• 한국음향학회지
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• 제23권7호
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• pp.497-502
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• 2004

Poly (sodium 4-styrenesulfonate) 수용액에 대한 3 MHz의 초음파 음속측정과 0.2-2.2 MHz의 범위에 대한 흡수계수를 측정하였다. 음속은 펄스법을 사용하여 농도 5-25 wt%, 온도 10-90 ℃에 대하여 측정한 결과, 농도 25, 20, 15, 10, 5 wt%에 대한음속의 최대치 온도는 각각 55, 59, 63, 67, 71 ℃이였다. 흡수계수측정은 광 회절 초음파공명법을 사용하여 농도 5-25 wt%, 20 ℃에서 행하였다. 그 결과, 200 kHz부근에서 고분자 chain의 부분운동에 의한 완화현상을, 1 MHz 부근에서는 술폰기 (SO₃)의 proton의 전이에 의한 완화현상을 각각 관측하였다. 흡수계수와 점성은 농도와 함께 증가하였으나 온도증가에 대해서는 감소하였다.

• Macromolecular Research
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• 제12권6호
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• pp.559-563
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• 2004

Both the ultrasonic velocity at 3 MHz and the absorption coefficient in the frequency range from 0.2 to 2 MHz were measured for aqueous solutions of poly(sodium 4-styrenesulfonate) over the concentration range from 5 to $25\%$ (by weight). The pulse echo overlap method was employed to measure the ultrasonic velocity over the temperature range from 10 to $90^{\circ}C;$ the high-Q ultrasonic resonator method was used for the measurement of the absorption coefficient at $20^{\circ}C.$ The velocities exhibited their maximum values at ca. 55, 59, 63, 67, and $71^{\circ}C.$ for the 25, 20, 15, 10, and $5\%$ solutions, respectively. The velocity increased with respect to the poly(sodium 4-styrene-sulfonate) concentration at a given temperature. A study of the concentration dependence of the both the relaxation frequency and amplitude indicated that the relaxation at ca. 200 kHz is related to structural fluctuations of the polymer molecules, such as the segmental motions of the polymer chains and that the relaxation at ca. 1 MHz resulted from the proton transfer reactions of the oxygen sites of $SO_3.$ Both the absorption and the shear viscosity increase upon increasing the polymer concentration, but they decrease upon increasing the temperature.

• 동력기계공학회지
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• 제9권2호
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• pp.33-39
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• 2005

Experiments are performed to study the mixed convection flow and heat transfer in an inclined parallel plates with the upper part cooled and the lower part heated uniformly. The Reynolds number ranges from $4.0{\times}10^{-3}\;to\;6.2{\times}10^{-2}$, the angle of inclination, ${\theta}$, from 0 to 45 degree from the horizontal line, and Pr of the high viscosity fluid is 909. In this paper, the PIV(Particle image velocimetry) with TLC(Thermo-sensitive liquid crystal) tracers is used for visualizing and analysis. This method allows simultaneous measurement of velocity and temperature field at a given instant of time. Quantitative data of the temperature and velocity are obtained by applying the color-image processing to a visualized image, and neural network is applied to the color-to-temperature calibration. This paper describes the methods, and presents the quantitative visualization of mixed convection. From this study, it is found that the flow pattern can be classified into three patterns which are affected by Reynolds number and the angle of inclination.

• Macromolecular Research
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• 제13권1호
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• pp.14-18
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• 2005

Under irradiation in a microwave oven, six novel poly(amide-imide)s containing tetrahydropyrimidinone, tetrahydro-2-thioxopyrimidine moieties and trimellitic rings in their main chains were synthesized through the polycondensation reaction of N,N'-(4,4'-diphenylether)bis(trimellitimide) diacid chloride with six different derivatives of tetrahydropyrimidinone and tetrahydro-2-thioxopyrimidine in the presence of a small amount of a polar organic medium, such as o-cresol. The polycondensation proceeded rapidly and completed within 7-9 min, producing a series of new poly(amide-imide)s in high yield that showed inherent viscosities in the range 0.33-0.52 dL/g. These poly(amide-imide)s were characterized by elemental analysis, viscosity measurement, thermal gravimetric analysis, solubility test, and FT-IR spectroscopy. All of the polymers were soluble at room temperature in polar solvents such as N,N-dimethylacetamide, N,N-dimethylformamide, dimethylsulfoxide, tetrahydrofuran, and N-methyl-2-pyrrolidone.

