• 한국산학기술학회논문지
• /
• 제11권1호
• /
• pp.49-54
• /
• 2010

자동차의 A.C 제너레이터(alternating current generator) 부품으로 사용되는 로터폴(rotor pole)을 가공할 때는 트랜스퍼온간단조금형(transfer warm forging die)으로 성형한다. 소재를 온간가공 영역으로 가열한 후 즉시 금형안으로 이송시켜 제1스테이지(1st stage)에서 업세팅가공(upsetting work)하고 제2스테이지(2nd stage)로 이송하여 측방압출(lateral extrusion)가공을 한다. 이때 측방압출 스테이지의 금형에서 다이블록(die block), 다이부싱(die bushing), 센터펀치(center punch), 사이드펀치(side punch)의 접촉면이 압출시의 과혹(過酷)한 조건에 견디지 못하여 쉽게 마멸(abrasion)되어 금형수명(die life)을 단축시키고 있다. 이 때문에 생산량 감소로 인한 납기지연, 금형의 수리보수시간 과다, 제품의 정밀도 저하 등의 문제점이 발생되고 있다. 이러한 문제점을 해결하기 위하여 금형재질 선정과 열처리 작업 싸이클 개선, 방전가공시의 트러블 해소, 핵심부품의 구조변경 등을 연구하여 금형수명을 40~50% 연장 하고자 하였다.

• 한국환경보건학회지
• /
• 제32권1호
• /
• pp.67-70
• /
• 2006

A gas chromatography/mass spectrometric method was developed for the determination of formaldehyde in hair. 0.3mg of hair was placed in 10ml headspace vial. 1.5mM pentafluorophenylhydrazine solution (pH 2) in 0.03 M phosphoric acid and $20\;{\mu}l$ of 500 mg/l $acetone-d_6$ as internal standard were added in vial and sealed tightly with cap. The solution was heated for 30 min at $90^{\circ}C$ in heating block. The extraction, the derivatization and the evaporation were performed simultaneously. After heating of the solution, 0.5 ml of headspace was taken up and analyzed by gas chromatography-mass spectrometry (GC-MS). Low limit of detection (LaD) and Low limit of quantitation (LOQ) of formaldehyde were 0.5 and 1.5 ng/g, respectively. The method was used to analyze formaldehyde in rat hair after oral exposure. The developed method may be valuable to be used to analyze formaldehyde in human hair.

• 대한임상검사과학회지
• /
• 제40권2호
• /
• pp.113-117
• /
• 2008

It designed a study to examine the efficiency of DNA and RNA extraction from archival formalin-fixed, paraffin-embedded tissues using an non-heating and heating method. Archival paraffin blocks of liver, kidney, colon were randomly selected. Each paraffin block was prepared in 20 microtubes. For each paraffin blocks were tested non-heating DNA extraction to 10 microtubes and heating protocol under pH 7.0 and $100^{\circ}C$ to 10 microtubes. Evaluation of the results of DNA extraction was carried out by measuring concentration by UV spectrophotometry and then PCR amplification. DNA extraction content that non-heating method was liver $5{\pm}0.7{\mu}g/mL$, kidney $2{\pm}0.3{\mu}g/mL$, colon $6{\pm}0.4{\mu}g/mL$ and heating method was liver $12{\pm}0.6{\mu}g/mL$, kidney $7{\pm}0.5{\mu}g/mL$, colon $10.{\pm}0.3{\mu}g/mL$. Successful RNA extraction was observed, by ${\beta}$-actin amplification, in 46.7% sections for samples treated by the heating method versus 30.0% using non-heating DNA extraction. The extracted nucleic acid showed better values for samples heated at $100^{\circ}C$. Therefore heating extraction of nucleic acid is reliable, quick and efficiency.

• 대한기계학회논문집B
• /
• 제25권9호
• /
• pp.1237-1244
• /
• 2001

An experimental study was carried out to identify the various regimes of natural convective pool boiling and to determine the boiling heat transfer curve and Critical Heat Flux(CHF) on a vertical square surface having a 70mm width and a 70mm height. The heater made of copper block with embedded cartridge heaters is submerged in a water tank at atmospheric pressure. As the heat flux increases from 100kW/㎡ to 1.2MW/㎡, the heat transfer regime migrates from the nucleate boiling to the film boiling. The boiling heat transfer data are fitted by Rohsenow type correlation. An explosive vapor generation on the heated surface, whose size and frequency are characterized by the heat flux, is visualized using a high speed digital imaging system.

