• Title/Summary/Keyword: Heat stability

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Microstructures and Grain Stabilities of Mg-Zn-(Zr) Alloys (Mg-Zn-(Zr) 합금의 미세조직과 결정립의 안정성)

  • Jun, Joong-Hwan
    • Journal of the Korean Society for Heat Treatment
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    • v.23 no.6
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    • pp.309-314
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    • 2010
  • Microstructures and grain growth behaviors at elevated temperatures have been investigated for extruded Mg-2%Zn and Mg-2%Zn-0.3%Zr alloys, in order to clarify the role of Zr in grain stability of Mg-Zn alloy. The grain size of Zr-free alloy increased continuously with an increase in annealing temperature, when isochronally annealed for 60 min from 573 to 723K, while the grains of the Zr-containing alloy were relatively stable up to 723 K. The activation energies for grain growth ($E_g$) between 573 and 723 K were calculated as 77.8 and 118.6 kJ/mole for the Mg-2%Zn and Mg-2%Zn-0.3%Zr alloys, respectively, which indicates that grains in the Zr-added alloy possess higher thermal stabilities at elevated temperatures. TEM observations on the annealed Mg-2%Zn and Mg-2%Zn-0.3%Zr alloys revealed that enhanced grain stability resulting from Zr addition into Mg-Zn alloy would be ascribed to the restriction of grain growth by stable Zn-Zr nano-precipitates distributed in the microstructure.

Thermal Comfort and Tactile Wearing Performance of Wool/nylon Fabrics for Tra-biz Garment (울/나일론 tra-biz 의류용 직물 소재의 열적 쾌적성과 착용특성)

  • Kim, Hyun Ah
    • Fashion & Textile Research Journal
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    • v.18 no.6
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    • pp.878-888
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    • 2016
  • In this study, wool/nylon(50/50%) blend yarn and its fabrics for tra-biz(complex word of travel+business) garment were prepared, and its wear comfort characteristics were investigated through thermal manikin and human-body wearing experiment. In addition, tactile wearing performance from fabric mechanical properties and the dimensional stability and the pilling of the fabric specimen during wearing and dry-cleaning were measured and compared with those of wool 100% fabric specimen. Heat keepability of the wool/nylon(50/50%) blend fabric by thermal manikin experiment was superior than that of wool 100% fabric, this result was verified with human-body wearing experiment and its result coincided well with this experimental result. Tactile wearing performance of the wool/nylon(50/50%) fabric from fabric mechanical properties measured by FAST system was better than that of the wool 100% fabric. The dimensional stability of the wool/nylon(50/50%) fabric was more stable than that of the wool 100% fabric. Because relaxation shrinkage was lower and hygral expansion of wool 100% fabric was more high. However, the breathability and pilling property of the wool/nylon(50/50%) fabric were inferior than those of the wool 100% fabric. The possibility of application for tra-biz garment of wool/nylon(50/50%) blend fabric was observed because of good heat keepability, tactile wearing performance and washing fastness.

A Study on the Thermal Stability of Duplex High Mn-Steel Structure (고 망간강 2상 혼합조직의 열적 안정성에 관한 연구)

  • Wey, Myeong Yong
    • Journal of the Korean Society for Heat Treatment
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    • v.5 no.1
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    • pp.13-22
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    • 1992
  • The thermal stability of duplex high Mn-steel structure have been investigated using 15%Mn~1.0~2.4%C steels which are composed of ${\gamma}$-and ${\theta}$-phases in the range of temperature from 900 to $1100^{\circ}C$, and time from 50 to 300h. The results are as follows ; 1) The grain growth in single-phase region proceeds by grain boundary migration and the relation between mean radius $\bar{r}$ and annealing time t is described as follows ; $\bar{r}^2-{\bar{r}_0}^2=k_0{\cdot}t$ 2) The grain growth of duplex, (${\gamma}+{\theta}$), strucrure is slower than that single phase because the chemical composition of ${\gamma}$-and ${\theta}$-phases differs esch others. 3) The grain of (${\gamma}+{\theta}$) duplex structure grow slowly in a mode of Ostwald ripening. Because grain boundaries of ${\gamma}$-phase migrate under a restriction of pinning by ${\theta}$-phases. 4) In the duplex structures. the dispersed structures change to the dual-structures, as the volume fraction of the dispersed second-phase increase. Consequently, the growth-law, which is controlled by boundary-diffusion change to that of the volume diffusion-mechanism.

