• 제목/요약/키워드: High-pressure experiment

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세라믹 축전물질들의 미량성분 분석방법 (Analytical method of trace elements in ceramic capacitor materials)

  • 최종금;김태현;임흥빈
    • 분석과학
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    • 제10권1호
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    • pp.35-42
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    • 1997
  • Barium titanate 및 PZT와 같은 세라믹 축전물질의 분석을 위해 고압 산분해법을 이용한 시료 전처리 기술을 연구하였다. 질산이나 증류수를 첨가하고 염산의 농도를 변화시키면서, 이들 시료의 정량분석을 유도결합 플라즈마 방출분광법에 의해 수행하였다. 분석 결과를 보면 Ba, Mn, Zn, Si 등 대부분의 원소들은 염산의 농도에 영향을 받지 않으나, Nb와 Zr은 이에 민감한 것으로 밝혀졌다. 그러나 분해시간은 상대적으로 분석 결과에 거의 영향을 미치지 않았다. Nb의 경우에는 가장 좋은 분석 결과를 얻기 위해 염산과 증류수의 비가 3:1(v / v) 보다는 더 진해야 함을 알았다. 또한 Pb의 분석에 있어서 염산과 질산의 혼산을 사용하는 경우보다 붉은 염산만을 사용하였을 경우에 더 좋은 분석 결과를 나타내었다.

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직접모사법을 이용한 극음속 대기 유동과 측면 제트의 상호 작용 해석 (Analysis of the Interaction Between Hypersonic Free Stream and Side Jet Flow Using a DSMC Method)

  • 김민규;권오준
    • 한국항공우주학회지
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    • 제33권3호
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    • pp.1-9
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    • 2005
  • 본 논문에서는 직접모사법을 이용하여 고 고도 희박 영역에서 로켓의 자세 제어에 필수적인 측면 제트 분사와 그에 따른 자유 흐름 유동과 측면 제트의 상호 작용에 대한 연구를 수행하였다. 밀도 차가 큰 자유 흐름 유동과 제트 유동을 동시에 모사하기 위해 입자 가중치 기법을 사용하였다. 두 수직한 평판 사이의 유동 및 측면 제트 분사에 의한 상호 작용 해석을 수행하였고 그 결과를 실험치와 비교하여 프로그램을 검증하였다. 좀 더 실제적인 로켓 모델로 blunted cone cylinder 형상에 대하여 받음각을 변화시켜가며 자유 흐름 유동과 측면 제트의 상호 작용에 대한 연구를 수행하였다. 표면 압력 차이의 분포를 기준으로 람다(lambda) 충격파와 후류의 영향을 토의하였다. 받음각이 있는 유동의 경우 leeward 방향으로는 제트와 자유 흐름 유동의 상호 작용이 약해지며, windward 방향으로는 상호 작용이 매우 강해지는 것을 확인할 수 있었다.

포식압력 하에 치어 보호 구조물이 피식자의 생존율에 미치는 영향에 관한 실험적 연구 (Experimental Study on Effect on Prey Survival by Juvenile Fish Shelter (JFS) under Pressure by Piscivorous Fishes)

  • 안창혁;주진철;이새로미;안호상;박재로;송호면
    • 한국물환경학회지
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    • 제29권6호
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    • pp.746-753
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    • 2013
  • The aim of this study was to evaluate artificial fish shelter, which was known to increase prey survival and expand habitat space to improve species diversity and fish communities in a freshwater ecosystem. The experiment was performed at an outdoor test-bed for three months from 2011 by comparing the responses to adjustments in the volume of the artificial patch (juvenile fish shelter, JFS) in the control and experimental groups. Analysis of the environmental conditions over two periods (Period1 ~ 2) showed minor differences in the physichemical characteristics of water quality, phytoplankton, and zooplankton biomass, thus, allowing comparative analysis of feeding ecology. However, high water temperature conditions in Period1 ($25.6{\pm}2.0^{\circ}C$), affected the predation activity of the piscivorous fishes, Coreoperca herzi (C. herzi, size $89{\pm}4mm$). Survival rates of the prey fishes, Rhynchocypris oxycephalus (R. oxycephalus, size $29{\pm}1mm$), improved as the patch volume increased and were higher than those of the control group by 35.9 ~ 46.7%. Analysis showed that JFS reduced the chances of predator-prey encounter, and thereby minimized prey vulnerability.

