• Title/Summary/Keyword: Gravimetric method

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Estimation of the optimal heated inlet air temperature for the beta-ray absorption method: analysis of the PM10 concentration difference by different methods in coastal areas

  • Shin, So Eun;Jung, Chang Hoon;Kim, Yong Pyo
    • Advances in environmental research
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    • v.1 no.1
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    • pp.69-82
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    • 2012
  • Based on the measurement data of the particulate matter with an aerodynamic diameter of less than or equal to a nominal 10 ${\mu}m$ (PM10) by the ${\beta}$-ray absorption method (BAM) equipped with an inlet heater and the gravimetric method (GMM) at two coastal sites in Korea, the optimal inlet heater temperature was estimated. By using a gas/particle equilibrium model, Simulating Composition of Atmospheric Particles at Equilibrium 2 (SCAPE2), water content in aerosols was estimated with varying temperature to find the optimal temperature increase to make the PM10 concentration by BAM comparable to that by GMM. It was estimated that the heated air temperature inside the BAM should be increased up to $35{\sim}45^{\circ}C$ at both sites. At this temperature range, evaporation of volatile aerosol components was minor. Similar ($30{\sim}50^{\circ}C$) temperature range was also obtained from the calculation based on the absolute humidity which changed with ambient absolute humidity and chemical composition of hygroscopic species.

A Study on the Quantitative Measurement of Oil Carry-over in Natural Gas Vehicle fueling Station Using A Gravimetric Method (무게측정법을 이용한 천연가스 자동차 충전소 오일전이 정량 분석에 대한 연구)

  • Hwang, Sung-Soo;Oh, Jun-Seok;Kim, Ki-Dong;Oh, Young-Sam;Choi, Kyung-Sik;Kim, Hack-Eun
    • Journal of the Korean Institute of Gas
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    • v.19 no.1
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    • pp.12-17
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    • 2015
  • The core of the CNG fueling station is the compressor and most of CNG compressors in Korea require lubrication. Lubrication oil of CNG compressor that can be transferred into the pressure regulators and the engines of fueling system can cause a negative effect on NGV(Nature Gas Vehicle) performance during refueling due to oil Carry-over. In order to avoid the problem, it is necessary to enhance the quality of the compressed natural gas by measuring quantitatively the amount of the transferred oil. In this research, a sampling device and sampling tube were developed, which can be used with a gravimetric method of detection to measure CNG oil Carry-over. In addition, CNG samples were taken at 6 pre-selected CNG fueling stations and analysed for their trace oil Carry-over. The measured total oil Carry-over ranged from 2.569 to 6.509 ppm. This test measurements were compared with those of previous studies to verify the results.

A Study on the Measurement of Water Content in Hydrogel Contact Lens by Gravimetric Method (중량측정법에 의한 하이드로젤 콘택트렌즈의 함수율 측정에 관한 연구)

  • Kim, Tae-Hun;Ye, Ki-Hun;Sung, A-Young
    • Journal of Korean Ophthalmic Optics Society
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    • v.13 no.4
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    • pp.59-63
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    • 2008
  • Purpose: The purpose of this study is to understand a relation of water content measurement with two different method, water removal method and dry method. Methods: 72 hydrogel contact lens containing various water content (ranged from 47% to 58%) were measured by the gravimetric method at 20$^{\circ}C$and 21% of the humidity. We weighed the dried test specimen at room temperature for 30 min after cooling. Results: In dry blotting method, the water content was measured to 47.43${\pm}$8.48%. The water contents was measured to 48.15${\pm}$8.36% with wet blotting condition. It was found that wet blotting method showed the higher water content of about 7% than dry blotting method. In water content with two dry methods, each of results was measured by 47.89${\pm}$8.06% and 49.56${\pm}$7.06%. In case of microwave method, the water content was measured significantly higher water content of about 1.67% than vacuum oven method. However, no statistical difference was found (p>0.05). Conclusions: In water removal method (Dry blotting method and Wet blotting method) to weigh hydrated test specimen, wet blotting method showed significantly higher water content than dry blotting method. Also in case of dry methods (vacuum oven and microwave) to weigh dry test specimen, water content of microwave method showed higher water content than vacuum oven method, but it should be noted that microwave oven method must be used carefully to measure accurateness on the specimen position and wave power.

