth 1wt%, AI$_2$O$_3$+Y$_2$O$_3$additives.

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無加壓 열처리에 의한 ${\beta}$-SIC-TiB$_2$ 複合體의 製造와 特性 (Manufacture and Properties of ${\beta}$-SIC-TiB$_2$ Composites Densified by Pressureless Annealing)

  • 신용덕;주진영;박미림
    • 대한전기학회논문지:전기물성ㆍ응용부문C
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    • 제50권5호
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    • pp.221-225
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    • 2001
  • The effect of $Al_2O_3+Y_2O_3$ additives on fracture toughness of ${\beta}-SiC-TiB_2$ composites by hot-pressed sintering was investigated. The ${\beta}-SiC-TiB_2$ ceramic composites were hot-press sintered and pressureless-annealed by adding 16, 20, 24 wt% ${\beta}-SiC-TiB_2$(6:4 wt%) powder as a liquid forming additives at low temperature(1800 $^{\circ}C$) for 4 h. Phase analysis of composites by XRD revealed mostly of ${\alpha}$-SiC(6H), $TiB_2$, and YAG($Al_5Y_3O_{12}$). The relative density was over 95-88 % of the theoretical density, and the porosity increased with increasing $Al_2O_3+Y_2O_3$ contents because of the increasing tendency of pore formation. The fracture toughness showed the highest value of 5.88 MPa${\cdot}m^{1/2}$ for composites added with 20 wt% $Al_2O_3+Y_2O_3$ additives at room temperature. The electrical resistivity showed the lowest value of $5.22{\times}10^{-4}\;{\Omega}\;{\cdot}\;cm$ for composite added with 20 wt% $Al_2O_3+Y_2O_3$ additives at room temperature, and was all positive temperature coefficeint resistance(PTCR) against temperature up to 900 $^{\circ}C$.

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방사선 조사 고추장의 발효 특성 (Fermentation Properties of Irradiated Kochujang)

  • 김문숙;오진아;김인원;신동화;한민수
    • 한국식품과학회지
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    • 제30권4호
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    • pp.934-940
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    • 1998
  • Kochujang, fermented hot pepper soybean paste, was prepared by traditional method, and irradiated with gamma ray of $^{60}Co{\;}up{\;}to{\;}15{\pm}1.5{\;}kGy$ for confirming main factor of kochujang fermentation. Nonirradiated (control) and irradiated samples kochujang were fermented at $25^{\circ}C$ and analyzed biochemical properties including enzyme activities and viable cell count during fermentation for 60 days. The total viable count in irradiated kochujang decreased to $10^4{\;}CFU/g$ which was $10^8{\;}CFU/g$ in the control. Because of a little changing enzyme activities of ${\alpha}{\cdot}{\beta}{\;}amylase$ and acid neutral protease by irradiation at the above level, amino type nitrogen which is the main quality reference of kochujang was comparable to the control. By irradiation, gas production was completely stopped which is one of biggest problems during distribution of kochujang. Total volume of gas produced at $25^{\circ}C$ from the control kochujang was 453 mL/100 g which was composed of over 90% of $CO_2$. The odor of irradiated kochujang was inferior to the control which seemed to be related to reduced microbial populations.

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대향분출류가 있는 맥동연소기의 비정상 점화현상 (Unsteady Ignition in the Pulse Combustor with Counter Jet Flows)

  • 이창진
    • 한국추진공학회지
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    • 제1권1호
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    • pp.64-72
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    • 1997
  • 맥동연소의 비정상 점화현상을 연구하기 위하여 이론적인 해석을 수행하였다. 맥동연소에서는 연소기의 양쪽에서 유입되는 고온의 연소가스와 미연 혼합가스가 연소실 내부에서 충돌하여 정체면을 형성하며 유동변형율이 임계 값 이하가 될 때까지 점화가 억제된다. 본 연구에서는 유동의 유동변형율의 변화에 대한 점화현상의 반응을 연구하기 위하여 활성화 에너지 점근법과 비가역 1단계 화학반응을 이용하였다. 또한 유동에 의한 유동변형율은 두 가지 요인에 의하여 발생하는 것으로 모델링 하였는데, 비정상 유동에 의한 평균 유동변형율과 난류에 의하여 유도되는 유동변형율이 그것이다. 해석 결과에 의하면, 맥동연소에서는 잘 정의된 점화지연이 존재하며, 점화 또는 소염의 발생 여부는 Damkohler 수에 의하여 거의 결정된다.

