• Title/Summary/Keyword: H-반사

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Studies on the Near Infrared Diffuse Reflection Spectroscopy for Meat Components (근적외선 반사분광분석법에 의한 정육 및 그 구성성분의 반사 spectra에 관한 연구)

  • Oh, Eun-Kyong;Grossklaus, Dieter
    • Korean Journal of Food Science and Technology
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    • v.24 no.5
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    • pp.404-407
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    • 1992
  • This study was conducted to determine the effect of the physical and chemical factors on the absorbance when the chemical component of food was rapidly and effectively analyzed with near infrared reflection spectrophotometer. The absorbance was measured within the wavelength range of 1100 and 2500m and at the various sample temperatures. The absorbance was greatly increased with the rising sample temperature. When the grinding time of samples prolonged, the absorbance was decreased. The absorption peaks occurring in the near infrared spectra of meat, meat protein, pork fat and water were attributed to the overtone and combination vibration of C-H, N-H, O-H or C=O bond within the macromolecules of each sample. The absorbance was lower for meat protein than other meat components. Pork fat was characterized by the ${\cdot}CH_2{\cdot}$ absorption peak at the wavelength of 1700 and 2300 nm and water by the relatively high absorption peak at the wavelength of 1450 and 1930 nm. As a result, the absorbance of near infrared reflection spectrum of meat was affected mainly by fat and water in meat.

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The Early Stages of Formation of the Passivation Film on Iron Electrode. Electrochemical and Automatic Ellipsometry Investigation (철전극 표면 부동화막의 생성과 초기단계의 변화)

  • In-Hyeong Yeo;Woon-Kie Paik
    • Journal of the Korean Chemical Society
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    • v.28 no.5
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    • pp.271-278
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    • 1984
  • Ellipsometric and reflectance measurements were made with magneto-optically self-nulling ellipsometer on the iron surface being passivated. The passivation was induced by abruptly changing potential of the mechanically polished high purity iron from the reduction potential to the oxidation potential in basic solutions. From the differences in the optical paramates(${\Delta},\;{\psi}$) and reflectance (R) between the reduced (film-free) and oxidized (film-covered) states, the thickness(${\tau}$) and optical constants (n, k) of the film in the early stage of its formation were computed as functions of pH and time. From the computed values, it was deduced that the properties of the anodic film did not undergo a drastic change with time which would indicate a transformation of the film before effective passivity is attained, and that the film reached its stady state within a few second. The thickness of anodic film was $14\;{\sim}\;23{\AA}$. The anodic films also seemed to have small values of optical absorption coefficient. The film formed in high pH environments had thinner and denser structure than that formed in low pH.

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UV/H2O2 Advanced Oxidation of Photo Processing Chemicals in a UV-free Reflecting Reactor (사진현상폐수의 UV-자유반사 반응조에서의 UV/H2O2 고급산화처리)

  • Choi, Kyung-Ae;Kim, Young-Ju
    • Journal of Korean Society of Environmental Engineers
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    • v.22 no.2
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    • pp.241-249
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    • 2000
  • In this study, UV-catalyzed $H_2O_2$ oxidation and $H_2O_2$ oxidation to remove contaminants from photo processing chemicals were investigated at various conditions. Photo processing chemicals contains high concentrations of organic compounds and has very low biodegradability. Hydrogen peroxide is subjected to gradual decomposition as metastable substance. In the process, short-lived and highly reactive hydroxyl radicals are formed. The decomposition can be significantly accelerated by use of appropriate catalyst, such as ultraviolet radiation. The experiments were conducted in a UV-free reflecting reactor in batch and a high-pressure mercury lamp was used as UV source. Mixing, cooling and ventilation of the reactor were operated during experiments. In $UV/H_2O_2$ oxidation and $H_2O_2$ oxidation, the removal efficiencies of $COD_{Cr}$, TOC and chromaticity increased with the increase of $H_2O_2$ dosage and were higher in the controlled pH condition of 3 than in original pH condition of 8. In $UV/H_2O_2$ oxidation under the optimum condition of pH 8 and 1.3 stoichiometric $H_2O_2$ dosage, the removal efficiencies of $COD_{Cr}$, TOC and chromaticity were 47.5%, 75.0% and 91.5% respectively and $BOD/COD_{Cr}$ ratio was significantly increased from 0.04 to 0.21.

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PECVD를 이용한 결정질 태양전지 표면 반사방지막의 최적화

