• Title/Summary/Keyword: Granular material

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Characteristics of Electroplated Sn-2.5Cu Alloy Layers for Surface Finishing (표면마무리를 위한 Sn-2.5Cu 합금 도금막의 특성)

  • Kim, Ju-Youn;Bae, Kyoo-Sik
    • Korean Journal of Materials Research
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    • v.13 no.2
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    • pp.133-136
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    • 2003
  • Sn-2.5Cu alloy layers were deposited on the Alloy 42 lead-frame substrates by the electroplating method, and their microstructures, adhesion strength, and electrical resistivity were measured to evaluate the applicability of Sn-Cu alloy as a surface finishing material of electronic parts. The Sn-2.5Cu layers were electroplated in the granular form, and composed of pure Sn and Cu$_{6}$Sn$_{5}$ intermetallic compound. Surfaces of the electroplated Sn-2.5Cu layers were rather rough and also the thickness variance was large. The adhesion strength of the Sn-2.5Cu electroplated layers was highly comparable to that of the electroplated Cu alloy layer and the electrical conductivity was about 10 times higher than the pure Sn. After the 20$0^{\circ}C$ 30 min. annealing of the electroplated Sn-2.5Cu layers, the surface roughness was reduced, and adhesion strength and conductivity were improved. These results showed the Sn-Cu alloys can be used as an excellent surface finishing material.ial.

Effect of nitrogen concentration on the microstructures of AlN thin films fabricated by reactive RF sputtering (반응성 RF 마그네트론 스퍼터링으로 증착한 AlN 박막의 특성에 질소농도 변화가 미치는 영향)

  • Lim, Dong-Ki;Kim, Byoung-Kyun;Jeong, S.W.;Roh, Yong-Han
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2008.06a
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    • pp.367-367
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    • 2008
  • Aluminum nitride (AlN) thin films have been deposited on Si substrate by using reactive RF magnetron sputtering method in a gas mixture of Ar and $N_2$ at different $N_2$ concentration. It was found that $N_2$ concentration was varied in the range up to 20-100%, highly c-axis oriented film can be obtained at 50% $N_2$ with full width at half maximum (FWHM) $4.5^{\circ}$. Decrease in surface roughness from 7.5 nm to 4.6 nm found to be associated with decrease in grain size, with $N_2$ concentration; however, the AlN film fabricated at 20% $N_2$ exhibited a granular type of structure with non-uniform grains. The absorption peak was observed around 675 $cm^{-1}$ in fourier transform infrared spectroscopy (FTIR). It is concluded that the AlN film deposited at $N_2$ concentration of 50% exhibited the most desirable properties for the application of high-frequency surface acoustic devices.

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Assessment of recycled concrete aggregates as a pavement material

  • Jayakody, Shiran;Gallage, Chaminda;Kumar, Arun
    • Geomechanics and Engineering
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    • v.6 no.3
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    • pp.235-248
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    • 2014
  • Population increase and economic developments can lead to construction as well as demolition of infrastructures such as buildings, bridges, roads, etc resulting in used concrete as a primary waste product. Recycling of waste concrete to obtain the recycled concrete aggregates (RCA) for base and/or sub-base materials in road construction is a foremost application to be promoted to gain economical and sustainability benefits. As the mortar, bricks, glass and reclaimed asphalt pavement (RAP) present as constituents in RCA, it exhibits inconsistent properties and performance. In this study, six different types of RCA samples were subjected classification tests such as particle size distribution, plasticity, compaction test, unconfined compressive strength (UCS) and California bearing ratio (CBR) tests. Results were compared with those of the standard road materials used in Queensland, Australia. It was found that material type 'RM1-100/RM3-0' and 'RM1-80/RM3-20' samples are in the margin of the minimum required specifications of base materials used for high volume unbound granular roads while others are lower than that the minimum requirement.

