• Title/Summary/Keyword: Fracture Resistance Behavior

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Electrochemical and Cavitation-Erosion Characteristics of Duplex Stainless Steels in Seawater Environment (해수 환경에서 듀플렉스 스테인리스강의 전기화학적 거동 및 캐비테이션 특성)

  • Heo, Ho-Seong;Kim, Seong-Jong
    • Corrosion Science and Technology
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    • v.20 no.6
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    • pp.466-474
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    • 2021
  • A wet type scrubber for merchant vessel uses super austenitic stainless steels with pitting resistance equivalent number (PREN) of 40 or higher for operation in a harsh corrosive environment. However, it is expensive due to a high nickel content. Thus, electrochemical behavior and cavitation erosion characteristics of UNS S32750 as an alternative material were investigated. Microstructure analysis revealed fractions of ferritic and austenitic phases of 48% and 52%, respectively, confirming the existence of ferritic matrix and austenitic island. Potentiodynamic polarization test revealed damage at the interface of the two phases because of galvanic corrosion due to different chemical compositions of ferritic and austenitic phases. After a cavitation test, a compressive residual stress was formed on the material surface due to impact pressure of cavity. Surface hardness was improved by water cavitation peening effect. Hardness value was the highest at 30 ㎛ amplitude. Scanning electron microscopy revealed wave patterns due to plastic deformation caused by impact pressure of the cavity. The depth of surface damage increased with amplitude. Cavitation test revealed larger damage caused by erosion in the ferritic phase due to brittle fracture derived from different strain rate sensitivity index of FCC and BCC structures.

Electrical Reliability of ITO Film on Flexible Substrate During bending Deformations and Bending Fatigue (유연 기판상 ITO 전극의 굽힘변형 및 굽힘피로에 따른 전기적 신뢰성 연구)

  • Seol, Jea-Geun;Kim, Byoung-Joon
    • Journal of the Microelectronics and Packaging Society
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    • v.24 no.4
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    • pp.47-52
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    • 2017
  • Recently, a great attention has been paid to the mechanical behavior of ITO (Indium Tin Oxide) film, which is widely used in current smart devices due to its excellent electrical properties and transparency. In this study, the reliability of ITO thin films on flexible substrates was investigated using bending test and bending fatigue test. According to the relative position of ITO and substrate, the experiment was conducted on both outer and inner bending conditions. Inner bending condition exhibited superior electrical stability compared to outer bending test. The electrical resistance during outer bending fatigue test significantly increased compared to that in the inner bending fatigue. The crack nucleation and propagation differs according to the stress state and they have a great influence on the electrical resistance. The crack morphologies were observed by scanning electron microscopy.

Evaluation of the Effect of High Temperature on the Interface Characteristics between Solid Oxide Fuel Cell and Ag Paste (고온열처리가 고체산화물연료전지의 전극과 Ag 페이스트의 계면에 미치는 특성 평가)

  • Jeon, Sang Koo;Nahm, Seung Hoon;Kwon, Oh Heon
    • Journal of the Korean Society of Safety
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    • v.30 no.1
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    • pp.21-27
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    • 2015
  • In this study, interfacial characteristics between SOFC and Ag paste as current collector was estimated in the high temperature environment. The Ag paste was used to connect the unit cell of SOFC strongly with interconnector and provide the electrical conductivity between them. To confirm electrical conductivity, Ag paste was treated in the furnace at $800^{\circ}C$ for 48 hours. The sheet resistance of Ag paste was measured to compare the resistance values before and after the heat treatment. Also, the four-point bending test was performed to measure the interfacial adhesion. The unit cell of SOFC and $SiO_2$ wafer were diced and then attached by Ag paste. The $SiO_2$ wafer had the center notch to initiate a crack from the tip of the notch. The modified stereomicroscope combined with the CCD camera and system for measuring the length was used to observe the fracture behavior. To compare the characteristics before heat treatment and after heat treatment, the specimen was exposed in the furnace at $800^{\circ}C$ for 48 hours and then the interfacial adhesion was evaluated. Finally, the interfacial adhesion energy quantitatively increases $1.78{\pm}0.07J/m^2$ to $4.9{\pm}0.87J/m^2$ between the cathode and Ag paste and also increase $2.9{\pm}0.47J/m^2$ to $5.12{\pm}1.01J/m^2$ between the anode and Ag paste through the high temperature. Therefore, it is expected that Ag paste as current collector was appropriate for improving the structural stability in the stacked SOFC system if the electrical conductivity was more increased.