• 한국재료학회지
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• 제11권2호
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• pp.137-145
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• 2001

수용액 매체에서 젤케스팅을 이용하여 복잡한 형상의 세라믹스를 제조하기 위한 새로운 공정을 연구하였다 용융실리카 분말과 첨가제로서 지르콘과 코디어라이트 조성으로 혼합된 현탁액을 electrosteric 방법으로 안정화시켰다. 슬립은 다성분계 세라믹 현탁액에 단량체, 이량체 그러고 분산제를 혼합하고, 볼밀하여 준비하였다. 슬립의 유동학적 특성을 평가하기 위해 점도를 측정하였으며 , 낮은 점도를 갖는 50vo1%의 고농도 다성분계 세라믹 슬립의 제조가 가능하였다. 슬립의 점도는 고분자 분산제의 함량과 단량체 및 이량체의 혼합비에 크게 의존하였다. 성형체는 안정화시킨 슬립을 몰드에 부어 상온에서 젤화시킨 후 $25^{\circ}C$, 80~85% 상대습도 분위기 하에서 48시간동안 건조시켜 제조하였으며 건조된 성형체에는 균열이 발생하지 않았다.

• 한국조리학회지
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• 제19권3호
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• pp.142-155
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• 2013

들깨분말을 기능성 식품으로 이용하기 위하여 들깨분말 첨가비율을 달리하여 만든 반죽의 물성특성과 식빵을 제조한 후 물리화학적, 기계적, 관능적 품질특성을 분석하여 들깨분말을 첨가한 식빵의 최적의 배합비를 찾고 기능성 재료로 가능성을 확인하였다. 들깨분말의 일반성분은 수분함량은 6.60%, 조단백은 23.04%, 조지방은 51.62%, 조회분 함량은 3.46%로 나타났다. 들깨분말 첨가 식빵 반죽의 sedimentation value와 pelshenke value는 첨가량이 증가할수록 감소하였다. Farinograph 측정 결과 반죽의 consistency, water absorption와 tolerance index은 첨가량이 증가할수록 증가하였고 stability와 time breakdown은 감소 하였다. Amylograph 측정 결과 pasting temperature, peak viscosity, hot past viscosity, final viscosity, breakdown과 setback은 첨가물이 증가될수록 감소하였다. 들깨 식빵의 굽기 손실률과 비용적은 첨가량이 증가할수록 감소하였다. 색도는 L값과 b값은 첨가량이 증가할수록 감소하였고 a값은 증가하였다. Texture 측정 결과 경도는 첨가량이 증가할수록 증가하였고 응집성, 탄력성과 씹힘성은 감소하였다. 기호도 검사는 15% 첨가군이 색, 향, 맛, 외관, 질감이 가장 좋게 나타났으며 전체적인 기호도는 15% 첨가군이 가장 좋게 나타났다.

• 한국지역사회생활과학회지
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• 제17권2호
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• pp.61-68
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• 2006

This Study was conducted to investigate the processing quality of high-amylose content rice(goami) flour for noodle. The potassium and magnesium contents of rice flour were negatively associated with gross score of noodle making mixed with wheat flour. The high-amylose content of rice flour was closed associated with gel consistency negatively and with hardness of rice noodle positively, Setback viscosity of rice flour measured in a rapid visco-analyser(RVA) was significantly affected by amylose content as well as gel consistency. Also the amylose content decreased, the amylogram pasting temperature and the breakdown ratio increased. The low-amylose content rice(Chucheong) flour showed higher values in solubility. Cooking quality and texture were measured, and sensory evaluation was performed with the noodles prepared. Texture measurement showed that the noodles of composite flour containing 40% goami rice flour were superior to those wheat flour alone. Water binding capacity of the composite flour containing 40% goami rice flour was lower than that of 40% chucheong rice flour. In sensory evaluation, chewiness, overall acceptability of noodle with 40% goami ricer was evaluated as the best.