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Study on Improving the Mechanical Stability of 3D NAND Flash Memory String During Electro-Thermal Annealing (3D NAND 플래시메모리 String에 전열어닐링 적용을 가정한 기계적 안정성 분석 및 개선에 관한 연구)

  • Kim, Yu-Jin;Park, Jun-Young
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.35 no.3
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    • pp.246-254
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    • 2022
  • Localized heat can be generated using electrically conductive word-lines built into a 3D NAND flash memory string. The heat anneals the gate dielectric layer and improves the endurance and retention characteristics of memory cells. However, even though the electro-thermal annealing can improve the memory operation, studies to investigate material failures resulting from electro-thermal stress have not been reported yet. In this context, this paper investigated how applying electro-thermal annealing of 3D NAND affected mechanical stability. Hot-spots, which are expected to be mechanically damaged during the electro-thermal annealing, can be determined based on understanding material characteristics such as thermal expansion, thermal conductivity, and electrical conductivity. Finally, several guidelines for improving mechanical stability are provided in terms of bias configuration as well as alternative materials.

An Experimental Study on the Flame Stability of Natural Gas/Air Mixture on the Metal Mesh (금속매쉬에서 천연가스/공기 표면연소의 화염안정성에 관한 실험적 연구)

  • You, Hyun-Seok;Lee, Hyun-Chan;Lee, Joong-Sung
    • Proceedings of the KSME Conference
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    • 2001.06d
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    • pp.49-53
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    • 2001
  • A conventional flame type gas combustion major portion of heat is transferred to the body by convection due to small radiant ability of the gas flame. Increasing the radiation component of heat flux in the combustion zone allows to augment the efficiency of gas utilization. Such effect can be reached by using radiative gas burner applied to metal mesh combustion. Basically the gas radiant burner consists of metallic mesh of high heat resisting steels. In terms of this regards, we have made the burner consisted of metal mesh and measured the radiative flame stability of natural gas/air mixture on the metal mesh burner. The pressure loss through the metal mesh is defined by pressure-velocity slope. The more increased the pressure-velocity slope of the metal mesh is, the wider the stable zone of radiave flame on the metal mesh burner is. And the augmentation of mixture flowrate through the metal mesh make narrow the permissible range of equivalence ratio.

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The Experimental Study of Flux Improvement of Wet Underwater Arc Welding Electrode (습식 수중 용접봉의 피복제 개발에 관한 기초연구)

  • Kim, Min-Nam;Kang, Jung-Gun
    • Journal of Ocean Engineering and Technology
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    • v.13 no.4 s.35
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    • pp.28-36
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    • 1999
  • Wet underwater arc welding process is investigated by using experimentally developed flux coated underwater arc welding electrode and SS400 steel plate of 12mm thickness as base metal. Three kinds of different flux covered wet arc welding electrode of 4mm diameter(BK-01, BK-02, BK-03) are individually developed, and one of the improved underwater welding electrode (BK-03) may be put to practical use for underwater wet arc welding process. The results obtained from this experimental study are as follows : 1. Arc stability of developed underwater wet welding electrode is better than that of the domestic covered arc welding electrode. 2. Workability of welding electrode, remove ability of slag and bead appearances using improved underwater wet welding electrode are remarkably better than that of others. 3. Heat affected zone of test specimen welded in the underwater gets to become a lot smaller than that of test specimen welded in the air, and the maximum hardness of heat affect zone of developed underwater wet welding electrode is lower to that of domestic arc welding electrode.

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Preparation of Fuel Cell Electrode Impregnated Platinum by Methanol Reduction Method -Effect of Surfactant and Heat Treatment at Pt Impregnation- (메탄올 환원법에 의한 연료전지용 백금담지 전극제조 -촉매담지시 계면활성제 첨가와 열처리 온도 효과-)

  • Jung, Eun-Ey;Yoo, Duck-Young;Eun, Yeong-Chan;Lee, Ju-Seong
    • Applied Chemistry for Engineering
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    • v.8 no.1
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    • pp.16-22
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    • 1997
  • When platinum wan impregnated on carbon by methanol, surfactant have an important effect on the stability of platinum colloid. As the increase of amounts of surfactant enhanced the stability of platinum colloid, the particle size of platinum on carbon was diminished. But, after heat treatment, residue of surfactant remained in electrode to decrease current density of oxygen reduction. To remove surfactant, as temperature of heat treatment enhanced, platinum particle was aggromerated and current density was decreased.

