• Title/Summary/Keyword: High Pressure Extraction

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Polyphenolic Compounds, Physiological Activities, and Digestive Enzyme Inhibitory Effect of Aster scaber Thunb. Extracts According to Different Extraction Processes (추출방법에 따른 참취(Aster scaber Thunb.)의 페놀화합물 함량과 생리활성 및 소화효소 저해 효과)

  • Kim, Jae-Won;Youn, Kwang-Sup
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.43 no.11
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    • pp.1701-1708
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    • 2014
  • Phenolic compounds, physiological properties, and digestive enzyme inhibitory effect of 70% ethanol extracts from Aster scaber with different extraction methods (stirrer extraction, SE; reflux extraction, RE; autoclave extraction, AE; low temperature high pressure extraction, LTPE; ultrasonification extraction, USE) were investigated. Total polyphenols and flavonoids contents in LTPE were significantly higher than those of other extracts. The amount of substances related to cynarin (1,3-O-dicaffeoylquinic acid) was highest in USE (34.34 mg/g), followed by LTPE (33.83 mg/g), RE (32.27 mg/g), AE (25.40 mg/g), and SE (18.17 mg/g). Chlorogenic acid (5-O-caffeoylquinic acid) and astragalin (kaempferol-3-O-glucopyranoside) were highest in AE and LTPE, respectively. Xanthine oxidase, angiotensin- I converting enzyme, 3-hydroxy-3-methylglutaryl coenzyme A reductase and acetylcholin esterase inhibitory activities of LTPE and USE at a concentration of 50 mg% (w/v) were somewhat higher than those of other extracts. The ${\alpha}$-amylase, ${\alpha}$-glucosidase, trypsin and lipase activities showed the same tendency as physiological properties (concentration of 500 mg%, w/v). Additionally, there was significantly higher or slightly lower inhibitory activity compared to the control group. These results suggest that extracts from Aster scaber have potential to act as functional materials, and LTPE and USE are superior for the enhancement of biological activity.

Antioxidant and digestive enzyme inhibitory effects of Eisenia bicyclis extracted by different methods (추출방법에 따른 대황 추출물의 항산화 및 소화효소 저해 효과)

  • Kim, Jin-Hak;Park, La Young;Lee, Shin-Ho
    • Food Science and Preservation
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    • v.23 no.1
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    • pp.97-103
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    • 2016
  • The antioxidant and digestive enzyme inhibitory effects of Eisenia bicyclis extracted by various extraction methods (RE, reflux extraction; SE, ultrasonification extraction; AE, autoclave extraction; LE, low-temperature high-pressure extraction) were investigated. The extraction yield (55.21%) and the laminarin (39.03%), fucoidan (24.75%), total polyphenol (115.68 mg GAE/g) and flavonoid (36.67 mg RHE/g) contents of AE were higher than those in other methods. The DPPH radical (86.60%, 500 mg%), ABTS radical (58.56%, 25 mg%), nitrite (86.38%, 100 mg%) scavenging activities of the Eisenia bicyclis extracted by AE were higher than those of Eisenia bicyclis extracted by other methods. The ABTS radical and nitrite scavenging activities were above 98% in all tested Eisenia bicyclis extracts and these activities were dependent on its concentration. The inhibitory effects of AE against amylase (50 mg%) and ${\alpha}$-glucosidase (5 mg%) were 64.76% and 86.71%, respectively. The AE showed the best inhibitory effect of Eisenia bicyclis extracts (50 mg%) against trypsin (24.37%) and ${\alpha}$-chymotrypsin (49.05%), respectively. These results suggest that Eisenia bicyclis extracted by AE can be used as a bioactive and functional material in the food industry.