Hydrogen Embrittlement Resistance and Diffusible Hydrogen Desorption Behavior of Multipass FCA Weld Metals (다층 FCA 용착금속의 수소취성 저항성 및 확산성 수소 방출 거동)

  • Yoo, Jaeseok;Xian, Guo;Lee, Myungjin;Kim, Yongdeok;Kang, Namhyun
    • Journal of Welding and Joining
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    • v.31 no.6
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    • pp.112-118
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    • 2013
  • In this study, constant loading test (CLT) was performed to evaluate the hydrogen embrittlement resistance for multipass FCA weld metals of 600MPa tensile strength grade. The microstructures of weld metal-2 having the smallest carbon equivalent (Ceq=0.37) consisted of grain boundary ferrite and widmanstatten ferrite in the acicular ferrite matrix. The weld metal-1 having the largest Ceq=0.47, showed the microstructures of grain boundary ferrite, widmanstatten ferrite and the large amount of bainite (vol.%=19%) in the acicular ferrite matrix. The weld metal-3 having the Ceq=0.41, which was composed of grain boundary ferrite, widmanstatten ferrite, and the small amount of bainite (vol.%=9%) in the acicular ferrite matrix. Hydrogen desorption spectrometry (TDS) used to analyze the amount of diffusible hydrogen and trapping site for the hydrogen pre-charged specimens electrochemically for 24 hours. With increasing the current density of hydrogen pre-charging, the released amount of diffusible hydrogen was increased. Furthermore, as increasing carbon equivalent of weld metals, the released diffusible hydrogen was increased. The main trapping sites of diffusible hydrogen for the weld metal having a low carbon equivalent (Ceq=0.37) were grain boundaries and those of weld metals having a relatively high carbon equivalent (Ceq: 0.41~0.47) were grain boundaries and dislocation. The fracture time for the hydrogen pre-charged specimens in the constant loading test was decreased as the carbon equivalent increased from 0.37 to 0.47. This result is mainly due to the increment of bainite that is vulnerable to hydrogen embrittlement.

Behavior of High-elastic Stress Absorbing Interlayer for Reflective Cracking Resistance (고탄성 응력흡수층의 반사균열 저항특성 연구)

  • Park, Tae Soon;Lee, Yo Seop
    • KSCE Journal of Civil and Environmental Engineering Research
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    • v.26 no.3D
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    • pp.445-451
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    • 2006
  • This study was conducted to develop the interlayer mixture that absorbs the stress between the old concrete pavement and the asphalt overlay pavement layer. The elasticity, the flexibility, the consistency and the impermeability is required for high-elastic Stress Absorbing Interlayer(HSAI) to absorb and disperse the stress that causes the flexural and horizontal movements of the joint and the crack. The HSAI developed from foreign product was satisfied with the design criteria. The specimens using the HSAI showed the significant reduction of the reflective crack compared those not using the HSAI. The significance included that the life of shear failure and horizontal displacement resistance increased 4 times. The life of the share failure increased to 5 times and the horizontal displacement increased to 9 times according to the selection of surface course material which showed the excellence of the HSAI.

A Study on Crystalline Structural Variations of the Rigid Spherical-Tip scratch on the Surface of α-Titanium substrates via Molecular Dynamics Simulations (α-티타늄 평판표면에서 강체 구형팁의 스크래치로 인한 내부 결정구조 특성 변화에 대한 연구)

  • Yeri Jung;Jin Ho Kim;Taeil Yi
    • Tribology and Lubricants
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    • v.39 no.5
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    • pp.167-172
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    • 2023
  • Titanium alloys are widely recognized among engineering materials owing to their impressive mechanical properties, including high strength-to-weight ratios, fracture toughness, resistance to fatigue, and corrosion resistance. Consequently, applications involving titanium alloys are more susceptible to damage from unforeseen events, such as scratches. Nevertheless, the impact of microscopic damage remains an area that requires further investigation. This study delves into the microscopic wear behavior of α-titanium crystal structures when subjected to linear scratch-induced damage conditions, utilizing molecular dynamics simulations as the primary methodology. The configuration of crystal lattice structures plays a crucial role in influencing material properties such as slip, which pertains to the movement of dislocations within the crystal structure. The molecular dynamics technique surpasses the constraints of observing microscopic phenomena over brief intervals, such as sub-nano- or pico-second intervals. First, we demonstrate the localized transformation of lattice structures at the end of initialization, indentation, and wear processes. In addition, we obtain the exerted force on a rigid sphere during scratching under linear movement. Furthermore, we investigate the effect of the relaxation period between indentation and scratch deformation. Finally, we conduct a comparison study of nanoindentation between crystal and amorphous Ti substrates. Thus, this study reveals the underlying physics of the microscopic transformation of the α-titanium crystal structure under wear-like accidental events.

