• Journal of Conservation Science
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• 제28권3호
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• pp.205-216
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• 2012

65 samples of glass bead excavated from Mahan tombs of Asan Bakjimeure site consists of 13 of potash glass group and 52 of soda glass group and soda glass is superior in numbers. When classified according to color, purple blue glass bead is accompanied potash and soda glass group whereas purple glass bead is potash glass group and red, greenish blue, green and gold foil glass bead is soda glass group. Purple blue glass bead is classified as LCA type in which the content of the stabilizer is low. Of this, the soda glass categorized as LMK type with low content of MgO and $K_2O$ is determined that natron is used as the raw material. As to red glass, the homogeneous glass is LCA-B/HMK type and the heterogeneous glass is HCLA/LMK type. Thus, each of these two types are likely to be used plant ash and natron respectively. Greenish blue and green glass depends of the type that round glass is LCA-A/LMHK type and the segmented glass is LCA-B/HMK type. The gold foil glass bead is manufactured by the purity of 19.9~22.6K gold foil and the soda glass of HCLA/LMK type. In other words, the most of the glass bead of Asan Bakjimeure site is similar to the composition of the glass confirmed in other sites of the Baekche period. On the other hand, the greenish blue and green segmented bead and some red round bead is a different chemical composition is considered that the difference in raw materials. These characteristics is expected to be an important evidence for the understanding of the trade system of the ancient glass.

• Restorative Dentistry and Endodontics
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• 제18권1호
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• pp.1-26
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• 1993

The purpose of this study was to investigate the effect of acid etching on the surface appearance and fracture toughness of five glass ionomer cements. Five kinds of commercially available glass ionomer cements including chemical curing filling type, chemical curing lining type, chemical curing metal reinforced type, light curing tilling type and light curing lining type were used for this study. The specimens for SEM study were fabricated by treating each glass ionomer cement with either visible light curing or self curing after being inserted into a rubber mold (diameter 4mm, depth 1mm). Some of the specimens were etched with 37% phosphoric acid for 0, 15, 30, 60, go seconds, at 5 minutes, 1 hour and 1 day after mixing of powder and liquid. Unetched ones comprised the control group and the others were the experimental groups. The surface texture was examined by using scanning electron microscope at 20 kV. (S-2300, Hitachi Co., Japan). The specimens for fracture toughness were fabricated by curing of each glass ionomer cement previously inserted into a metal mold for the single edge notch specimen according to the ASTME399. They were subjected to a three-point bend test after etching for 0, 30, 60, and 90 seconds at 5 minutes-, 1 hour-and 1 day-lapse after the fabrication of the specimens. The plane strain fracture toughness ($K_{IC}$) was determined by three-point bend test which was conducted with cross-head speed of 0.5 mm/min using Instron universal testing machine (Model No. 1122) following seven days storage of the etched specimens under $37^{\circ}C$, 100% humidity condition. Following conclusions were drawn. 1. In unetched control group, crack was present, but the surface was generally smooth. 2. Deterioration of the surface appearance such as serious dissolving of gel matrix and loss of glass particles occured as the etching time was increased beyond 15 s following Immediate etching of chemical curing type of glass ionomer cements. 3. Etching after 1 h, and 1 d reduced surface damage, 15 s, and 30s etch gave rough surface appearance without loss of glass particle of chemical curing type of glass ionomer cements. 4. Light curing type glass ionomer cement was etched by acid, but there was no difference in surface appearances according to various waiting periods. 5. It was found that the value of plane stram fracture toughness of glass ionomer cements was highest in the light curing filling type as $1.79\;MNm^{-1.5}$ followed by the light curing lining type, chemical curing metal reinforced type, chemical curing filling type and chemical curing lining type. 6. The value of plane stram fracture toughness of the chemical curing lining type glass ionomer cement etched after 5 minutes was lower than those of the cement etched after 1 hour or day or unetched (P < 0.05). 7. Light curing glass ionomer cement showed Irregular fractured surface and chemical curing cement showed smooth fractured surface.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 한국소성가공학회 2009년도 춘계학술대회 논문집
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• pp.374-377
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• 2009

