• Title/Summary/Keyword: Heated Block

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A Research on Lengthening the Life of Warm Forging Die (온간단조금형의 수명연장에 관한 연구)

  • Kim, Sei-Hwan
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.11 no.1
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    • pp.49-54
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    • 2010
  • Rotor pole for AC(alternating current) generator is manufactured through transfer warm forging die. As soon as the material is heated at the warm manufacturing process, it is transferred to the first stage for upsetting work and then to the second stage for lateral extrusion work. The processes at the lateral extrusion work such as die block, die bushing, center punch, and side punch make severe condition and abrasion which leads to shorten the die life. This causes production decrease, long maintenance time, and low level of precision. Research on the die material selection, heat process cycle improvement, electric discharge machining trouble solution, and re-construction of main parts is expected to find a method to lengthen the die life up to 40 - 50%.

The Study on the Measurement of Formaldehyde in Hair by HS-GC-MS (헤드스페이스-가스크로마토그래피-질량분석법에 의한 체모 중 포름알데하이드 측정법 연구)

  • Shin Ho-Sang;Ahn Hye-Sil
    • Journal of Environmental Health Sciences
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    • v.32 no.1 s.88
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    • pp.67-70
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    • 2006
  • A gas chromatography/mass spectrometric method was developed for the determination of formaldehyde in hair. 0.3mg of hair was placed in 10ml headspace vial. 1.5mM pentafluorophenylhydrazine solution (pH 2) in 0.03 M phosphoric acid and $20\;{\mu}l$ of 500 mg/l $acetone-d_6$ as internal standard were added in vial and sealed tightly with cap. The solution was heated for 30 min at $90^{\circ}C$ in heating block. The extraction, the derivatization and the evaporation were performed simultaneously. After heating of the solution, 0.5 ml of headspace was taken up and analyzed by gas chromatography-mass spectrometry (GC-MS). Low limit of detection (LaD) and Low limit of quantitation (LOQ) of formaldehyde were 0.5 and 1.5 ng/g, respectively. The method was used to analyze formaldehyde in rat hair after oral exposure. The developed method may be valuable to be used to analyze formaldehyde in human hair.

he Study of Nucleic Acid Extraction Method from Archival Paraffin Blocks (보존된 파라핀 블록에서 핵산 추출기법에 관한 연구)

  • Joo, Kyung-Woong
    • Korean Journal of Clinical Laboratory Science
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    • v.40 no.2
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    • pp.113-117
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    • 2008
  • It designed a study to examine the efficiency of DNA and RNA extraction from archival formalin-fixed, paraffin-embedded tissues using an non-heating and heating method. Archival paraffin blocks of liver, kidney, colon were randomly selected. Each paraffin block was prepared in 20 microtubes. For each paraffin blocks were tested non-heating DNA extraction to 10 microtubes and heating protocol under pH 7.0 and $100^{\circ}C$ to 10 microtubes. Evaluation of the results of DNA extraction was carried out by measuring concentration by UV spectrophotometry and then PCR amplification. DNA extraction content that non-heating method was liver $5{\pm}0.7{\mu}g/mL$, kidney $2{\pm}0.3{\mu}g/mL$, colon $6{\pm}0.4{\mu}g/mL$ and heating method was liver $12{\pm}0.6{\mu}g/mL$, kidney $7{\pm}0.5{\mu}g/mL$, colon $10.{\pm}0.3{\mu}g/mL$. Successful RNA extraction was observed, by ${\beta}$-actin amplification, in 46.7% sections for samples treated by the heating method versus 30.0% using non-heating DNA extraction. The extracted nucleic acid showed better values for samples heated at $100^{\circ}C$. Therefore heating extraction of nucleic acid is reliable, quick and efficiency.

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An Experimental Investigation of the Boiling Heat Transfer on the Vertical Square Surface (수직면에서의 비등 열전달에 대한 실험적 연구)

  • Kim, Jae-Kwang;Song, Jin-Ho;Kim, Sin;Kim, Sang-Baik;Kim, Hee-Dong
    • Transactions of the Korean Society of Mechanical Engineers B
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    • v.25 no.9
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    • pp.1237-1244
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    • 2001
  • An experimental study was carried out to identify the various regimes of natural convective pool boiling and to determine the boiling heat transfer curve and Critical Heat Flux(CHF) on a vertical square surface having a 70mm width and a 70mm height. The heater made of copper block with embedded cartridge heaters is submerged in a water tank at atmospheric pressure. As the heat flux increases from 100kW/㎡ to 1.2MW/㎡, the heat transfer regime migrates from the nucleate boiling to the film boiling. The boiling heat transfer data are fitted by Rohsenow type correlation. An explosive vapor generation on the heated surface, whose size and frequency are characterized by the heat flux, is visualized using a high speed digital imaging system.

