• Title/Summary/Keyword: Heat-treatment Technique

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Die Life Estimation of Hot Forging for Surface Treatment and Lubricants (표면처리 및 윤활제에 따른 열간 단조 금형의 수명 평가)

  • 이현철;김병민;김광호
    • Journal of the Korean Society for Precision Engineering
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    • v.20 no.7
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    • pp.26-35
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    • 2003
  • This study explains the effects of lubricant and surface treatment on hot forging die life. The mechanical and thermal load, and thermal softening which is happened by the high temperature of die, in hot and warm forging, cause die wear, heat checking and plastic deformation, etc. This study is fur the effects of solid lubricants and surface treatment condition for hot forging die. Because cooling effect and low friction are essential to the long life of dies, optimal surface treatment and lubricant are very important to improve die life for hot forging process. The main factors, which affect die hardness and heat transfer, are surface treatments and lubricants, which are related to thermal diffusion coefficient and heat transfer coefficient, etc. For verifying these effects, experiments are performed for hot ring compression test and heat transfer coefficient in various conditions as like different initial billet temperatures and different loads. The effects of lubricant and surface treatment for hot forging die life are explained by their thermal characteristics. The new developed technique in this study for predicting tool life can give more feasible means to improve the tool life in hot forging process.

Effects of Heat Treatment on the Nutritional Quality of Milk: V. The Effect of Heat Treatment on Milk Enzymes (우유의 열처리가 우유품질과 영양가에 미치는 영향: V. 열처리가 우유효소에 미치는 영향)

  • Shin, Hanseob;Oh, Sejong
    • Journal of Dairy Science and Biotechnology
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    • v.36 no.1
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    • pp.49-71
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    • 2018
  • Heat treatment is the most popular processing technique in the dairy industry. Its main purpose is to destroy the pathogenic and spoilage bacteria in order to ensure that the milk is safe throughout its shelf life. The protease and lipase that are present in raw milk might reduce the quality of milk. Plasmin and protease, which are produced by psychrotrophic bacteria, are recognized as the main causes of the deterioration in milk flavor and taste during storage. The enzymes in raw milk can be inactivated by heat treatment. However, the temperature of inactivation varies according to the type of enzyme. For example, some Pseudomonas spp. produce heat-resistant proteolytic and lipolytic enzymes that may not be fully inactivated by the low temperature and long time (LTLT) treatment. These types of enzymes are inhibited only by the high temperature and short time (HTST) or ultra-high temperature (UHT) treatment of milk.

Effects of Heat Treatment on Secondary Phase Formation and Nanoindentation Creep Behavior of Nanocrystalline CoCrFeMnNi High-entropy alloy (나노결정립 CoCrFeMnNi 고엔트로피합금의 열처리에 따른 이차상 형성 및 나노압입 크리프 거동 변화 연구)

  • Dong-Hyun Lee;Jae-il Jang
    • Journal of the Korean Society for Heat Treatment
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    • v.36 no.3
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    • pp.128-136
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    • 2023
  • In this study, the effects of heat treatment on the nano-scale creep behavior of CoCrFeMnNi high-entropy alloy (HEA) processed by high-pressure torsion (HPT) was investigated through nanoindentation technique. Nanoindentation experiments with a Berkovich indenter were performed on HPT-processed alloy subjected to heat treatment at 450℃, revealing that the hardness of the HPT-processed alloy (HPT sample) significantly increased with the heat treatment time. The heat treatment-induced microstructural change in HPT-processed alloy was analyzed using transmission electron microscopy, which showed the nano-sized Cr-, NiMn-, and FeCo-rich phases were formed in the HPT-processed alloy subjected to 10 hours of heat treatment (HPT+10A sample). To compare the creep behavior of HPT and HPT+10A samples, constant load nanoindentation creep experiments were performed using spherical indentation indenters with two different radii. It was revealed that the predominant mechanism for creep highly depended on the applied stress level. At low stress level, both HPT and HPT+10A samples were dominated by Coble creep. At high stress level, however, the mechanism transformed to dislocation creep for HPT sample, but continued to be Coble creep for HPT+10A sample, leading to higher creep resistance in the HPT+10A sample.