• Journal of Applied Biological Chemistry
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• 제50권4호
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• pp.234-238
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• 2007

The effects of ultra-fine pulverization on the physicochemical properties of rice starch (RS) were investigated using a high impact planetary mill. After pulverization, RVA characteristics, peak viscosity, break down, and set back values of RS decreased from 274.75 to 9.42 RVU, 214.46 to 6.17 RVU, and 87.80 to 17.00 RVU, respectively. The pasting properties also changed significantly. X-Ray diffractogram revealed RS had four A-type peaks, which disappeared after pulverization. The peak temperature and gelatinization enthalpy of RS using differential scanning calorimetry (DSC) were 13.99 J/g at $75.14^{\circ}C$, whereas the pulverized RS (PRS) had two peaks, 0.13 J/g at $63.88^{\circ}C$ and 1.23 J/g at $101.24^{\circ}C$. DSC measurement showed the retrogradation degree of PRS was lower than that of RS after storage at 4 and $25^{\circ}C$. The enzymatic (${\alpha}$-amylase) digestibilities of RS and PRS were 72.7 and 77.3%, respectively.

• ETRI Journal
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• 제35권4호
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• pp.625-631
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• 2013

For the formation of solder bumps with a fine pitch of 130 ${\mu}m$ on a printed circuit board substrate, low-volume solder on pad (LVSoP) technology using a maskless method is developed for SAC305 solder with a high melting temperature of $220^{\circ}C$. The solder bump maker (SBM) paste and its process are quantitatively optimized to obtain a uniform solder bump height, which is almost equal to the height of the solder resist. For an understanding of chemorheological phenomena of SBM paste, differential scanning calorimetry, viscosity measurement, and physical flowing of SBM paste are precisely characterized and observed during LVSoP processing. The average height of the solder bumps and their maximum and minimum values are 14.7 ${\mu}m$, 18.3 ${\mu}m$, and 12.0 ${\mu}m$, respectively. It is expected that maskless LVSoP technology can be effectively used for a fine-pitch interconnection of a Cu pillar in the semiconductor packaging field.

• 한국재난정보학회 논문집
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• 제9권1호
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• pp.56-64
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• 2013

본 연구에서는 소입경 골재와 중온 기술을 사용한 저소음 포장의 현장 적용성 검토를 수행하였다. 배합설계 및 실내실험 수행결과, 소입경 골재를 사용하면 골재간의 맞물림 면적이 증가하여 비산저항성이 향상되는 것으로 나타났다. 고점도 아스팔트 바인더를 사용하는 저소음 아스팔트 포장은 선회다짐기를 통한 다짐온도 결정이 적합하였으며, 중온 첨가제 사용시 약 $15^{\circ}C$의 다짐온도 저감효과를 얻을 수 있었다. 시험 시공 후 현장투수시험과 소음측정을 하였으며 현장투수시험을 통해 저소음 포장이 충분한 공극을 확보하였음을 확인하였다. 소음측정결과 10mm 소입경 저소음 포장의 소음감소효과가 가장 뛰어난 것으로 나타났으며 공극률이 다소 작게 확보된 10mm 중온 소입경 저소음 포장도 13mm 저소음 포장에 비해 높은 소음감소효과가 나타나 소입경 골재의 사용이 저소음 포장의 소음감소에 효과적이었으며, 특히 저속에서의 소음감소효과가 뛰어났다.