Glass fiber reinforced nylon has been used in many plastic industries. Mechanical properties of reinforced plastics depend upon types of glass fiber as well as loading of glass fiber. Tensile properties of glass fiber reinforced nylon66 have been studied for different glass fiber types and sizes. Types of glass fibers were circular and flat, and diameters were 7, 10, and 13 micrometers. Orientations of glass fibers in the matrix of nylon66 have been analyzed through X-ray CT. Tensile specimens were prepared by cutting out of square plates of $100{\times}100{\times}3mm$ with different angles such as 0, 45, and $90^{\circ}$ to the flow direction. As the loading of glass fiber increases to 45 wt% tensile strength increases up 2.5 times compare with neat nylon66. Anisotropic tensile strength has been observed and minimum tensile strength was measured in the specimen cut from perpendicular to the flow direction.

• Journal of the Korean Society for Precision Engineering
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• 제11권4호
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• pp.165-173
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• 1994

Retroreflector is different from other reflecting surfaces as it mades reflection in which radiation is returned in directions close to its incoming direction. Because of this characteristics, retroreflectors find many applications in traffic safety related areas. Retroreflectors are usually made using comer cubes, or partially coated glass beads. These glass beads can be made very small, so that they can be coated on sheets or mixed with paints. The design of glass type retroreflector depends on glass bead's shape and material, and its optical characteristics are related to the refractive index of glass. In this paper, a method of anlyzing glass bead type retroreflector's sptical characteristics with respect to shape and optica property of the glass, is presented. First, the coefficient of retroreflection, which is a measure of retroreflector's optical characteristics, is derived analytically using geometrical optics method. And the result is plotted using numerical methods. The results show good match with those obtained experimentally, which were supplied from a commercial retroreflector manufacturer.

• Journal of the Korean Wood Science and Technology
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• 제42권5호
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• pp.571-578
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• 2014

As a way of developing wooden joint development, a glass fiber reinforced wood plate was manufactured to replace a steel plate. Also, the fracture toughness was evaluated. Through application to a cantilever-type specimen made of a column and a beam, the moment resistance performance was evaluated. For the fracture toughness specimen of the wood plate, 12 types were manufactured by varying the combination of a main member (veneer and plywood) and reinforcement (glass fiber sheet and glass fiber cloth). The results of the fracture toughness test indicated that the 5% yield load of the specimen using plywood was 18% higher than that of the specimen using veneer, and that the specimen reinforced by inserting glass fiber sheets between testing materials (Type-3-PS) had the highest average 5% yield load 4841 N. Thus, a moment resistance strength test was performed by applying Type-3-PS to a column-beam joint. The results of the test indicated that compared to the specimen using a steel plate and a drift pin (Type-A), the maximum moment ratio of the specimen using a glass fiber reinforced wood plate (Type-3-PS) and a drift pin (Type-B) was 0.79; and that a rupture occurred in the wood plate due to high stiffness of the drift pin. The maximum moment ratio of the specimen using a glass fiber reinforced wood plate (Type-3-PS) and a glass fiber reinforced wooden laminated pin (Type-C) was 0.67, which showed low performance. However, unlike Type-A, a ductile fracture occurred on Type-C, and the load gradually decreased even after the maximum moment.

• Ceramist
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• 제22권4호
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• pp.429-451
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• 2019

Quartz glass is a key material for making semiconductor process components because of its purity, low thermal expansion, high UV transmittance and relatively low cost. Domestic quartz glass has a market worth about 500 billion won in 2018, and the market power of Japanese materials is very high. Quartz glass for semiconductor process can be divided into general process and exposure. For general process, molten quartz glass is mainly used, but synthetic quartz glass with higher purity is preferred. Synthetic quartz glass is used as the photomask for the exposure process. Recently, as semiconductors started the sub-nm process, the transition from the transmission type using ArF ultraviolet (194 nm) to the reflection type using EUV ultraviolet (13.5 nm) began. Therefore, the characteristics required for the synthetic quartz glass substrates used so far are also rapidly changing. This article summarizes the current technical trends of quartz glass and recent technical issues. Lastly, the present situation and development possibility of quartz glass technology in Korea were diagnosed.