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Interpretation of Physical Properties of Marine Sediments Using Multi­Sensor Core Logger (MSCL): Comparison with Discrete Samples

  • Kim, Gil-Young;Kim, Dae-Choul
    • Journal of the korean society of oceanography
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    • v.38 no.4
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    • pp.166-172
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    • 2003
  • Multi­Sensor Core Logger (MSCL) is a useful system for logging the physical properties (compressional wave velocity, wet bulk density, fractional porosity, magnetic susceptibility and/or natural gamma radiation) of marine sediments through scanning of whole cores in a nondestructive fashion. But MSCL has a number of problems that can lead to spurious results depending on the various factors such as core slumping, gas expansion, mechanical stretching, and the thickness variation of core liner and sediment. For the verification of MSCL data, compressional wave velocity, wet bulk density, and porosity were measured on discrete samples by Hamilton Frame and Gravimetric method, respectively. Acoustic impedance was also calculated. Physical property data (velocity, wet bulk density, and impedance) logged by MSCL were slightly larger than those of discrete sample, and porosity is reverse. Average difference between MSCL and discrete sample at both sites is relatively small such as 22­24 m/s in velocity, $0.02­-0.08\;g/\textrm{cm}^3$ in wet bulk density, and 2.5­2.7% in porosity. The values also show systematic variation with sediment depth. A variety of factors are probably responsible for the differences including instrument error, various measurement method, sediment disturbance, and accuracy of calibration. Therefore, MSCL can be effectively used to collect physical property data with high resolution and quality, if the calibration is accurately completed.

Determination of Precise Regional Geoid Heights on and around Mount Jiri, South Korea

  • Lee, Suk-Bae
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.36 no.1
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    • pp.9-15
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    • 2018
  • Precise regional geoid heights on and around Mount Jiri were calculated and were compared to the KNGeoid14 (Korean National Geoid 2014) model. In this study, gravimetric geoid heights were calculated by using RCR (Remove-Compute-Restore) technique and then hybrid geoid heights were calculated by using the LSC (Least Square Collocation) method in the same area. In addition, gravity observation and GNSS(Global Navigation Satellite System) surveying performed in this study were utilized to determine gravimetric geoid heights and to compute hybrid geoid heights, respectively. The results of the study show that the post-fit error (mean and standard deviation) of hybrid geoid heights was evaluated as $0.057{\pm}0.020m$, while the mean and standard deviation of the differences were -0.078 and 0.085 m, respectively for KNGeoid14. Therefore, hybrid geoid heights in this study show more considerable progress than KNGeoid14.

Geoid Models Referred to the Bessel Ellipsoid of South Korea (벳셀타원체 기준의 남한지역 지오이드 모델(KGM95))

  • 이영진
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.13 no.2
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    • pp.125-133
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    • 1995
  • The geoidal heights of a country may be computed from astrogedetic, gravimetric or satellite data. In this paper, the geoid models to the Bessel ellipsoid(KGM95-A) have been determined by the astrogedetic method, which is surface fitting techniques using deflections of the vertical and geoid height constraints. Transformation equations and the gravimetric geocentric geoid(KGM93-C) were applied to obtain the geoid height referred to the Tokyo Datum of the Korean geodetic network, the comparison of the astrogedetic results and discussions of the geoid information were added.

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Corrosion Resistance Properties of Rice Husk Ash Blended Concrete

  • Ganesan, K.;Rajagopal, K.;Thangavel, K.
    • Corrosion Science and Technology
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    • v.6 no.1
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    • pp.12-17
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    • 2007
  • Portland cement incorporating supplementary cementing material develops excellent mechanical properties and long term durability characteristics. India is a leading rice producing country and rice husk is considered as waste in the rice milling industries. In this present work, the rice husk ash (RHA) was added to concrete as cement replacement from 0 to 30%. Corrosion performance of reinforcing steel embedded in RHA blended concretes was studied using linear polarization, AC impedance and gravimetric methods. The corrosion rate of steel bars embedded in RHA concretes were compared with control concrete. The results clearly indicate that the corrosion rate of reinforcing steel embedded in concrete is significantly reduced with the incorporation of RHA. A good correlation among gravimetric method and electrochemical methods was observed. Electrochemical impedance study showed 98 percentage reduction in corrosion rate to the RHA blended concrete with 15% replacement than control concrete.