• Journal of Welding and Joining
• /
• 제29권4호
• /
• pp.48-53
• /
• 2011

A thermal distortion analysis which takes strains directly as boundary conditions removed barrier of analysis time for the evaluation of welding distortion in a large shell structure like ship block. If the FE analysis time is dramatically reduced, the structure modeling time or the input-value calculating time will become a new issue. On the contrary to this, if the calculation time of analysis input-value is dramatically reduced and its results also are more meaningful, a little longer analysis time could be affirmative. In this study, instead of using inherent strain based on elastic analysis, a thermal strain based on elasto-plastic analysis is used as the boundary condition of weldments in order to evaluate the welding distortion. Here, the thermal strain at the weldment was established by using a stress-strain curve established from the test results. It is possible to automatically recognize the modeling induced-stiffness in the shrinkage direction of welded or heated region. The validity of elasto-plastic thermal distortion analysis was verified through the experiment results with various welding sequence.

• 농업생명과학연구
• /
• 제46권1호
• /
• pp.29-34
• /
• 2012

소나무 톱밥보드로 제조된 우드세라믹에 전선을 연결하여 목재 틀과 콘크리트 블록 속에 넣고 통전하여 강화마루판과 합판마루판의 표면온도 상승과 하강변화를 조사 하여 우드세라믹을 온돌마루판 하부소재로 이용할수 있는 가능성을 검토하였다. 통전시간 60분 후 마루판의 표면온도와 처음 시작온도 차이는 강화마루판이 크게 나타나 합판마루판보다 열전달이 빠름을 알 수 있었다. 목재 틀에서 우드세라믹 표면설정온도가 $70^{\circ}C$와 $80^{\circ}C$일 때 60분 후 강화마루판의 표면온도는 각각 $37.8^{\circ}C$와 $39.4^{\circ}C$로 높게 나타나 열전달이 우수하였다. 각 우드세라믹 표면설정온도별 처음 시작온도와 30분후의 표면온도 하강차이는 목재 틀이 콘크리트 블록보다, 강화마루판이 합판마루판보다 커서 온도하강이 빠름을 알 수 있었다. 우드세라믹 자체의 표면온도 하강은 목재 틀보다 콘크리트 블럭에서 하강속도가 빨랐으며, 마루판의 하강속도가 우드세라믹의 하강속도보다 느려 마루판이 오랜 시간 열을 유지하고 있음을 알 수 있었다.

• 한국재료학회지
• /
• 제10권6호
• /
• pp.409-414
• /
• 2000

3%C-10%Cr-5%Mo-5%W, 3%C-10%V-5%Mo-5%W 및 3%C-17%Cr-3%V의 3종류 고합금백주철에 있어서 열처리후의 기지조직의 변태거동을 연구하였다. 15kg 용량의 고주파 유도용해로에 선철, 고철, Fe-Cr, Fe-V, Fe-Mo 및 Fe-W 등을 장입시켜 용해시킨 후 슬래그를 제거시키고 $1550^{\circ}C$에서 Y-block의 펩 주형에 주입시켰다. 적당한 크기로 절단한 시편을 진공분위기하에$950^{\circ}C$에서 5시간동안 우선 균질화처리를 실시하였다. 그 후 다시 이 시편을 $1050^{\circ}C$에서 2시간동안 오스테나이징시킨 후 강제공냉을 행하였다. 강제공냉된 시편을 $300^{\circ}C$에서 3시간 유지시킨 후 템퍼링을 실시하였다. 주방상태에서의 기지조직은 3합금 공히 퍼얼라이트이었으며 강제공냉후에는 마르텐사이트 및 오스테나이트로 변태하였다. 또한 기지조직내에 무수히 많은 이차탄화물 입자들의 석출되었다. 템프링 후 일부 오스테나이트 및 마르텐사이트는 템퍼드마르텐사이트로 변태하였다. 변태하였다.

