• 한국결정성장학회지
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• 제26권1호
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• pp.28-34
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• 2016

원적외선 방사세라믹은 인체의 피부 안쪽으로 깊숙이 적외선을 침투시켜 온열 및 치료환경을 주는 매력적인 재료로써, 열적 치료 장치, 온열 매트, 히터 등과 같은 분야에 많은 응용이 되고 있다. 본 연구에서는 소결 온도와 시간을 변화시킴으로써 높은 방사율을 가지는 원적외선 방사세라믹의 소결 조건을 최적화하고자 하였다. 원적외선 방사체의 상 분석은 XRD로, 그 파단면의 미세구조는 SEM을 이용하여 분석하였다. 원적외선 방사율의 측정은 FT-IR으로 행하여, 결과를 종합적으로 해석하여 소결체의 최적 공정 조건을 확립하였다.

• 한국해양공학회지
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• 제25권4호
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• pp.66-71
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• 2011

The flexural strength of $MoSi_2$ based composites reinforced with Nb sheets has been investigated, based on the detailed examination of their microstructure and fractured surface. Both sintered density and porosity of Nb/$MoSi_2$ composites were also examined. Nb/$MoSi_2$ composites were fabricated by different conditions such as temperature, applied pressure and its holding time, using a hot-press device. The volume fraction of Nb sheet in this composite system was fixed as 10%. The characterization of Nb/$MoSi_2$ composites were investigated by means of optical microscopy, scanning electron microscope and three point bending test. Nb/$MoSi_2$ composites represented a dense morphology at the interfacial region, accompanying the creation of two types of reaction layer by the chemical reaction of Nb and $MoSi_2$. Nb/$MoSi_2$ composites possessed an excellent density at the fabricating temperature of $1350^{\circ}C$, corresponded to about 95% of theoretical density. The flexural strength of Nb/$MoSi_2$ romposites were greatly affected by the pressure holding time at the same fabricating temperature, owing to the large suppression of porosity in the microstructure. Especially, Nb/$MoSi_2$ composites represented a good flexural strength of about 310 MPa at the fabricating condition of $1350^{\circ}C$, 30MPa and 60min, accompanying the pseudo-ductile fracture behavior by the deformation of Nb sheet and the interfacial delamination.

• 한국전기전자재료학회논문지
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• 제27권11호
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• pp.712-717
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• 2014

Glass ceramic has a high mechanical strength and low sintering temperature. So, it can be used as a thick film substrate or a high strength insulator. A series of glass ceramic samples based on MgO-$Al_2O_3-SiO_2-ZrO_2$ (MASZ) were prepared by melting at $1,600^{\circ}C$, roll-quenching and heat treatment at various temperatures from $900^{\circ}C$ to $1,400^{\circ}C$. Dependent on the heat treatment temperature used, glass ceramics with different crystal phases were obtained. Their nucleation behavior, microstructure and mechanical properties were investigated with differential thermal analysis (DTA), X-ray diffraction (XRD), scanning electron microscopy (SEM), and Vicker's hardness testing machine. With increasing the heat treatment temperature of MASZ samples, their hardness and toughness initially increase and then reach the maximum points at $1,300^{\circ}C$, and begin to decrease at above this temperature, which is likely to be due to the softening of glass ceramics. As the content of $ZrO_2$ in MAS glass ceramics increases from 7.0 wt.% to 13 wt.%, Vicker's hardness and fracture toughness increase from $853Kg/mm^2$ to $878Kg/mm^2$ and $1.6MPa{\cdot}m^{1/2}$ to $2.4MPa{\cdot}m^{1/2}$ respectively, which seems to be related with the nucleation of elongated phases like fiber.