Influence of Residual Oxygen on the growth of AlN Thin Films with Substrate Temperature (기판 온도 변화에 따른 AlN 박막 성장에 잔류 산소가 미치는 영향)

  • Kim, Byoung-Kyun;Lee, Eul-Tack;Kim, Eung-Kwon;Jeong, Seok-Won;Roh, Yong-Han
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.5
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    • pp.463-467
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    • 2008
  • Aluminum nitride (AlN) thin films have been deposited on Au electrodes by using reactive RF magnetron sputtering method in a gas mixture of Ar and $N_2$ at different substrate temperature. It was found that substrate temperature was varied in the range up to $400^{\circ}C$, highly c-axis oriented film can be obtained at $300^{\circ}C$ with full width at half maximum (FWHM) $3.1^{\circ}$. Increase in surface roughness from 3.8 nm to 5.9 nm found to be associated with increase in grain size, with substrate temperature; however, the AlN film fabricated at $400^{\circ}C$ exhibited a granular type of structure with non-uniform grains. The Al 2p and N 1s peak in the X-ray photoelectron spectroscopy (XPS) spectrum confirmed the formation of Al-N bonds. The XPS spectrum also indicated the presence of oxynitrides and oxides, resulting from the presence of residual oxygen in the vacuum chamber. It is concluded that the AlN film deposited at substrate temperature of $300^{\circ}C$ exhibited the most desirable properties for the application of high-frequency surface acoustic devices.

Effect of Process Parameters on the Morphology and Size of Spray-Dried Granule Powder for Fabrication of SiAlON Raw Material (SiAlON 원료분말제조를 위한 분무건조 과립분말의 형상과 크기에 미치는 공정변수효과)

  • Choi, Jae-Hyeong;Lee, Soyul;Han, Yoonsoo;Lee, Sung-Min;Nahm, Sahn;Kim, Seongwon
    • Korean Journal of Materials Research
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    • v.27 no.12
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    • pp.716-721
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    • 2017
  • SiAlON-based ceramics are some of the most typical ceramic materials used as cutting tools for HRSA(Heat Resistant Super-Alloys). SiAlON can be fabricated using ceramic processing, such as mixing, granulation, compaction, and sintering. Spray drying is a widely-used method for producing a granular powder of controlled morphology and size with flowability. In this study, we report a systematic investigation aimed at optimizing spherical granule morphology by controlling spray-drying parameters such as gas flow and feed rate. Before spray drying, the viscosities of the raw material slurries were also optimized with the amount of dispersant added.

Optimization of Synthesis Condition for Nanoscale Zero Valent Iron Immobilization on Granular Activated Carbon (영가철이 고정된 입상활성탄 제조를 위한 최적 합성조건 도출)

  • Hwang, Yuhoon;Mines, Paul D.;Lee, Wontae;Andersen, Henrik R.
    • Journal of Korean Society of Environmental Engineers
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    • v.38 no.9
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    • pp.521-527
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    • 2016
  • Nanoscale zero valent iron (nZVI) has been intensively studied for the treatment of a plethora of pollutants through reductive reaction, however, the nano size should be of concern when nZVI is considered for water treatment, due to difficulties in recovery. The loss of nZVI causes not only economical loss, but also potential risk to human health and environment. Thus, the immobilization onto coarse or structured support is essential. In this study, two representative processes for nZVI immobilization on granular activated carbon (GAC) were evaluated, and optimized conditions for synthesizing Fe/GAC composite were suggested. Both total iron content and $Fe_0$ content can be significantly affected by preparation processes, therefore, it was important to avoid oxidation during preparation to achieve higher reduction capacity. Synthesis conditions such as reduction time and existence of intermediate drying step were investigated to improve $Fe_0$ content of Fe/GAC composites. The optimal condition was two hours of $NaBH_4$ reduction without intermediate drying process. The prepared Fe/GAC composite showed synergistic effect of the adsorption capability of the GAC and the degradation capability of the nZVI, which make this composite a very effective material for environmental remediation.