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후판 압연공정에서 퍼지 두께제어 구현 (An Implementation of Fuzzy Automatic Gauge Control for the Plate Steel Rolling Process)

  • 허윤기;최영규
    • 제어로봇시스템학회논문지
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    • 제15권6호
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    • pp.634-640
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    • 2009
  • The plate manufacturing processes are composed of the reheating furnace, finishing mill, cooling process and hot leveling. The finishing rolling mill (FM) as a reversing mill has produced the plate steel through multiple pass rolling. The automatic gauge control (AGC) is employed to maintain the thickness tolerance. The high grade products are forming greater parts of the manufacturing and customers are requiring strict thickness margin. For this reason, the advanced AGC method is required instead of the conventional AGC based on the PI control. To overcome the slow response performance of the conventional AGC and the thickness measurement delay, a fuzzy AGC based on the thickness deviation and its trend is proposed in this paper. An embedded controller with the fuzzy AGC has been developed and implemented at the plate mill in POSCO. The fuzzy AGC has dynamically controlled the roll gap in real time with the programmable logic controller (PLC). On line tests have been performed for the general and TMCP products. As the results, the thickness deviation range (maximum - minimum of the inner plate) is averagely from 0.3 to 0.1 mm over the full length. The fuzzy AGC has improved thickness deviation and completely satisfied customer needs.

Mg-3%Zn-0.5%Sn계 판재합금의 기계적 성질과 성형성에 미치는 미량합금원소의 영향 (Effects of Minor Alloying Elements on the Mechanical Properties and Formability of Mg-3%Zn-0.5%Sn Base Sheet Alloys)

  • 김정민;박준식;김하영;김기태
    • 열처리공학회지
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    • 제21권2호
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    • pp.87-93
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    • 2008
  • A variety of minor alloying elements such as Zr, Sr, Y, and Gd were added to Mg-3%Zn-0.5%Sn base alloy to form various fine precipitates and their effects on the microstructure, tensile properties, and sheet metal formability were investigated. Various very fine precipitates along with fine second phases were observed by the additions. It was found that Zr or Gd additive has a role to suppress the grain coarsening of alloy sheets during the hot working process. The Zr-added alloy showed the highest tensile elongation at $250^{\circ}C$ whereas the Gd-added alloy exhibited the best sheet metal forming characteristics in terms of CCV (conical cup value) and spring-back tendency.

발사체 연소기 제작에서 스피닝 공정 개발 동향 (Developing Trends of Spinning Process for Manufacturing Thrust Chamber of Launch Vehicle)

  • 이금오;유철성;최환석;허성찬;곽준영;최윤호
    • 한국추진공학회지
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    • 제19권6호
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    • pp.64-71
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    • 2015
  • 스피닝 공정은 축대칭의 얇은 두께를 가지고 있는 속이 빈 실린더형 단면을 가지고 있는 부품에 일반적으로 사용된다. 전통적인 스피닝 제작 기술은 컨벤셔널 스피닝과 파워 스피닝(전단 스피닝과 유동성형)으로 구분된다. 액체추진로켓의 연소기의 재생냉각 챔버와 확대노즐부에서 적용된 스피닝에 대한 문헌조사를 수행하였다. 연소실과 노즐의 제작에 사용되는 스피닝은 대부분 맨드럴을 사용하였다. 최근에는 전통적인 냉간 스피닝에 비해 열간 스피닝도 많이 사용되고 있었다.

폴리머-탄소나노튜브 복합체 에어로졸 입자의 생성 및 이를 이용한 하이브리드 복합체 박막 제조 (Synthesis of Polymer-Carbon Nanotubes Composite Nanoparticles and Their Applications into Forming Hybrid Composite Thin Films)

  • 김휘동;안지영;김수형
    • 한국입자에어로졸학회지
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    • 제6권2호
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    • pp.61-67
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    • 2010
  • In this paper, we describe a new method to form polymer thin films, in which carbon nanotubes (CNTs) are homogeneously distributed so that they can strengthen the mechanical property of resulting polymer film. To do so, we first homogeneously mixed CNTs with polymer in a DMF solvent. With the assistance of ultrasonic nebulizer, the polymer/CNT solution was then aerosolized into micro-sized droplets and finally turned into solidified polymer/CNT composite particles by gas-phase drying process. As the results of SEM and TEM analysis, CNTs were found to be homogeneously immobilized in the polymer matrix particles due to rapid drying process in the gas phase. For comparison purpose, (i) the polymer/CNTs composite particles prepared by aerosol processing method and (ii) polymer/CNTs sheets prepared by simple solution-evaporation method were employed to form polymer/CNTs composite thin films using a hot press. As the result, the aerosol processing of composite particles was found to be a much more effective method to form homogeneously distributed-CNTs in the polymer matrix thin film.