• Mycobiology
• /
• 제46권2호
• /
• pp.138-146
• /
• 2018

Two-hundred and fifty-five strains of actinomycetes isolated from soil samples were screened for their antagonistic activities against four well-known wood decay fungi (WDF), including a brown rot fungus, Gloeophyllum trabeum and three white rot fungi Donkioporia expansa, Trametes versicolor, and Schizophyllum commune. A dual culture assay using culture media supplemented with heated or unheated culture filtrates of selected bacterial strains was used for the detection of their antimicrobial activity against four WDF. It was shown that Streptomyces atratus, S. tsukiyonensis, and Streptomyces sp. greatly inhibited the mycelial growth of the WDF tested compared with the control. To evaluate the biocontrol efficacy of S. atratus, S. tsukiyonensis, and Streptomyces sp., wood blocks of Pinus densiflora inoculated with three selected Streptomyces isolates were tested for weight loss, compression strength (perpendicular or parallel to the grain), bending strength, and chemical component changes. Of these three isolates used, Streptomyces sp. exhibited higher inhibitory activity against WDF, especially G. trabeum, as observed in mechanical and chemical change analyses. Scanning electron microscopy showed that cell walls of the wood block treated with Streptomyces strains were thicker and collapsed to a lesser extent than those of the non-treated control. Taken together, our findings indicate that Streptomyces sp. exhibits the potential to be used as a biocontrol agent for wood decay brown rot fungus that causes severe damage to coniferous woods.

• 한국전기전자재료학회논문지
• /
• 제21권12호
• /
• pp.1135-1140
• /
• 2008

Bismuth-telluride based thin film materials are grown by Metal Organic Chemical Vapor Deposition(MOCVD). A planar type thermoelectric device has been fabricated using p-type $Bi_{0.4}Sb_{1.6}Te_3$ and n-type $Bi_2Te_3$ thin films. Firstly, the p-type thermoelectric element was patterned after growth of $4{\mu}m$ thickness of $Bi_{0.4}Sb_{1.6}Te_3$ layer. Again n-type $Bi_2Te_3$ film was grown onto the patterned p-type thermoelectric film and n-type strips are formed by using selective chemical etchant for $Bi_2Te_3$. The top electrical connector was formed by thermally deposited metal film. The generator consists of 20 pairs of p- and n-type legs. We demonstrate complex structures of different conduction types of thermoelectric element on same substrate by two separate runs of MOCVD with etch-stop layer and selective etchant for n-type thermoelectric material. Device performance was evaluated on a number of thermoelectric devices. To demonstrate power generation, one side of the sample was heated by heating block and the voltage output measured. As expected for a thermoelectric generator, the voltage decreases linearly, while the power output rises to a maximum. The highest estimated power of $1.3{\mu}W$ is obtained for the temperature difference of 45 K. we provide a promising procedure for fabricating thin film thermoelectric generators by using MOCVD grown thermoelectric materials which may have nanostructure with high thermoelectric properties.

• 한국전기전자재료학회:학술대회논문집
• /
• 한국전기전자재료학회 2008년도 추계학술대회 논문집 Vol.21
• /
• pp.425-425
• /
• 2008

Bismuth-antimony-telluride based thermoelectric thin film materials were prepared by metal organic vapor phase deposition using trimethylbismuth, triethylantimony and diisopropyltelluride as metal organic sources. A planar type thermoelectric device has been fabricated using p-type $Bi_{0.4}Sb_{1.6}Te_3$ and n-type $Bi_2Te_3$ thin films. Firstly, the p-type thermoelectric element was patterned after growth of $4{\mu}m$ thickness of $Bi_{0.4}Sb_{1.6}Te_3$ layer. Again n-type $Bi_2Te_3$ film was grown onto the patterned p-type thermoelectric film and n-type strips are formed by using selective chemical etchant for $Bi_2Te_3$. The top electrical connector was formed by thermally deposited metal film. The generator consists of 20 pairs of p- and n-type legs. We demonstrate complex structures of different conduction types of thermoelectric element on same substrate by two separate runs of MOCVD with etch-stop layer and selective etchant for n-type thermoelectric material. Device performance was evaluated on a number of thermoelectric devices. To demonstrate power generation, one side of the device was heated by heating block and the voltage output was measured. The highest estimated power of 1.3mW is obtained at the temperature difference of 45K. We provide a promising approach for fabricating thin film thermoelectric generators by using MOCVD grown thermoelectric materials which can employ nanostructures for high thermoelectric properties.