불응축가스량이 가변전열 히트파이프의 열수송 특성에 미치는 영향 (Influence of NCG Charging Mass on the Heat Transport Capacity of Variable Conductance Heat Pipe)

  • 서정세;박영식;정경택
    • 설비공학논문집
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    • 제18권4호
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    • pp.320-327
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    • 2006
  • Numerical analysis and experimental study are performed to investigate the effect of heat load and operating temperature on the thermal performance of several variable conductance heat pipe (VCHP) with screen meshed wick. The heat pipe is designed in 200 screen meshes, 500 mm length and 12.7 mm outer diameter tube of copper, water (4.8 g) is used as working fluid and nitrogen as non-condensible gas (NCG). Heat pipe used in this study has evaporator, condenser and adiabatic section, respectively. Analysis values and experimental data of wall temperature distribution along axial length are presented for heat transport capacity, condenser cooling water temperature change, degrees of an inclination angle and operating temperature. These analysis and experiment give the follow findings: For the same charging mass of working fluid, the operating temperature of heat pipe becomes to be high with the increasing of charging mass of NCG. When the heat flux at the evaporator section increases, the vapor pressure in the pipe rises and consequently compresses the NCG to the condenser end part and increases the active length of the condenser. From previous process, it is found out we can control the operating temperature effectively and also the analysis and experimental results are relatively coincided well.

Preliminary numerical study on hydrogen distribution characteristics in the process that flow regime transits from jet to buoyancy plume in time and space

  • Wang, Di;Tong, Lili;Liu, Luguo;Cao, Xuewu;Zou, Zhiqiang;Wu, Lingjun;Jiang, Xiaowei
    • Nuclear Engineering and Technology
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    • 제51권6호
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    • pp.1514-1524
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    • 2019
  • Hydrogen-steam gas mixture may be injected into containment with flow regime varying both spatially and transiently due to wall effect and pressure difference between primary loop and containment in severe accidents induced by loss of coolant accident. Preliminary CFD analysis is conducted to gain information about the helium flow regime transition process from jet to buoyancy plume for forthcoming experimental study. Physical models of impinging jet and wall condensation are validated using separated effect experimental data, firstly. Then helium transportation is analyzed with the effect of jet momentum, buoyancy and wall cooling discussed. Result shows that helium distribution is totally dominated by impinging jet in the beginning, high concentration appears near gas source and wall where jet momentum is strong. With the jet weakening, stable light gas layer without recirculating eddy is established by buoyancy. Transient reversed helium distribution appears due to natural convection resulted from wall cooling, which delays the stratification. It is necessary to concern about hydrogen accumulation in lower space under the containment external cooling strategy. From the perspective of experiment design, measurement point should be set at the height of connecting pipe and near the wall for stratification stability criterion and impinging jet modelling validation.

전기화학 에칭 공정을 이용한 스테인리스 스틸 메쉬의 방수 특성 연구 (A Study on Water-Proof Characteristics of a Stainless Steel Mesh by Electrochemical Etching Process)

  • 이찬;김지민;김형모
    • Tribology and Lubricants
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    • 제37권5호
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    • pp.189-194
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    • 2021
  • A straightforward, yet effective surface modification method of stainless steel mesh and its interesting anti-wetting characteristics are reported in this study. The stainless steel mesh is electrochemically etched, and the specimen has both micro and nano-scale structures on its surface. This process transforms the two types of mesh specimens known as the regular and dense specimens into hydrophobic specimens without applying any hydrophobic chemical coating process. The fundamental wettability of the modified mesh is analyzed through a dedicatedly designed experiment to investigate the waterproof characteristics, for instance, the penetration threshold. The waterproof characteristics are evaluated in a manner that the modified mesh resists as high as approximately 2.7 times the pressure compared with the bare mesh, i.e., the non-modified mesh. The results show that the penetration threshold depends primarily on the advancing contact angles, and the penetration stop behaviors are affected by the contact angle hysteresis on the surfaces. The findings further confirm that the inexpensive waterproof meshes created using the proposed straightforward electrochemical etching process are effective and can be adapted along with appropriate designs for various practical applications, such as underwater devices, passive valves, and transducers. In general, , additional chemical coatings are applied using hydrophobic materials on the surfaces for the applications that require water-repelling capabilities. Although these chemical coatings can often cause aging, the process proposed in this study is not only cost-effective, but also durable implying that it does not lose its waterproof properties over time.

고온 압축 공정에서 금형과 알루미늄 빌렛의 접촉 열전달 계수 도출에 관한 연구 (A Study on Derivation of Contact Heat Transfer Coefficient Between Die and Aluminum Billet in High Temperature Compression Process)

  • 전효원;서창희;오상균;권태하;강경필;육형섭
    • 소성∙가공
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    • 제30권3호
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    • pp.142-148
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    • 2021
  • In hot forging analysis, the interfacial heat transfer coefficient (IHTC) is a very important factor defining the heat flow between the die and the material. In particular, in the hot forging analysis of aluminum 6xxx series alloy, which are used in automobile parts, differences in load and microstructure occur due to changes in surface temperature according to the IHTC. This IHTC is not a constant value but changes depends on pressure. This study derived the IHTC under low load using aluminum 6082 alloy. An experiment was performed by fabricating a compression die, and a heat transfer analysis was performed based on the experimental data. The heat transfer analysis used DEFORM-2D, a commercial finite element analysis program. To derive the IHTC, heat transfer analysis was performed for the IHTC in the range of 10 to 50 kW/m2℃ at intervals of 10kW/m2℃. The heat transfer analysis results according to the IHTC and the actual experimental values were compared to derive the IHTC of the aluminum 6082 alloy under low load.