Numerical Study of Settlement Reduction Ratio for the Bottom Ash Mixture Compaction Pile (수치해석적 방법에 의한 저회혼합다짐말뚝의 침하저감비에 관한 연구)

  • Chu, Ickchan;Kim, Gooyoung;Do, Jongnam;Cho, Hyunsoo;Chun, Byungsik
    • Journal of the Korean GEO-environmental Society
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    • v.13 no.3
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    • pp.53-58
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    • 2012
  • In general, sand compaction pile(SCP) method and gravel compaction pile(GCP) method have been mainly used to reinforce soft soils such as soft clay or loose sandy ground. But the sand compaction pile method has problems such as lack of sand supply and destroying the nature while collecting sand, the gravel compaction pile method has a problem such as decreased permeability of the drainage material due to clogging. Recently, the study to replace sand with bottom ash which has similar engineering properties with sand is in active. As a fundamental research on bottom ash mixture compaction pile utilizing bottom ash, its behavioral characteristics depending on granular materials and replacement ratio has been simulated numerically. In particular, Settlement Reduction Ratio(SRR) according to the distance from the center of pile was calculated. The main findings were as follows. Change values of Mixture Compaction Pile's SRR according to granular materials showed similar patterns and stiffness of the composite soil is increased depending on the replacement ratio so SRR showed decreased patterns. Especially, when the replacement ratio is in 20~40%, it increase significantly. When the replacement ratio is over 40%, it increase slowly. When considering the economics, 30~40% replacement ratio is appropriate.

Oxyphilic Papillary Carcinoma of the Thyroid in Fine Needle Aspiration (갑상선의 호산성 유두상 암종의 세침흡인 세포학적 소견)

  • Kim, Young-Min;Gong, Gyung-Yub;Kim, On-Ja
    • The Korean Journal of Cytopathology
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    • v.8 no.1
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    • pp.52-56
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    • 1997
  • Oxyphilic (Hurthle) cells have abundant eosinophilic granular cytoplasms and occur in both benign and malignant neoplasms of the thyroid gland. Most published studies described mainly oxyphilic tumors of follicular type, and reports on oxyphilic papillary thyroid carcinomas are rare. The oxyphilic variant of papillary carcinoma differs from the classic papillary carcinoma in its more aggressive biological behavior. We report a case of oxyphilic papillary carcinoma exhibiting exclusively oxyphilic cells in a follicular pattern without papillary structures. The pattern of papillary carcinoma was confirmed by fine needle aspiration material and lymph nodal metastasis, both of which revealed typicaled papillary structures with characteristic nuclear features, psammoma bodies, and oxyphilic cytoplasm.

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Characterizing the geotechnical properties of natural, Israeli, partially cemented sands

  • Frydman, Sam
    • Geomechanics and Engineering
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    • v.3 no.4
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    • pp.323-337
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    • 2011
  • Israel's coastal region consists, mainly, of Pleistocene and Holocene sands with varying degrees of calcareous cementation, known locally as "kurkar". Previous studies of these materials emphasized the difficulty in their geotechnical characterization, due to their extreme variability. Consequently, it is difficult to estimate construction stability, displacements and deformations on, or within these soils. It is suggested that SPT and Menard pressuremeter tests may be used to characterize the properties of these materials. Values of elastic modulus obtained from pressuremeter tests may be used for displacement analyses at different strain levels, while accounting for the geometric dimensions (length/diameter ratio) of the test probe. A relationship was obtained between pressuremeter modulus and SPT blow count, consistent with published data for footing settlements on granular soils. Cohesion values, for a known friction angle, are estimated, by comparing field pressuremeter curves to curves from numerical (finite element or finite difference) analyses. The material analyzed in the paper is shown to be strain-softening, with the initial cohesion degrading to zero on development of plastic shear strains.

Determination of Opening Size of Geotextiles (토목섬유의 유효구멍크기 측정방법 및 측정결과 평가)

  • Cho, Sam-Deok;Kim, Ju-Hyong;Lee, Kwang-Wu
    • Proceedings of the Korean Geotechical Society Conference
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    • 2006.03a
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    • pp.111-120
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    • 2006
  • Opening size of 3 types of geotextile were tested using dry and wet sieving methods to evaluate characteristics of test methods and to compare the test results. Judging from test results, dry sieving method is a poor test, having many problems causing many errors but a simple-quick test. Wet sieving method is a very specific test avoiding many of the problems of dry sieving such as electrostatic charges, trapping in the geotextiles and so on. However, one of wet sieving tests, KSK ISO12956, takes long time to complete a test and is too strict to handle loss of granular material. Generally, opening size of a geotextile by wet sieving test is smaller than that of dry sieving test. Especially, opening size by KSF 2126 which is one of wet sieving test but disused at present anymore is similar or smaller than that by KSK ISO12956 method.

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