Influence of complex geological structure on horizontal well productivity of coalbed methane

  • Qin, Bing;Shi, Zhan-Shan;Sun, Wei-Ji;Liang, Bing;Hao, Jian-Feng
    • Geomechanics and Engineering
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    • v.29 no.2
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    • pp.145-154
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    • 2022
  • Complex geological conditions have a great influence on the mining of coalbed methane (CBM), which affects the extraction efficiency of CBM. This investigation analyzed the complicated geological conditions in the Liujia CBM block of Fuxin. A geological model of heterogeneities CBM reservoirs was established to study the influence of strike direction of igneous rocks and fault structures on horizontal well layout. Subsequently, the dual-porosity and dual-permeability mathematical model was established, which considers the dynamic changes of porosity and permeability caused by gas adsorption, desorption, pressure change. The results show that the production curve is in good agreement with the actual by considering gas seepage in matrix pores in the model. Complicated geological structures affect the pressure expansion of horizontal wells, especially, the closer to the fault structure, the more significant the effect, the slower the pressure drop, and the smaller the desorption area. When the wellbore extends to the fault, the pressure expansion is blocked by the fault and the productivity is reduced. In the study area, the optimal distance to the fault is 70 m. When the horizontal wellbore is perpendicular to the direction of coal seam igneous rock, the productivity is higher than that of parallel igneous rock, and the horizontal well bore should be perpendicular to the cleat direction. However, the well length is limited due to the dense distribution of igneous rocks in the Liujia CBM block. Therefore, the horizontal well pumping in the study area should be arranged along the direction of igneous rock and parallel plane cleats. It is found that the larger the area surrounded by igneous rock, the more favorable the productivity. In summary, the reasonable layout of horizontal wells should make full use of the advantages of igneous rock, faults and other complex geological conditions to achieve the goal of high and stable production.

Discharge Characteristics of Large-Area High-Power RF Ion Source for Neutral Beam Injector on Fusion Devices

  • Chang, Doo-Hee;Park, Min;Jeong, Seung Ho;Kim, Tae-Seong;Lee, Kwang Won;In, Sang Ryul
    • Proceedings of the Korean Vacuum Society Conference
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    • 2014.02a
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    • pp.241.1-241.1
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    • 2014
  • The large-area high-power radio-frequency (RF) driven ion sources based on the negative hydrogen (deuterium) ion beam extraction are the major components of neutral beam injection (NBI) systems in future large-scale fusion devices such as an ITER and DEMO. Positive hydrogen (deuterium) RF ion sources were the major components of the second NBI system on ASDEX-U tokamak. A test large-area high-power RF ion source (LAHP-RaFIS) has been developed for steady-state operation at the Korea Atomic Energy Research Institute (KAERI) to extract the positive ions, which can be used for the NBI heating and current drive systems in the present fusion devices, and to extract the negative ions for negative ion-based plasma heating and for future fusion devices such as a Fusion Neutron Source and Korea-DEMO. The test RF ion source consists of a driver region, including a helical antenna and a discharge chamber, and an expansion region. RF power can be transferred at up to 10 kW with a fixed frequency of 2 MHz through an optimized RF matching system. An actively water-cooled Faraday shield is located inside the driver region of the ion source for the stable and steady-state operations of RF discharge. The characteristics and uniformities of the plasma parameter in the RF ion source were measured at the lowest area of the expansion bucket using two RF-compensated electrostatic probes along the direction of the short- and long-dimensions of the expansion region. The plasma parameters in the expansion region were characterized by the variation of loaded RF power (voltage) and filling gas pressure.

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Investigation of Structural and Optical Properties of III-Nitride LED grown on Patterned Substrate by MOCVD (Patterned substrate을 이용하여 MOCVD법으로 성장된 고효율 질화물 반도체의 광특성 및 구조 분석)