A Study on Weldment Boundary Condition for Elasto-Plastic Thermal Distortion Analysis of Large Welded Structures (대형 용접구조물의 탄소성 열변형 해석을 위한 용접부의 변형률 경계조건에 관한 연구)

  • Ha, Yun-Sok
    • Journal of Welding and Joining
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    • v.29 no.4
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    • pp.48-53
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    • 2011
  • A thermal distortion analysis which takes strains directly as boundary conditions removed barrier of analysis time for the evaluation of welding distortion in a large shell structure like ship block. If the FE analysis time is dramatically reduced, the structure modeling time or the input-value calculating time will become a new issue. On the contrary to this, if the calculation time of analysis input-value is dramatically reduced and its results also are more meaningful, a little longer analysis time could be affirmative. In this study, instead of using inherent strain based on elastic analysis, a thermal strain based on elasto-plastic analysis is used as the boundary condition of weldments in order to evaluate the welding distortion. Here, the thermal strain at the weldment was established by using a stress-strain curve established from the test results. It is possible to automatically recognize the modeling induced-stiffness in the shrinkage direction of welded or heated region. The validity of elasto-plastic thermal distortion analysis was verified through the experiment results with various welding sequence.

Surface Temperature of Flooring Board Using Woodceramics with Sending an Electric Current (우드세라믹 통전에 의한 마루판의 표면온도 변화)

  • Oh, Seung-Won
    • Journal of agriculture & life science
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    • v.46 no.1
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    • pp.29-34
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    • 2012
  • To examine possibilities to make use of woodceramics for the lower material of hot-floored ondol boards, woodceramics made from sawdust board with Pinus densiflora, put them in a wood frame and concrete block and heated them sending an electric current, and measured changes in surface temperature of a laminated floor board and a plywood floor board. As the sending an electric current to time passed, their surface temperature increased rapidly up to 20 minutes, and then gradually ascended. In terms of the surface temperature in the wood frame, the beginning temperature of a plywood floor board was higher than that of laminated floor one; however, as time passed, a laminated floor board's temperature rose, and after 60 minutes, it showed similar to the temperature of a floor board of lamination. On the other hand, the surface temperature in a concrete block showed that the laminated floor board was higher than the plywood floor board in both early and 60-minute later temperatures. With the lapse of time after switching off, the surface temperature of floor boards slowly dwindled up to 9 minutes, and from that time on, began to drop sharply. In terms of the descent speed of surface temperature, when woodceramics' surface temperature was adjusted at $70^{\circ}C$, the laminated floor board was the highest; when it was at $80^{\circ}C$, the plywood floor board was the highest, resulting in rapid descent speed of heat.

Effects of Heat-Treatments on Transformation Behavior of Matrix Structures in High Alloyed White Cast Iron (고합급백주철에 있어서 열처리가 기지조직의 변태에 미치는 영향)

  • Shin, Sang-Woo;Ryu, Seong-Gon
    • Korean Journal of Materials Research
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    • v.10 no.6
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    • pp.409-414
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    • 2000
  • Three different white cast irons alloyed with Cr, V, Mo and W were prepared in order to study their transformation behavior of matrix structures in heat-treated conditions. The specimens were produced using a 15kg-capacity high frequency induction furnace. Melts were super-heated to $1600^{\circ}C$, and poured at $1550^{\circ}C$ into Y-block pepset molds. Three combinations of the alloying elements were selected so as to obtain the different types of carbides and matrix structures : 3%C-10%Cr-5%Mo-5%W(alloy No. 1), 3%C-10%V-5%Mo-5%W(alloy No. 2) and 3%C-17%Cr-3%V(alloy No. 3). The heat-treatments were conducted as follows: frist of all, as-cast specimens were homogenized at $950^{\circ}C$ for 5h under the vacuum atmosphere. Then, they were austenitized at $1050^{\circ}C$ for 2h and followed by air-hardening in air. The air-hardened specimens were tempered at $300^{\circ}C$ for 3h. The observation of morphology of the matrix structures was carried out in the states of as-cast(AS), air-hardened(AHF) and tempered(AHFT). The matrix structures of each alloy were almost fully pearlitic in the as-cast state but it was transformed to martensite, tempered martensite and retained austenite by the heat-treatments such as air-hardening and tempering.