• 한국분말재료학회지
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• 제5권2호
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• pp.98-110
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• 1998

$Ti_{52}Al_{48}$ and $(Ti_{52}Al_{48})_{100-x}B_x(x=0.5, 2, 5)$ alloys have been Produced by mechanical milling in an attritor mill using prealloyed powders. Microstructure of binary $Ti_{52}Al_{48}$ powders consists of grains of hexagonal phase whose structure is very close to $Ti_2Al$. $(Ti_{52}Al_{48})_{95}B_5$ powders contains TiB2 in addition to matrix grains of hexagonal phase. The grain sizes in the as-milled powders of both alloys are nanocrystalline. The mechanically alloyed powders were consolidated by vacuum hot pressing (VHP) at 100$0^{\circ}C$ for 2 hours, resulting in a material which is fully dense. Microstructure of consolidated binary alloy consists of $\gamma$-TiAl phase with dispersions of $Ti_2AlN$ and $A1_2O_3$ phases located along the grain boundaries. Binary alloy shows a significant coarsening in grain and dispersoid sizes. On the other hand, microstructure of B containing alloy consists of $\gamma$-TiAl grains with fine dispersions of $TiB_2$ within the grains and shows the minimal coarsening during annealing. The vacuum hot pressed billets were subjected to various heat treatments, and the mechanical properties were measured by compression testing at room temperature. Mechanically alloyed materials show much better combinations of strength and fracture strain compared with the ingot-cast TiAl, indicating the effectiveness of mechanical alloying in improving the mechanical properties.

• 터널과지하공간
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• 제17권6호
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• pp.438-447
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• 2007

본 기술보고서는 Lisbon에서 개최된 2007 ISRM Congress에서 발표된 논문을 소개한 것이다. 이는 SRM(합성암반체)에 관한 연구결과이며, 이의 중요성과 향후 잠재력을 강조하고 있는 Fairhurst 교수가 직접 발표한 논문이다. 절리 암반의 특성을 규명하는 SRM 접근법은 현존하는 경험적 접근법이나 절리 암반의 거동에 대한 현재의 이해정도와 관련지어 재검토된다. 이 재검토 논문에서 절리 암반의 역학적 거동에 영향을 미치는 주요 요소들이 어떻게 고려되는가를 기술하며, 또 SRM 접근법이 상당히 발전되어 현장에 적용된 사례를 보여준다. PFC-3D에서 BP 모델링과 DFN 모사법 등의 두개의 잘 정립된 방법에 기초를 두고 있는 이 기법은 새로운 미끄러지는 절리모델을 사용한다. 이 모델은 모든 응력경로에 의하여 힘을 받고 있는 수천개의 기존 절리를 포함하는 대규모 암반체를 모사할 수 있게 하는 것이다. 암반의 강도 및 취성도, 완전 순응 행렬의 전개, 그리고 초기의 파쇄 등이 SRM 시험에서 얻어지는 결과이다.

• 한국재료학회지
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• 제20권7호
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• pp.379-384
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• 2010

The usual ceramic process of mixing and milling in state of oxides $ZrO_2$ and $CeO_2$ was adopted in this study in a wet process to manufacture Ce-TZP. $CeO_2$-$ZrO_2$ ceramics containing 8~20 mol% $CeO_2$ were made by heat treatment at $1250\sim1500^{\circ}C$ for 5hr. The maximum dispersion point of every slurry manufactured with a mixture of $ZrO_2$ and $CeO_2$ was neat at pH10. A stable slurry with average particle size of 90 nm can be manufactured when it is dispersed with the use of ammonia water and polycarboxylic acid ammonium. The sintered Ce-TZP ceramics manufactured with the addition of $CeO_2$ in a concentration of less than 10 mol% progressed to the fracture of the specimen due to the existence of a monoclinic phase of more than 30% at room temperature. More than 99% of the tetragonal phase was created for the sintered body with the addition of $CeO_2$ beyond 18 mol%, but the degradation of the mechanical properties on the entire specimen was brought about due to the $CeO_2$ existing in a percentage above 3%. Consequently, the optimal Ce-TZP level combined in the oxide state was identified to be 16 mol% of $CeO_2$ contents.