Evaluation of Plasma Spray Hydroxy Apatite coatings on Metallic Materials

  • Take, S.;Mitsui, K.;Kasahara, M.;Sawai, R.;Izawa, S.;Nakayama, M.;Itoi, Y.
    • Corrosion Science and Technology
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    • v.6 no.6
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    • pp.286-290
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    • 2007
  • Biocompatible Hydroxy apatite (HAp) coatings on metallic substrate by plasma spray techniques have been developed. Long-term credibility of plasma spray HAp coatings has been evaluated in physiological saline by electrochemical measurements. It was found that the corrosion resisitance of SUS316L based HAp/Ti conbined coatings was excellent even after more than 10 weeks long-term immersion. It was shown that postal heat treatment improved both the crystallinity and corrosion resistance of HAp. By lowering cooling rate during heat treatment process, less cracks produced in HAp coating layer, which lead to higher credibility of HAp during immersion in physiological saline. The ICP results showed that the dissolution level of substrate metallic ions was low and HAp coatings produced in this research can be acceptable as biocompatible materials. Also, the concentration of dissolved ions from HAp coatings with postal heat treatment was lower compared to those from samples without postal heat treatment. The adherence of HAp coatings with Ti substrate and other mechanical properties were also assessed by three-point bending test. The poor adhesion of HAp coating to titanium substrate can be improved by introducing a plasma spray titanium intermediate layer.

Effects of Thermal Treatments on Microstructural Features and Magnetic Properties of Rapidly Quenched Fe-6.5%Si Strip (열처리에 따른 급냉 Fe-6.5%Si 스트립의 미세구조 및 자기특성 변화)

  • Sung, Jin-Kyung;Kim, Mun-Chul
    • Journal of Korea Foundry Society
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    • v.15 no.4
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    • pp.397-407
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    • 1995
  • The objectives of this study are first, to expand our understanding of relationship between magnetic properties and microstructural features such as grain size and texture, and second to reduce core loss of Fe-6.5%Si strip through optimizing heat treatment conditions. A rapid solidification technique, planar flow casting(PFC), was adopted to produce Fe-6.5%Si strips. The strips were heat treated under various conditions. The results show that heat treatment conditions can change not only grain size but also (200) texture formation on the strip surface. Variation in magnetic properties of Fe-6.5%Si strip is analyzed in terms of the change in grain size as well as (200) texture on the strip surface. The heat treatment conditions of $1100^{\circ}C$ over 2 hr or $1150^{\circ}C$ $1{\sim}2hr$ in $N_2+5%H_2$ appear to minimize core loss of Fe-6.5%Si strips.

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Metallic pattern Heat treatment by means of CW Nd:YAG Laser (CW Nd:YAG 레이저를 이용한 금형열처리)

  • Shin, Ho-Jun;Yoo, Young-Tae;Oh, Yong-Seak;Ro, Kyoung-Bo
    • Proceedings of the KSME Conference
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    • 2003.11a
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    • pp.1898-1904
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    • 2003
  • Laser heat treatment is an effective technique used to improve the tribological properties and also to increase the service life of automobile components such as camshafts, crankshatfs, lorry brake drums and gears. High power $CO_{2}$ lasers and Nd:YAG lasers are employed for localized hardening of materials and hence are of potential application in the automobile industries. The heat is conducted rapidly into the bulk of the specimen causing self-quenching to occur and the formation of matrensitic structure. In this investigation, the microstructrual features occurring in Nd:YAG laser hardening SM45C and $STD_{11}$ steel are discussed with the use of optical microscopic and scanning electron microscopic analysis. Moreover, This paper describes the optimisation of the processing parameters for maximum hardened depth of SM45C and $STD_{11}$ steel specimens of 10mm thickness by using CW Nd:YAG laser.

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Laser Hardening of Piston Ring Groove (피스톤 링그루브의 레이저 열처리)

  • Song, Y.K.;Suh, S.
    • Journal of the Korean Society for Heat Treatment
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    • v.10 no.3
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    • pp.165-171
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    • 1997
  • Laser hardening for the piston ring groove of ductile cast iron was tried. Mechanical and microstructural investigation for the hardened area indicated that the laser heating technique could replace conventional induction hardening process completely and further showed that post grinding process would be eliminated by minimizing bulging of heat treated area. In laser hardening, the volume increase caused by martensitic phase transformation proved to be less than $10{\mu}m$, which insures no post machining on the hardened surface. As expected, the depth of hardening was inversely proportional to the beam scanning velocity and the highest surface hardness was obtained at the beam velocity of 0.75m/min. Heat treatment using phosphate coating demonstrated quite comparable result to the case of graphite suscepter.