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Screening and Evaluation of Streptomyces Species as a Potential Biocontrol Agent against a Wood Decay Fungus, Gloeophyllum trabeum

  • Jung, Su Jung;Kim, Nam Kyu;Lee, Dong-Hyeon;Hong, Soon Il;Lee, Jong Kyu
    • Mycobiology
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    • v.46 no.2
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    • pp.138-146
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    • 2018
  • Two-hundred and fifty-five strains of actinomycetes isolated from soil samples were screened for their antagonistic activities against four well-known wood decay fungi (WDF), including a brown rot fungus, Gloeophyllum trabeum and three white rot fungi Donkioporia expansa, Trametes versicolor, and Schizophyllum commune. A dual culture assay using culture media supplemented with heated or unheated culture filtrates of selected bacterial strains was used for the detection of their antimicrobial activity against four WDF. It was shown that Streptomyces atratus, S. tsukiyonensis, and Streptomyces sp. greatly inhibited the mycelial growth of the WDF tested compared with the control. To evaluate the biocontrol efficacy of S. atratus, S. tsukiyonensis, and Streptomyces sp., wood blocks of Pinus densiflora inoculated with three selected Streptomyces isolates were tested for weight loss, compression strength (perpendicular or parallel to the grain), bending strength, and chemical component changes. Of these three isolates used, Streptomyces sp. exhibited higher inhibitory activity against WDF, especially G. trabeum, as observed in mechanical and chemical change analyses. Scanning electron microscopy showed that cell walls of the wood block treated with Streptomyces strains were thicker and collapsed to a lesser extent than those of the non-treated control. Taken together, our findings indicate that Streptomyces sp. exhibits the potential to be used as a biocontrol agent for wood decay brown rot fungus that causes severe damage to coniferous woods.

Growth of Bi-Te Based Materials by MOCVD and Fabrication of Thermoelectric Thin Film Devices (MOCVD 법에 의한 Bi-Te계 열전소재 제조 및 박막형 열전소자 제작)

  • Kwon, Sung-Do;Ju, Byeong-Kwon;Yoon, Seok-Jin;Kim, Jin-Sang
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.12
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    • pp.1135-1140
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    • 2008
  • Bismuth-telluride based thin film materials are grown by Metal Organic Chemical Vapor Deposition(MOCVD). A planar type thermoelectric device has been fabricated using p-type $Bi_{0.4}Sb_{1.6}Te_3$ and n-type $Bi_2Te_3$ thin films. Firstly, the p-type thermoelectric element was patterned after growth of $4{\mu}m$ thickness of $Bi_{0.4}Sb_{1.6}Te_3$ layer. Again n-type $Bi_2Te_3$ film was grown onto the patterned p-type thermoelectric film and n-type strips are formed by using selective chemical etchant for $Bi_2Te_3$. The top electrical connector was formed by thermally deposited metal film. The generator consists of 20 pairs of p- and n-type legs. We demonstrate complex structures of different conduction types of thermoelectric element on same substrate by two separate runs of MOCVD with etch-stop layer and selective etchant for n-type thermoelectric material. Device performance was evaluated on a number of thermoelectric devices. To demonstrate power generation, one side of the sample was heated by heating block and the voltage output measured. As expected for a thermoelectric generator, the voltage decreases linearly, while the power output rises to a maximum. The highest estimated power of $1.3{\mu}W$ is obtained for the temperature difference of 45 K. we provide a promising procedure for fabricating thin film thermoelectric generators by using MOCVD grown thermoelectric materials which may have nanostructure with high thermoelectric properties.

MOCVD를 이용한 $BiSbTe_3$ 박막성장 및 열전소자 제작

  • Kwon, Sung-Do;Yoon, Seok-Jin;Ju, Byeong-Kwon;Kim, Jin-Sang
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.11a
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    • pp.425-425
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    • 2008
  • Bismuth-antimony-telluride based thermoelectric thin film materials were prepared by metal organic vapor phase deposition using trimethylbismuth, triethylantimony and diisopropyltelluride as metal organic sources. A planar type thermoelectric device has been fabricated using p-type $Bi_{0.4}Sb_{1.6}Te_3$ and n-type $Bi_2Te_3$ thin films. Firstly, the p-type thermoelectric element was patterned after growth of $4{\mu}m$ thickness of $Bi_{0.4}Sb_{1.6}Te_3$ layer. Again n-type $Bi_2Te_3$ film was grown onto the patterned p-type thermoelectric film and n-type strips are formed by using selective chemical etchant for $Bi_2Te_3$. The top electrical connector was formed by thermally deposited metal film. The generator consists of 20 pairs of p- and n-type legs. We demonstrate complex structures of different conduction types of thermoelectric element on same substrate by two separate runs of MOCVD with etch-stop layer and selective etchant for n-type thermoelectric material. Device performance was evaluated on a number of thermoelectric devices. To demonstrate power generation, one side of the device was heated by heating block and the voltage output was measured. The highest estimated power of 1.3mW is obtained at the temperature difference of 45K. We provide a promising approach for fabricating thin film thermoelectric generators by using MOCVD grown thermoelectric materials which can employ nanostructures for high thermoelectric properties.

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