  • Lee, Gyeong-Dong;Kim, Yeong-Do;Park, Seong-Eun;Tak, Seong-Ju;Kim, Dong-Hwan
    • Proceedings of the Korean Vacuum Society Conference
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    • 2012.02a
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    • pp.212-212
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    • 2012
  • 수소화된 실리콘 질화막은 결정질 태양전지 산업에서 반사방지막 과 패시베이션 층으로 널리 사용되고 있다. 또한, 수소화된 질화막은 금속 소성공정과 같은 높은 공정온도를 거친 후에도 결정질 실리콘 태양전지의 표면층으로서 충족되는 특성들이 변하지 않고 유지되어야 한다. 본 연구에서는 PECVD 장치를 이용한 수소화된 실리콘 질화막의 특성 변화에 대한 경향성을 알아보기 위하여 증착조건의 변수(온도, 증착거리, 무선주파수 전력, 가스비율 등.)들을 다양하게 가변하여 증착조건의 최적화를 찾았다. 이후 수소화된 실리콘 질화막의 전구체가 되는 사일렌(SiH4)과 암모니아(NH3) 가스비를 변화시켜가며 결정질 실리콘 태양전지에 사용되기 위한 박막의 광학 전기 화학적 그리고 표면 패시베이션 특성들을 분석하였다. 가스 비율에 따른 수소화된 실리콘 질화막의 굴절률 범위는 1.90-2.20까지 나타내었다. 결정질 실리콘 태양전지에 사용하기 위한 가장 적합한 특성은 3.6(NH3/SiH4)의 가스비율을 나타내었다. 이를 통하여 PECVD 내에서 구현 할 수 있는 가스의 혼합(SiH4+NH3+N2, SiH4+NH3, SiH4+N2)을 달리하여 박막의 광학적 및 패시베이션 특성을 분석하였다. 이후 $156{\times}156mm$ 대면적 결정질 실리콘 태양전지를 제작하여 SiH4+NH3+N2 의 가스 혼합에서 17.2%의 변환 효율을 나타내었다.

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Identification of Flaw Signals Using Deconvolution in Angle Beam Ultrasonic Testing of Welded Joints (용접부 초음파 사각 탐상에서 디컨볼루션을 이용한 균열신호와 기하학적 반사신호의 식별)

  • Song, Sung-Jin;Kim, Jun-Young;Kim, Young-H.
    • Journal of the Korean Society for Nondestructive Testing
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    • v.22 no.4
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    • pp.422-429
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    • 2002
  • The identification of ultrasonic flaw signals is a truly difficult task in the angle beam testing of welded joints due to non-relevant signals from the geometric reflectors such as weld roots and counter bores. This paper describes a new approach called "technique for identification of flaw signal using deconvolution(TIFD)" in order to identify the flaw signals in such a problematic situation. The concept of similarity function based on the deconvolution is introduced in the proposed approach. The "reference" signals from both flaws and geometric reflectors and test signals are acquired and normalized. The similarity functions are obtained by deconvolution of test signals with reference signals. The flaw signals could be identified by the patterns of similarity function. The initiative results show great potential of TIFD to distinguish notch comer signals from the geometric reflections.

Improved Antireflection Property of Si by Au Nanoparticle-Assisted Electrochemical Etching (금 나노입자 촉매를 이용한 단결정 실리콘의 전기화학적 식각을 통한 무반사 특성 개선)

  • Ko, Yeong-Hwan;Joo, Dong-Hyuk;Yu, Jae-Su
    • Journal of the Korean Vacuum Society
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    • v.21 no.2
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    • pp.99-105
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    • 2012
  • We fabricated the textured silicon (Si) surface on Si substrates by the electrochemical etching using gold (Au) nanoparticle catalysts. The antireflective property of the fabricated Si nanostructures was improved. The Au nanoparticles of ~20-150 nm were formed by the rapid thermal annealing using thermally evaporated Au films on Si. In the chemical etching, the aqueous solution containing $H_2O_2$ and HF was used. In order to investigate the effect of electrochemical etching on the etching depth and reflectance characteristics, the sample was immersed in the aqueous etching solution for 1 min with and without applied cathodic voltages of -1 V and -2 V. As a result, the solar weighted reflectance, i.e., the averaged reflectance with considering solar spectrum (air mass 1.5), could be efficiently reduced for the electrochemically etched Si by applying the cathodic voltage of -2 V, which is expected to be useful for Si solar cell applications.

The Effect of Directivity of Antenna for the Evaluation of Abnormal Area Using Ground Penetrating Radar (지하투과레이더를 이용한 이상구간 평가 시 안테나 지향성의 영향)

  • Kang, Seonghun;Lee, Jong-Sub;Lee, Sung Jin;Park, Young-Kon;Hong, Won-Taek
    • Journal of the Korean Geotechnical Society
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    • v.33 no.11
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    • pp.21-34
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    • 2017
  • The ground penetrating radar (GPR) signal can be measured with different amplitudes according to the directivity, so the directivity of the antenna should be considered. The objective of this study is to investigate the directivity of antenna by analyzing the reflection characteristics of electromagnetic waves radiated from the antenna, and to evaluate effective range of angle that can inspect an abnormal area according to the directivity of antenna. For the measurement of the directivity, a circular metal bar is used as reflector and the signals are measured by changing the angle and the distance between reflector and antenna in the E- and H-plane. The boundary distance between the near field and the far field is determined by analyzing the amplitudes of reflected signals, and two points with different distances from each of near and far fields are designated to analyze radiation patterns in near and far fields. As a result of radiation pattern measurement, in the near field, minor lobes are observed at angle section at more than $50^{\circ}$ in both E- and H-plane. Therefore, antenna has the directivity for the direction of main lobe and minor lobes in near field. In the far field, antenna has the directivity for a single direction of main lobe because minor lobes are not observed. The amplitude of the signal reflected from the near field is unstable, but it can be distinguished from noise. Therefore, in the near field, the ground anomaly can be detected with high reliability. On the other hand, the amplitude of the signal reflected from the far field is stable, but it is hard to distinguish between reflected signal and noise because of the excessive loss of electromagnetic wave. The analyses of directivity in the near and the far fields performed in this study may be effectively used to improve the reliability of the analyses of abnormal area.