  • Kim, Sun-Woon;Kim, Je-Won
    • Korean Journal of Materials Research
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    • v.15 no.10
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    • pp.626-631
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    • 2005
  • GaN-related compound semiconductors were grown on the corrugated interface substrate using a metalorganic chemical vapor deposition system to increase the optical power of white LEDs. The patterning of substrate for enhancing the extraction efficiency was processed using an inductively coupled plasma reactive ion etching system and the surface morphology of the etched sapphire wafer and that of the non-etched surface were investigated using an atomic force microscope. The structural and optical properties of GaN grown on the corrugated interface substrate were characterized by a high-resolution x-ray diffraction, transmission electron microscopy, atomic force microscope and photoluminescence. The roughness of the etched sapphire wafer was higher than that of the non-etched one. The surface of III-nitride films grown on the hemispherically patterned wafer showed the nano-sized pin-holes that were not grown partially. In this case, the leakage current of the LED chip at the reverse bias was abruptly increased. The reason is that the hemispherically patterned region doesn't have (0001) plane that is favor for GaN growth. The lateral growth of the GaN layer grown on (0001) plane located in between the patterns was enhanced by raising the growth temperature ana lowering the reactor pressure resulting in the smooth surface over the patterned region. The crystal quality of GaN on the patterned substrate was also similar with that of GaN on the conventional substrate and no defect was detected in the interface. The optical power of the LED on the patterned substrate was $14\%$ higher than that on the conventional substrate due to the increased extraction efficiency.

Analysis and Flight Test Verification of T/A-50 Engine Horsepower Extraction Capability (T/A-50 엔진 축마력(Horsepower) 능력 해석 및 비행시험 검증)

  • 이상효;이부일;정주현;이상백
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.34 no.7
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    • pp.105-111
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    • 2006
  • The aircraft engine is to generate thrust for the maneuver of aircraft and to provide the power to the related hydraulic system and electrical system. Since the power provided to the systems is extracted from the high pressure compressor of aircraft engine, the extracted power is called horsepower extraction (HPX). If the HPX provided from the engine is smaller than the HPX required from the related systems, there could be abnormal engine behavior, like engine rollback or stall. Analysis on comparing the required HPX and the engine HPX capability had been performed during the T/A-50 FSD (Full Scale Development) period. The analysis results make the engine schedule changed, and T/A-50 flight test has been performed with the changed engine schedule. The analysis results and changing the engine control schedule were verified to be valid with the flight test results.

Characterization of Polysaccharides Obtained from Purslane (Portulaca olerace L.) Using Different Solvents and Enzymes

  • Choi, Ae-Jin;Kim, Chul-Jin;Cho, Yong-Jin;Kim, Yang-Ha;Cha, Jae-Yoon;Hwang, Jae-Kwan;Kim, In-Hwan;Kim, Chong-Tai
    • Food Science and Biotechnology
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    • v.16 no.6
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    • pp.928-934
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    • 2007
  • Physiochemical properties, such as yield and molecular weight distribution of polysaccharide fractions, of polysaccharides in the enzymatic hydrolysates of purslane were investigated and characterized. A higher amount of micro nutrients, such as potassium (9,413 mg/100 g), phosphorus acid (539 mg/100 g), leucine, alanine, lysine, valine, glycine, and isoleucine, was present in whole purslane. The yield of water soluble polysaccharides (WSP) was 0.29, 7.01, and 7.94% when extracted using room temperature water (RTW), hot-water (HW), and hot temperature/high pressure-water (HTPW), respectively, indicating that HW or HTPW extraction may be effective to obtain WSP from purslane. The average ratio of L-arabinose:D-galactose in the WSP was 37:49, 34:37, and 27:29, when extracted using RTW, HW, and HTPW, respectively. These results indicate that water was a suitable extraction solvent for preparation of the arabinogalactan component of whole purslane. A higher yield and total carbohydrate content was obtained by using Viscozyme L instead of Pectinex 5XL during extraction of the WSP, which indicates that enzymatic treatment of purslane may be an effective method to control the Mw of polysaccharides. Finally, it was confirmed that Viscozyme L is a suitable enzyme for the hydrolysis and separation of polysaccharides obtained from purslane.