• Composites Research
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• 제26권5호
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• pp.328-333
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• 2013

본 연구에서는 유리섬유/폴리프로필렌 복합재료 고정판을 인조골에 체결하여 실제 골절치료 시술 상황을 모사하였으며, 고정판의 적합성을 판단하기 위하여 수분 흡수율, 스크류의 체결 상태, 하중 조건의 변화에 따른 피로 실험을 진행하였다. 실험 결과 0~12주 동안 수분 흡수가 이루어진 모든 시편에서 기대 수명인 65만 사이클을 넘는 100만 사이클 이상의 피로 수명을 가짐을 확인하였다. 스크류 체결 상태는 골절부의 변형률 차이에 주목할만한 영향을 미치지 못하였다. 본 논문에서는 유리섬유/폴리프로필렌 복합재료 고정판을 다양한 환경조건 하에서 압축-압축 피로실험을 수행하여 기계적 우수성을 입증하였으며, 이 결과는 향후 금속 고정판을 복합재료 고정판으로 대체하기 위한 관련 연구에 유용한 정보를 제공할 것으로 기대된다.

• 한국정보디스플레이학회:학술대회논문집
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• 한국정보디스플레이학회 2008년도 International Meeting on Information Display
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• pp.1441-1444
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• 2008

We developed ultra-accelerated quantum chemical molecular dynamics and spectroscopic characterization simulators for development of PDP materials. By combination of these simulators, realistic structure of PDP materials is drawn on the computer. Furthermore, based on the structures, various properties such as cathode luminescence spectrum and secondary electron emission, is successfully evaluated. The strategy of "Experiment integrated Computational Chemistry" using developed simulators will presented that has the potential in being powerful tool for designing the PDP materials.

• Composites Research
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• 제32권6호
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• pp.360-367
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• 2019

자전거 프레임 및 산업 부품과 같은 다양한 산업 분야에 PETG 열가소성 복합 재료를 적용하려면 제조 된 복합 재료의 내충격성, 내구성, 기계적 특성 및 3D 분석을 안정성 검증이 필수적이다. 본 연구에서는 비정질 수지인 PETG 수지의 기계적 특성, 내구성 및 내충격성을 향상시키기 위해 다양한 질량분율의 POE(폴리올레핀 엘라스토머)를 보강하여 화합물 및 사출 성형 공정을 수행 하였다. POE질량분율에 따른 PETG 열가소성 복합재의 열적 및 기계적 특성 및 샤르피 충격 강도 등에 대한 분석을 수행 하였다. 열적 및 기계적 특성 분석 결과, POE 소재가 첨가 된 PETG 열가소성 복합재의 경우 열적 및 기계적 특성이 감소하는 경향이 있지만 내충격성이 우수한 경향을 나타내었고, POE첨가에 따른 3D 전산해석 결과, 파손여부 없이 우수한 안정성을 나타내었다.

• 한국안전학회지
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• 제28권4호
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• pp.26-32
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• 2013

A digital image correlation(DIC) method is a whole-field measurement technique that acquires surface displacements and strains from images information which characterized a random speckle as intensity grey levels. Recently years, this DIC method is being developed and used increasingly in various research. In this study, we tried to apply to aluminum alloy(Al 6061-T6) using DIC method and strain gauge. DIC results demonstrated the usefulness and ability to determine a strain. The test specimen used in this study was an aluminum alloy(Al 6061-T6, thickness 1 mm). For a strain measurement, a strain gauge was attached at the center of a specimen. A specimen was lightly sprayed with a white paint and a black dot pattern was sprayed on its fully dried white surface to obtain a random speckle. The experimental apparatus used to perform the tensile test consisted of universal dynamic tester(5 kN; T.O. Co.) under displacement speed of 0.5, 1.0 and 3.0 mm/min. A Model 5100 B Scanner(V. Co.) used to obtain a strain. A CCD camera connected to a PC uses to record the images of the specimen surface. After acquisition, the images were transferred to PC where the DIC software was implemented. An acquired image was evaluated by the DIC program. DIC method for displacement and strain was suggests and it results show a good consistent remarkably. DIC results demonstrated the usefulness and ability to determine surface strain was better than by using classical measurements. The strain field measurement using a DIC is so useful that it can be applied to map strain distributions at a full area. DIC method can evaluate a strain change so it can predict a location of fracture. The findings of the investigation suggest that the DIC method is an efficient and reliable tool for full-field monitoring and detailed damage characterization of materials.