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The Study for Application of the Hot Medicinal Compress Technique of the Donguibogam ("동의보감(東醫寶鑑)"에 기재된 위법(熨法)의 활용에 대한 조사)

  • Kwon, O-Sang;Baek, Seung-Min;Kim, Sul-Gi;Choi, Sun-Mi
    • Korean Journal of Acupuncture
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    • v.28 no.4
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    • pp.137-145
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    • 2011
  • Objectives : This research dealt with the content of the hot medicinal compress technique in Donguibogam in order to develope the hot medicinal compress technique as a new therapy technique. Methods : In this research, we searched for the hot medicinal compress treatment in Donguibogam. Results : The hot medicinal compress technique mainly cures the diseases on the body surface and it can be applied to digestive troubles and gynecologic diseases. The hot medicinal compress technique is operated mainly at wound around the affected parts and it is applied to the constitutional symptom at the abdominal region. In the hot medicinal compress technique was used much more with medication, and the herbs used in the treatment consists of hot tastes and the warm characteristics. In the hot medicinal compress method with direct heating the herbs was mainly used. Conclusions : The hot medicinal compress technique is considered as treatment which can be utilized easily and it can be used an easy and useful self-treatment.

Effects of Ca Implantation on the Sintering and Crack Healing Behavior of High Purity $Al_2$O$_3$ Using Micro-Lithographic Technique-III: Stability of Crack-Like Pore (Ion Implantation으로 Ca를 첨가된 단결정 $Al_2$O$_3$의 Crack-Like Pore의 Healing 거동-III: Stability of Crack-Like Pore)

  • 김배연
    • Journal of the Korean Ceramic Society
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    • v.36 no.9
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    • pp.887-892
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    • 1999
  • The inner crack-like pore with controlled amount of Ca impurity in the high purity alumina single crystal sapphire had been created by micro-fabrication technique which includes ion implanation photo-lithography Ar ion milling and hot press technique. The crack-like pores in two-hour hot pressed specimen were extremely stable even after heat treating at 1,80$0^{\circ}C$ for 5 hours almost no healing was observed. But the crack-like pores in one-hour hot pressed specimen at 1,30$0^{\circ}C$ were healed by heat treatment and the amount of healing was increased with the heat treatment time and temperature and the amount of Ca addition. The edges of crack-like pore parallel to <1100> direction in (001) basal plane were stable but the edges normal to this direction in (00101) plane <1120> direction were unstable to facetting This means that the surface energy of alumina along the <1100> direction in (0001) basal plane in much lower than <1120> direction.

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A Study on the Surface Phenomena of Re-creational Gilt Layer by Conditions of Heat Treatment (열처리 조건에 따른 재현 도금층의 표면현상 연구)

  • Yang, Seok-Woo;Kim, Soo-Ki
    • Journal of Conservation Science
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    • v.28 no.1
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    • pp.29-37
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    • 2012
  • This study discusses a mercury amalgam gilding technique and examines how the color, surface and section of the gilt layer changes as the condition of heat treatment with mercury amalgam gilt object is changed. Some previous studies have mentioned reasons for various colors on gilt bronze artifacts depending on gilding manufacture and environment. However, reason for reddish color with gold on the artifacts' surface brought on high temperature corrosion has yet to be discussed and analyzed. A methodology was found in representing the mercury amalgam gilding technique and heat treatment test. According to the result of the heat treatment test, in the conditions of higher temperature and longer time, the oxidized layer on the gilt layer was distributed more widely and in the part when the oxide layer was eliminated, the gilt layer with a reddish color was observed. Moreover, in the surface observation of the specimen on which yellow and reddish colors were agitated, the changing aspects of its surface condition differed by colors. When investigated the section, it was observed that the void density and size became larger. After a test, the surface components changed; the temperature of heat treatment increased, component ratio of Hg and Au decreased gradually but component ratio of Cu increased. In regard to the gilt layer, as the time was longer and the temperature became higher for the heat treatment, the component ratio of Au and Cu by layers tended to change in inverse proportion. It is concluded that gilding techniques and the burial environment can make a difference in the surface color of the gilt layer on the gilt bronze artifacts, the high temperature corrosion that occurs by heat after they are manufactured is also one of the factors that affects their surface color.