• 한국정밀공학회지
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• 제21권2호
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• pp.168-176
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• 2004

Interrupted creep tests were carried out on the Mod.9Cr-1Mo steel in order to investigate the structural degradation during creep. The ranges of creep stress and temperature were from 71 to 167MPa and 873 to 923k, respectively. The change of hardness and tempered martensitic lath width were measured in the grip and gauge parts of interrupted specimens. The lath structure was thermally stable in static conditions, but was not stable during creep, and the structural evolution was enhanced by creep strain. The relation between the change in lath width and strain was described in the from, $\delta$W= a ($W_s-W_o$)$cdot;varepsilon$, where $\varepsilon$ is the strain, $W_o$is the initial lath width, $W_s$ is the final lath width depending solely on stress, and a is the constant of the magnitude of 0.67 $\mu$m /strain. The change in Victors hardness was expressed by a one-valued function of creep life consumption ratio. Based on the empirical relation between strain and lath width, a model was proposed to explain the relation between change in hardness and creep life consumption ratio. The model revealed that about 65$%$ of dislocations in lath structures were eliminated by the migration of subboundaries.

• Tribology and Lubricants
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• 제32권1호
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• pp.18-23
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• 2016

The effective case depth for case-hardened rolling bearing has been discussed. For this purpose, rolling contact fatigue tests for ball bearings built with inner race of various hardness values were conducted until L₁₀ calculating rating life using a bearing life test machine under radial loading. Then, the distribution of residual stress below the inner raceway, which depended on the hardness value, was measured by X-ray diffraction. As a result, the linear relationship was established between the hardness value of the inner race and the theoretical shear stress evaluated at the depth where the residual stress disappeared below the inner raceway. Based on the relationship, it could be found that the factor of safety in bearing manufacturer’s rules for the effective case depth of case hardened rolling bearings was set higher. However, it could be also found that the hardness values at the depth where the maximum shearing stress acted below the raceway surface in a tapered roller bearing hardened by the carburizing process, were not sufficient for preventing plastic deformation under the basic dynamic load rating. Consequently, further efforts were still required to reduce or to disperse the contact load on the material design of a rolling bearing in order to prolong its life.

• Tribology and Lubricants
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• 제34권6호
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• pp.262-269
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• 2018

In this work the friction and wear characteristics of the gray cast iron surface processed by broaching method, which is widely used in the machinery industry, were investigated. The broaching process is mainly used for mass production because it has high dimensional accuracy and processing speed, but the defects on surface can be easily generated. In order to improve the tribological characteristics, the approach was to reduce the roughness and hardness of the surface by adding a machining process to the broaching specimen. The secondary machining process using abrasive grains produces low roughness and hardness than broaching because it has high tool accuracy and removes the work hardened surface. The friction coefficient and the wear rate were assessed using a reciprocating-type tribotester to analyze the effects of surface finishing on the tribological properties. The friction tests were conducted under dry and lubricated conditions. The test results showed that the reduction of surface roughness and hardness through secondary machining process in lubricated condition improved the friction and wear characteristics. The reason why the same results did not appear in a dry condition was that wear occurred more rapidly than in lubricated condition. Thus, the positive effect of roughness and hardness of the surface obtained through the secondary machining process was not observed.

• Tribology and Lubricants
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• 제16권2호
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• pp.121-125
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• 2000

Silicon nitride ceramic has been verified as an excellent rolling bearing material because of its high strength and outstanding rolling fatigue life properties. However under some corrosive circumstances it showed drawbacks such as hardness reduction and severe wear caused by corrosion. In this work, the variations of the rolling wear and hardness of three kinds of ceramics were studied for the specimen aged 15 days in alkali water (90 $\pm$ 2$\^{C}$,25 wt% NaOH ). All of the specimens, ① Si$_3$N$_4$, ② 3Y-TZP and ③ 3Y-TZP alloyed with 5 wt% CeO$_2$, were sintered and post-HIPed, and then polished up to 0.02 $\mu$mRa of surface roughness. Rolling wear tests were conducted by MJ type rolling fatigue life tester under the initial theoretical maximum contact stress of 3.16 GPa and the spindle speed of 1,000 rpm. Spindle oil was used as a lubricant. The specimens were not worn before aging. For the specimen aged in alkali water, Si$_3$N$_4$ and 3Y-TZP were worn by rolling wear tests, and hardness was decreased. While aging the specimens, the phase was transformed from tetragonal to monoclinic in 3Y-TZP and the microstructure change occurred in Si$_2$N$_4$. 3Y-TZP specimens alloyed with 5 wt% CeO$_2$ were not worn after aging and no phase transformation occurred while aging.