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금속 이온을 이용한 Bacillus Stearothermophilus 호열성 단백질 분해효소의 역가 향상 및 호열 ${\cdot}$ 호기성 소화공정에의 응용

  • Kim, Yeong-Gi;Bae, Jin-Hye;Lee, Won-Hong;Choe, Jeong-U
    • 한국생물공학회:학술대회논문집
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    • 2000.11a
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    • pp.167-170
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    • 2000
  • Proteolytic hydrolysis is one of the main enzymatic reaction of waste activated sludge (WAS) digestion. Pretense excreted from Bacillus stearothermophilus (ATCC 31197) showed optimum temperature of $75^{\circ}C$ for maxium heat stable proteolytic activity against azo casein. The dependency of $Ca^{2+}$, $Zn^{2+}$ on heat stability of proteolytic enzymes were measured with various concentrations. It was shown that $Ca^{2+}$ ion enhanced heat stability of these enzymes. Then thermophilic aerobic digestion (TAD) was performed using B. sterothermophilus with the addition of divalent ions. Performance of TAD process with ATCC 31197 activated by $Ca^{2+}$, $Zn^{2+}$ions in terms of dissolved organic carbon (DOC) concentration, extracellular protein concentration, and scanning electrion microscopy (SEM) analysis. The best result of protein reduction concentration in digestion test was obtained with the addition of 2 mM $Ca^{2+}$ ion.

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A Study on the Thermo-mechanical Behavior of Underground Openings in lsotropic and Structurally Snisotropic Rock Masses (등방 및 이방성 암반내 공동의 열역학적 거동에 관한 전산모델연구)

  • 문현구;주광수
    • Tunnel and Underground Space
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    • v.1 no.2
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    • pp.181-203
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    • 1991
  • The effects of geologic structures such as rock joins and bedding planes on the thermal conductivity of a discontinuous rock mass are studied. The expressions for the equivalent thermal conductivities of jointed rock masses are derived and found to be anisotropic. The degree of anisotropy depends primarily on the thermal properties contrast between the joint phase and surrounding intact rock, the joint density expressed as volume fraction and the inclination angle of the joint. Within the context of 2-dimensional finite element heat transfer scheme, the isotherms around a circular hole are analyzed for both the isotropic and anisotropic rock masses in 3 different thermal boundary conditions. i.e. temperature, heat flux and convection boundary conditions. The temperature in the stratified anisotripic rock mass is greatly influenced by the thermal properties of the rock formation in contact with the heat source. Using the excavation-temperature coupled elastic plastic finite element method, analyzed is the thermo-mechanical stability of a circular opening subjected to 10$0^{\circ}C$ at a depth of 527m. It is found that the thermal stress concentration was enough to deteriorate the stability and form a plastic yield zone around the opening, in contrast to the safety factor greater than 2 resulted form the excavation-only analysis.

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Manufacturing of Cold-rolled TRIP Steel by Reversion Process (역변태에 의한 냉연 TRIP강의 제조기술)

  • 진광근;정진환;이규영
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 1999.08a
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    • pp.356-365
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    • 1999
  • The present study is aimed at developing the TRIP(transformation induced plasticity) aided high strength low carbon steel using reversion process. An excellent combination of elongation over 40% and tensile strength abut 100kgf/$\textrm{mm}^2$ achieved in processing of 0.15C-0.5 Si-6Mn steel by slow heating to intercritial temperature region and accelerated cooling into room temperature. This good combination is caused by TRIP phenomena of retained austenite in steels during deformation. The stability of retained austenite is very important for the good ductility and it depends on the diffusion of carbon and manganeses during heat treatment. The accelerated cooling after holding at annealing temperature retards the formation of pearlite and provides the carbon enrichment in retained austenite in steel, resulting in the increase in elongation of the cold-rolled TRIP steel. On the other hand, heat treating the steel at 600$^{\circ}C$ for 5 hour before cold rolling increases elongation but reduces the amount of retained austenite after reversion processing. It is accounted that the heat treating is effective for the increase in the stability of retained austenite.

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