Ga2O3초음파분무화학기상증착 공정에서 유동해석을 이용한 균일도 향상 연구 (Computational Fluid Dynamics for Enhanced Uniformity of Mist-CVD Ga2O3 Thin Film)

  • 하주환;이학지;박소담;신석윤;변창우
    • 반도체디스플레이기술학회지
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    • 제21권4호
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    • pp.81-85
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    • 2022
  • Mist-CVD is known to have advantages of low cost and high productivity method since the precursor solution is misting with an ultrasonic generator and reacted on the substrate under vacuum-free conditions of atmospheric pressure. However, since the deposition distribution is not uniform, various efforts have been made to derive optimal conditions by changing the angle of the substrate and the position of the outlet to improve the result of the preceding study. Therefore, in this study, a deposition distribution uniformity model was derived through the shape and position of the substrate support and the conditions of inlet flow rate using the particle tracking method of computational fluid dynamics (CFD). The results of analysis were compared with the previous studies through experiment. It was confirmed that the rate of deposition area was improved from 38.7% to 100%, and the rate of deposition uniformity was 79.07% which was higher than the predicted result of simulation. Particle tracking method can reduce trial and error in experiments and can be considered as a reliable prediction method.

VHF-CCP 설비에서 Ar/SF6 플라즈마 분포가 Si 식각 균일도에 미치는 영향 분석 (Analysis of Si Etch Uniformity of Very High Frequency Driven - Capacitively Coupled Ar/SF6 Plasmas)

  • 임성재;이인규;이하늘;손성현;김곤호
    • 반도체디스플레이기술학회지
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    • 제20권4호
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    • pp.72-77
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    • 2021
  • The radial distribution of etch rate was analyzed using the ion energy flux model in VHF-CCP. In order to exclude the effects of polymer passivation and F radical depletion on the etching. The experiment was performed in Ar/SF6 plasma with an SF6 molar ratio of 80% of operating pressure 10 and 20 mTorr. The radial distribution of Ar/SF6 plasma was diagnosed with RF compensated Langmuir Probe(cLP) and Retarding Field Energy Analyzer(RFEA). The radial distribution of ion energy flux was calculated with Bohm current times the sheath voltage which is determined by the potential difference between the plasma space potential (measured by cLP) and the surface floating potential (by RFEA). To analyze the etch rate uniformity, Si coupon samples were etched under the same condition. The ion energy flux and the etch rate show a close correlation of more than 0.94 of R2 value. It means that the etch rate distribution is explained by the ion energy flux.

바이오매스 합성가스 적용을 위한 LPG 엔진발전기 개조 및 성능평가 (Modification of an LPG Engine Generator for Biomass Syngas Application)

  • 엘리에젤 하비네자;홍성구
    • 한국농공학회논문집
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    • 제64권5호
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    • pp.9-16
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    • 2022
  • Syngas, also known as synthesis gas, synthetic gas, or producer gas, is a combustible gas mixture generated when organic material (biomass) is heated in a gasifier with a limited airflow at a high temperature and elevated pressure. The present research was aimed at modifying the existing LPG engine generator for fully operated syngas. During this study, the designed gasifier-powered woodchip biomass was used for syngas production to generate power. A 6.0 kW LPG engine generator was modified and tested for operation on syngas. In the experiments, syngas and LPG fuels were tested as test fuels. For syngas production, 3 kg of dry woodchips were fed and burnt into the designed downdraft gasifier. The gasifier was connected to a blower coupled with a slider to help the air supply and control the ignition. The convection cooling system was connected to the syngas flow pipe for cooling the hot produce gas and filtering the impurities. For engine modification, a customized T-shaped flexible air/fuel mixture control device was designed for adjusting the correct stoichiometric air-fuel ratio ranging between 1:1.1 and 1.3 to match the combustion needs of the engine. The composition of produced syngas was analyzed using a gas analyzer and its composition was; 13~15 %, 10.2~13 %, 4.1~4.5 %, and 11.9~14.6 % for CO, H2, CH4, and CO2 respectively with a heating value range of 4.12~5.01 MJ/Nm3. The maximum peak power output generated from syngas and LPG was recorded using a clamp-on power meter and found to be 3,689 watts and 5,001 watts, respectively. The results found from the experiment show that the LPG engine generator operated on syngas can be adopted with a de-ration rate of 73.78 % compared to its regular operating fuel.