A Comparison of the Gravimetric Geoid and the Geometric Geoid Using GPS/Leveling Data (GPS/Leveling 데이터를 이용한 기하지오이드와 중력지오이드의 비교 분석)

  • Kim, Young-Gil;Choi, Yun-Soo;Kwon, Jay-Hyoun;Hong, Chang-Ki
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.28 no.2
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    • pp.217-222
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    • 2010
  • The geoid is the level surface that closely approximates mean sea level and usually used for the origin of vertical datum. For the computation of geoid, various sources of gravity measurements are used in South Korea and, as a consequence, the geoid models may show different results. however, a limited analysis has been performed due to a lack of controlled data, namely the GPS/Leveling data. Therefore, in this study, the gravimetric geoids are compared with the geodetic geoid which is obtained through the GPS/Leveling procedures. The gravimetric geoids are categorized into geoid from airborne gravimetry, geoid from the terrestrial gravimetry, NGII geoid(geoids published by National Geographic Information Institute) and NORI geoid(geoi published by National Oceanographic Research Institute), respectively. For the analysis, the geometric geoid is obtained at each unified national control point and the difference between geodetic and gravimetric geoid is computed. Also, the geoid height data is gridded on a regular $10{\times}10-km$ grid so that the FFT method can be applied to analyze the geoid height differences in frequency domain. The results show that no significant differences in standard deviation are observed when the geoids from the airborne and terrestrial gravimetry are compared with the geomertric geoid while relatively large difference are shown when NGII geoid and NORI geoid are compared with geometric geoid. Also, NGII geoid and NORI geoid are analyzed in frequency domain and the deviations occurs in long-wavelength domain.

Hydrolysis of Rice Syrup Meal Using Various Commercial Proteases (쌀 시럽박의 단백질 가수분해 특성)

  • Kim, Chang-Won;Park, Jin-Woo;Choi, Hyuk-Joon;Han, Bok-Kyung;Yoo, Seung-Seok;Kim, Byung-Yong;Baik, Moo-Yeol;Kim, Young-Rok
    • Journal of Life Science
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    • v.21 no.2
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    • pp.309-315
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    • 2011
  • Rice syrup meal (RSM) was enzymatically hydrolyzed using eight commercial proteases (Protamex, Neutrase, Flavourzyme, Alcalase, Protease M, Protease N, Protease A, Molsin F) for 4 hr at optimum pH and temperature. Proteolytic hydrolysates were examined in supernatant and precipitate using Lowry protein assay, semimicro Kjeldahl method and gravimetric method using weight difference before and after enzymatic hydrolysis. Although RSM contains a high amount of protein (71.2%), only a very small amount of protein was hydrolyzed. Two proteases (Protease M and Protease N) were found to be the most effective in the hydrolysis of RSM protein. In Lowry method, 57.5 and 59.0 mg protein/g RSM were hydrolyzed after Protease M and Protease N treatments, respectively. In gravimetric method, 80.0 and 85.4 mg protein/g RSM were hydrolyzed after Protease M and Protease N treatments. In Kjeldahl method, 67.43 and 70.43 mg protein/g RSM were hydrolyzed after Protamex and Protease N treatments, respectively. For synergistic effect, two or three effective commercial proteases (Protease M, Protease N and Protease A) were applied to RSM at one time. The highest hydrolysis of RSM protein was observed in both Lowry protein assay (80.3 mg protein/g RSM) and gravimetric methods (153.2 mg protein/g RSM) when three commercial proteases were applied at one time, suggesting the synergistic effect of those proteases.

Studies on the Determination of Synthetic Food Colors (합성식용색소의 정량분석법에 관한 검토)

  • Om Ae-Son;Lee Heon-Ok;Shim Jae-Young;Shin Dong-Hwa;Kim Yong-Suk;Lee Young-Hwan;Bang Jeong-Ho;Shin Jae-Wook;Lee Tal-Soo;Hong Ki-Hyoung;Park Sung-Kwan;Choi Duck-Jang;Kim Hee-Yun
    • Journal of Food Hygiene and Safety
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    • v.20 no.2
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    • pp.73-76
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    • 2005
  • Center for Food Standard Evaluation, Korea Food and Drug AdministrationThis study was performed to compare analytical methods of nine synthetic food colors and six food color lakes in Korea, Japan, Joint FAO/WHO Expert Committee of Food Additives (JECFA), and USA. The experimental protocol of this study consists of three parts: titration method with titanium chloride, gravimetric and spectrophotometric method. To measure the total contents of food colors, Korea and Japan used titration method with titanium chloride, USA used the average value of titration method with titanium chloride equipped with Kipp generator and spectrophotometric method. Also, JECFA used titration method with titanium chloride equipped with KiPP generator. However, All the low organizations used gravimetric method to measure the total content of coloring matter on Food Red No.3. Although all organizations use various methods for analysis of coloring matters, total contents of coloring matter on food colors tested fell into the standard showing $85.08-96.40\%$ in synthetic food colors and $10.00-36.86\%$ in food color lakes.