• 한국윤활학회:학술대회논문집
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• 한국윤활학회 1999년도 제30회 추계학술대회
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• pp.154-159
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• 1999

Silicon nitride ceramic has been verified as an excellent rolling bearing material because of its high strength and outstanding rolling fatigue life properties. However under some corrosive circumstances it showed drawbacks such as hardness reduction and severe wear caused by corrosion. In this work, the variations of the rolling wear and hardness of three kinds of ceramics were studied for the specimen aged 15 days in alkali water (90$\pm$2$^{\circ}C$, 25 wt% NaOH). All of the specimens, \circled1Si$_3$N$_4$, \circled23Y-TZP and \circled33Y-TZP alloyed with 5 wt% CeO$_2$, were sintered and post-Hipped, and then polished up to 0.02 ${\mu}{\textrm}{m}$Ra of surface roughness. Rolling wear tests were conducted by MJ type rolling fatigue life tester under the initial theoretical maximum contact stress or 3.76 Gra and the spindle speed of 1,000 rpm. Spindle oil was used as a lubricant. The specimens were not worn before aging. For the specimen aged in alkali water, Si$_3$N$_4$and 3Y-TZP were worn by rolling wear tests, and hardness was decreased. While aging the specimens, the phase was transformed from tetragonal to monoclinic in 3Y-TZP and the microstructure change occurred in Si$_3$N$_4$. 3Y-TZP alloyed with 5 wt% CeO$_2$specimens were not worn after aging and no phase transformation occurred while aging.

• 산업식품공학
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• 제22권4호
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• pp.381-385
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• 2018

즉석밥의 물성을 효율적으로 측정하기 위한 방법을 모색하고자 다양한 경도를 가진 즉석밥을 대상으로 4가지 다른 물성 기법을 적용하고 그 경도 결과를 비교 분석하였다. 이를 위해 disk, cylinder, rod, cone probe를 사용한 물성 측정법을 즉석밥에 적용하여 이들의 상관관계를 조사하였다. 모든 측정 방법에 대하여 수분함량에 따른 경도와의 상관관계를 분석한 결과 비교적 높은 음의 선형관계를 보여주어 수분함량이 증가할수록 경도가 감소하는 패턴을 명확히 보여주었다. Cone probe 측정법의 경우 압축력과 전단력을 통한 개별 밥알 시료의 변형이 가능하여 가장 높은 상관관계를 보여주었고, disk probe 측정법 또한 높은 양의 상관관계를 보였지만 죽과 같이 유동성을 가진 시료에는 적용이 어려웠다. 더 나아가 측정된 힘 값을 응력 형태로 전환시켜 상호 비교한 결과 cone과 rod probe 방법 그리고 rod와 cylinder probe 방법의 Pearson 계수가 0.9에 가까운 높은 상관관계를 보여주었다. 본 연구를 통하여 얻어진 결과는 즉석밥의 물성 측정을 위한 다양한 기법을 좀 더 이해하는데 기여할 수 있을 것으로 판단되며, 다양한 형태의 즉석밥을 개발하는데 활용될 수 있을 것으로 기대된다. 아울러, 본 연구를 통해서 얻어진 기계적 측정 결과와 관능평가 결과를 연관 지을 수 있다면 실제 식품 산업에서 활용될 수 있는 보다 의미 있는 결과를 제공할 수 있어 이에 대한 후속 연구가 필요하다.

• 대한치과보철학회지
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• 제33권3호
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• pp.569-583
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• 1995

Disinfection of dental impressions are necessary due to contamination with patient’s saliva and blood, which is a potential for cross-infection. The purpose of this study was to evaluate the effects of disinfection of four hydrophilic rubber impression materials with three disinfecting solutions, on the dimensional stability and surface hardness of improved stone casts. Three hydrophilic vinyl polysiloxane impression materials(Express, Reprosil, Exafine) and one polyether impression material(Impregum-F) were mixed according to the manufacturer’s directions and impressions were made on a ADA specification No. 19 stainless-steeldie. On removal of the impressions, each impression was immersed in one of the disinfectants(Banicide, Potadine, Clorox) for 10 minutes. After disinfection, type IV improved stone. casts were poured. On this cast, the linear dimension and surface hardness were measuredusing a Measurescope(Nikon, Japan) and a Barcol hardness tester(Barber, Colman Co U. S. A). The results were as follows : 1. The improved stone casts from disinfected Reprosil and Impregum-F impression material did not show dimensional changes(P>0.01). Those from disinfected Express and Exafine impression material showed dimensional changes(P<0.01). The amount of shrinkage was not clinically significant. 2. The improved stone casts from disinfected Express impression material did not exhibit changes in surface hardness(P>0.01), but those from disinfected Reprosil, Exafine, Imp regnum-F impression material showed changes in surface hardness(P<0.01). 3. The dimensinal stability and surface hardness of the improved stone casts were satisfactory using Banicide on Express, all disinfectants used in this study on Reprosil, Potadin and Clorox on Exafine, Banicide and Clorox on Impregum-F. According to these results, immersion disinfection of hydrophilic rubber impression mate rials did not adversely affect the resultant casts. Nevertheless compatibility tests of impression materials and disinfectants should be done when disinfecting impressions.