Extraction of EPA and DHA from Tuna Oil Using Supercritical Carbon Dioxide (초임계 이산화탄소를 이용한 참치유에서의 EPA 및 DHA 추출)

  • Yoon, Jung-Ro
    • Korean Journal of Food Science and Technology
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    • v.25 no.3
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    • pp.288-294
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    • 1993
  • Solubilities of urea-crystallized tuna oil methyl esters in supercritical carbon dioxide were determined by a flow through extraction reactor. Experimental results obtained under a quasi-equlibrium condition showed that at 150 bar, solubilities of the esters in supercritical $CO_2$ were 0.075, 0.028 and 0.006(w/w) at $40^{\circ}C,\;60^{\circ}C\;and\;80^{\circ}C$, respectively. In the pressure and temperature ranges $(100{\sim}200bar\;and\;40{\sim}80^{\circ}C)$, the solubility increased with the density of $CO_2$. However, selectivity of supercritical carbon dioxide on the extracted compounds was much better at low density than at high density. Supercritical fractionation with a temperature gradient $(50{\sim}75^{\circ}C)$ resulted in concentrates of EPA and DHA in purities of 12% and 85%, respectively.

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Antioxidant activities of phenolic compounds from Angelica gigas Nakai extract using subcritical water (아임계수 추출 기술을 이용한 당귀 추출물의 유효성분 및 산화방지 평가)

  • Ko, Min-Jung;Lee, Jeong-Hyun;Nam, Hwa-Hyun;Chung, Myong-Soo
    • Korean Journal of Food Science and Technology
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    • v.49 no.1
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    • pp.44-49
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    • 2017
  • Subcritical water extraction can be used to selectively extraction compounds by varying the temperature-dependent dielectric constant of water. This study investigated subcritical water extraction of decursin and nodakenin yields from Angelica gigas Nakai (AN) quantitatively and qualitatively by HPLC, and HPLC-ESI/MS. Total phenolics, total flavonoid contents, and antioxidant activity were determined by DPPH and ABTS radical scavenging activity, including the effects of varying the extraction conditions of temperature ($110-200^{\circ}C$) and time (1-20 min) under high pressure (10 MPa). By subcritical water extraction under operating conditions of $120-130^{\circ}C$, the maximum yields of decursin ($6.64{\pm}0.42%$ in the dried material) and nodakenin ($3.71{\pm}0.28%$ in the dried material) were obtained. From $190-200^{\circ}C$ the maximum yields of total phenolics ($75.97{\pm}1.64mg$ gallic acid equivalent/g AN), flavonoids ($8.56{\pm}1.10mg$ quercetin equivalent/g AN), DPPH ($63.07{\pm}1.71%$), and ABTS ($72.32{\pm}2.82%$) were obtained.

A Comparison of Volatile Compounds in Pine Extracts Obtained by Supercritical Fluid Extraction with Those by Simultaneous Steam Distillation and Solvent Extraction (초임계유체 추출과 SDE에 의한 솔 추출물의 휘발성분 비교)

  • Woo, Gaung-Yaul;Kim, Kong-Hwan;Lee, Mi-Jung;Lee, Yang-Bong;Yoon, Jung-Ro
    • Korean Journal of Food Science and Technology
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    • v.31 no.5
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    • pp.1268-1274
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    • 1999
  • Pine twigs with buds were cut into $2{\sim}3\;mm$ long pieces and about 18g was used for each experiment. Pressure and temperature ranges employed were $100{\sim}300\;bar$ and $35{\sim}55^{\circ}C$, respectively. Volatile compounds of extracts were isolated and identified by gas chromatography and mass selective detector. Twenty three compounds from the extracts were identified. Limonene and ${\beta}-pinene$ were found to be the major components with $32.6{\sim}43.4%$ being limonene. Extracts obtained by supercritical fluid extraction were lower in monoterpene and higher in oxygenated terpenoids than those by steam distillation and solvent extraction (SDE). Sensory evaluation showed that the pine flavor extracted using supercritical carbon dioxide was much better in quality than that of SDE. In conclusion, it was found out that supercritical fluid extraction can successfully be applied to extract high quality flavor from pine.

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