• Journal of the Korean Wood Science and Technology
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• 제39권2호
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• pp.156-162
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• 2011

To evaluate the bonding performance of reinforced glulam, the textile type of glass fiber and aramid fiber, and the sheet type of glass fiber reinforced plastic (GFRP) and carbon fiber reinforced plastic (CFRP) were used as reinforcements. The reinforced glulam was manufactured by inserting reinforcement between the outmost and middle lamination of 5ply glulam. The types of adhesives used in this study were polyvinyl acetate resins (MPU500H, and MPU600H), polyurethane resin and resorcinol resin. The block shear strengths of the textile type in glass fiber reinforced glulam using MPU500H and resorcinol resin were higher than 7.1 N/$mm^2$, and these glulams passed the wood failure requirement of Korean standards (KS). In case of the sheet types, GFRP reinforced glulams using MPU500H, polyurethane resin and resorcinol resin, and CFRP reinforced glulams using MPU500H and polyurethane resin passed the requirement of KS. The textile type of glass fiber reinforced glulam using resorcinol resin after water and boiling water soaking passed the delamination requirement of KS. The only GFRP reinforced glulam using MPU500H after water soaking passed the delamination requirement of KS. We conclude that the bonding properties of adhesive according to reinforcements are one of the prime factors to determine the bonding performance of the reinforced glulam.

• Resources Recycling
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• 제13권1호
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• pp.54-58
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• 2004

Wollastonite-type glass ceramics were prepared by milling and firing at various temperatures using an automobile waste glass and waste shell as starting materials. Powder mixture ground by disk-type ball mill for 3 hours was pressed into a disk. The pressed specimen was fired at $850^{\circ}C$,$950^{\circ}C$ and $1050^{\circ}C$ for 1 hour in air. From FE-SEM observation, with an increase of the firing temperature from $850^{\circ}C$ to $1050^{\circ}C$, whisker-type phase was grown to about 10 $\mu\textrm{m}$ in length. Specimen fired at $1050^{\circ}C$ showed the formation of well-crystallized whisker-type wollastonite grains and the highest compressive strength.

• Laser Solutions
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• 제14권1호
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• pp.25-29
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• 2011

Micromachining of photosensitive glass by UV exposure, heat treatment, and etching processes is reported. Like photoresist, the photosensitive glass is also classified into positive and negative types by development characteristics. For the positive type, the exposed area is crystallized and etched away during the etching process in HF solution, whereas the unexposed area is crystallized and etched away for the negative type. The crystallized area of the photosensitive glass has an etch rate approximately 30~100 times faster than that of the amorphous area so that it becomes possible to fabricate microstructures in the glass. Based on the unique properties of glass such as high optical transparency, electrical insulation, and chemical/thermal stability, the glass micromachining technique introduced in this work could be widely applied to various devices in the fields of electronics, bio engineering, nanoelectonics and so on.

• Journal of the Korean Wood Science and Technology
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• 제43권4호
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• pp.463-469
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• 2015

In this study, to improve bending strength performance of Korean white pine, we made the curved composite glulam that was reinforced with glass fiber materials and larch lamina. Five types of Korean white pine curved glulams were made depending on whether they had been reinforced or not and how they had been reinforced. Type-A, reference specimen, was produced only with Korean white pine lamina, and Type-B was with larch lamina in the same thickness. Type-C was made by inserting a glass fiber cloth of textile shape between the each layer. Type-D was reinforced with two glass fiber cloths, which were placed inside and outside of the outermost lamina. Type-E was reinforced with GFRP sheet in the same way as Type-D. As a result of this bending strength test, the modulus of rupture (MOR) of Type-B, Type-C and Type-E were increased by 29%, 6%, and 48% in comparison with Type-A. However, MOR of Type-D was decreased by 2% in comparison with Type-A. In the failure modes, Type-A, Type-B and Type-C were totally fractured at the maximum load. However, load values of Type-D and Type-E decreased slowly because of reinforcement of fracture suppression, and the GFRP sheet (Type-E) had better reinforcing effect on compressive stress and tensile stress than the glass fiber cloth (Type-D).