• 한국치위생학회지
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• 제12권3호
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• pp.513-520
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• 2012

Objectives : In this study, contact angle and shore D hardness were measured, and a shark fin test was conducted after selecting five addition silicon(Blu-Mousse, BM; EXABITE II, EX; PERFECT, PF; Regisil$^{(R)}$ Rigid, RE; Silagum$^{(R)}$, SI) in order to figure out the properties of elastomeric interocclusal recording materials and reduce errors at interocclusal recording. 8) Methods : A contact angle was measured using a contact angle analyzer. After placing a drop of liquid on the surface of the specimens of interocclusal recording materials, a contact angle was photographed with a CCD camera on the equipment. In terms of a shark fin test, interocclusal recording materials were mixed for the time proposed by the manufacturer and inserted into the split ring of the Shark fin device. Twenty (20) seconds exactly, a metal rod was removed to make the materials slowly absorbed. Once they hardened, fin height was measured with a caliper after separating molds and trimming the specimens. The shore D hardness was measured with a shore D hardness tester(Model HPDSD, Hans Schmidt & Co. Gmbh, Germany) in sixty (60) minutes after fabricating specimens. In each experiment, five specimens, mean and standard deviation were calculated. A one-way ANOVA test was performed at the p>0.05 level of significance. In terms of correlation among the tests, Pearson correlation coefficient was estimated. For multiple comparison, Scheffe's test was carried out. Results : A contact angle was the highest in EX with $99.23^{\circ}$ (p<0.05) while the result of the shark fin test was the longest in RE with 5.45mm. SI was the lowest (0.27mm) with statistical significance. Among the interocclusal recording materials, significant difference was observed in terms of means (p<0.05). The shore D hardness was the highest in SI with 31.0 while RE was significantly low with 16.4 (p<0.05). Among the materials, statistically significant difference was observed in terms of means when compared to the rest materials (RE), BM, RE and SI (PF and EX) and the remaining materials (BM and SI) (p<0.05). In terms of correlations among the tests, a negative correlation occurred between shore D hardness and shark fin test(r=-0.823, p=0.000). Conclusions : According to the study above, it is necessary to understand the properties of interocclusal recording materials and consider contact angle, shark fin test and properties of shore D hardness to select appropriate materials.

• Journal of Welding and Joining
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• 제4권3호
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• pp.32-42
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• 1986

In this study, the influence of carbon equivalents on friction welds of dissimilar steels was investigated. Four types of carbon steels with 10mm diameter were welded to a high-speed tool steel SKH 9. Main experimental results could be summarized as follows (1) Under constant friction pressure, the friction time increased almost linearly with the increasing burn-off length, while the forge length decreased almost linearly. (2) The maximum hardness in carbon steels increased almost linearly with the increasing carbon equivalent, but was much lower than that in the high speed steel. (3) After quenching and tempering of dissimilar steel friction welds, the hardness in carbon steel weldments became similar as that in the base metal, while the hardness in SKH 9 weld was still higher that of the base metal. (4) Relative movement in the friction phae occurred not at the interface of the weldments, but in the high speed steed steel near the interface. (5) For considered material combinations and welding parameters, most of fractures in tension and twisting tests occurred in the base metal. And welds with so high strength could produced in a wide range of welding parameters.

• 한국정밀공학회지
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• 제23권10호
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• pp.74-79
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• 2006

In this study, the tempering effect on the wear characteristics of induction-hardened SPS5 steel was investigated. For this purpose, three tempering conditions were applied to control the hardness of heat-treated SPS5 steel. Ball-on-disk wear tests have been performed using zircornia balls on the tempered specimens to determine the variation of wear characteristics. The results showed that friction coefficient decreased with increasing hardness for induction hardening conditions. This seems to occur because real contact area between specimen and mating ball was affected by the specimen hardness.