Mechanical Properties and Impact Resistance Review of Carbon Fiber Reinforced Cement Composites with Different Fiber Contents and Fiber Lengths (섬유혼입률 및 섬유길이 변화에 따른 탄소섬유 보강시멘트 복합재료의 역학적 특성과 내충격성 검토)

  • Heo, Gwang-Hee;Song, Ki-Chang;Park, Jong-Gun;Han, Yoon-Jung;Lim, Cae-Young
    • Journal of the Korea institute for structural maintenance and inspection
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    • v.23 no.4
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    • pp.86-95
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    • 2019
  • Recently, the applications of carbon fiber have been broader than ever when it comes to such industrials as automobiles, ships, aerospace, civil engineering and architecture because of their lightweight-ness and high mechanical properties. This study analyzed mechanical properties and flexural behavior of carbon fiber reinforced cement composites(CFRC) with different fiber contents and fiber lengths, and also impact resistance by natural drop test on mortar specimens was compared and examined. In addition, contents of carbon fiber(CF) were varied by 0.5%, 1.0%, 2.0% and 3.0%. Fiber lengths was used for 6 mm and 12 mm, respectively. As a result of the test, the flow value was very disadvantageous in terms of fluidity due to the carbon fiber ball phenomenon, and the unit weight was slightly reduced. In particular, the compressive strength was decreased with increasing carbon fiber contents. On the other hand, the flexural strength was the highest with 12 mm fiber length and 2% fiber content. As the results of the impact resistance test, the specimens of plain mortar takes about 2~3 times to final fracture, while the specimens of CFRC is somewhat different depending on the increase of the fiber contents. However, when the fiber length is 12 mm and the fiber content is 2%, the impact resistance was the highest.

A STUDY ON FRACTURAL BEHAVIOR OF DENTIN-RESIN INTERFACE (상아질-복합레진 접착계면의 파괴거동에 대한 연구)

  • Ryu, Gil-Joo;Choi, Gi-Woon;Park, Sang-Jin;Choi, Kyung-Kyu
    • Restorative Dentistry and Endodontics
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    • v.32 no.3
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    • pp.208-221
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    • 2007
  • The fracture toughness test is believed as a clinically relevant method for assessing the fracture resistance of the dentinal restoratives. The objectives of this study were to measure the fracture toughness $(K_{1C})$ and microtensile bond strength of dentin-resin composite interface and compare their relationship for their use in evaluation of the integrity of the dentin-resin bond. A minimum of six short-rod specimens for fracture toughness test and fifteen specimens for microtensile bond strength test was fabricated for each group of materials used. After all specimens storing for 24 hours in distilled water at $37^{\circ}C$, they were tensile-loaded with an EZ tester universal testing machin. Statistical analysis was performed using ANOVA and Tukey's test at the 95% confidence level, Pearson's coefficient was used to verify the correlation between the mean of fracture toughness and microtensile bond strength. FE-SEM was employed on fractured surface to describe the crack propagation. Fracture toughness value of Clearfil SE Bond (SE) was the highest, followed by Adper Single Bond 2 (SB), OptiBond Solo (OB), ONE-STEP PLUS (0S), ScotchBond Multi-purpose (SM) and there was significant difference between SE and other 4 groups (p < 0.05). There were, however, no significant difference among SB, OB, OS, SM (p > 0.05). Microtensile bond strength of SE was the highest, followed by SB, OB, SM, OS and OS only showed significant lower value (p < 0.05). There was no correlation between fracture toughness and microtensile bond strength values. FE-SEM examination revealed that dentin bonding agent showed different film thickness and different failure pattern according to the film thickness. From the limited results of this study, it was noted that there was statistically no correlation between K1C and ${\mu}TBS$. We can conclude that for obtaining the reliability of bond strength test of dentin bonding agent, we must pay more attention to the test procedure and its profound scrutiny.

Fatigue Behavior of 23Cr26Ni Heat Resistant Steel (23Cr26Ni 내열강의 피로 특성)

  • Lee, H.W.;Kwun, S.I.
    • Journal of the Korean Society for Heat Treatment
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    • v.24 no.2
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    • pp.92-98
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    • 2011
  • The influence of the cooling condition after solution treatment on the high temperature fatigue resistance of 23Cr-26Ni heat resistant steel was investigated. Two different cooling conditions were applied to the steel after solution treatment at $1200^{\circ}C$ for 3 hours. One specimen was water quenched immediately after the solution treatment. The other one was furnace cooled at a rate of $0.5^{\circ}C/min$ down to $750^{\circ}C$ after the solution treatment. Then, both specimens were aged at $750^{\circ}C$ for 5 hours. Under two different heat treatment conditions, the low cycle fatigue (LCF) test was performed at $600^{\circ}C$ and room temperature (RT). Only cyclic hardening continued from the beginning until fracture at all strain amplitudes during LCF at $600^{\circ}C$. This phenomenon was attributed to the increase in the dislocation density due to cyclic deformation, which resulted in the interaction between the newly created dislocations and precipitates. Cyclic hardening followed by saturation and cyclic softening was observed at RT. Cyclic softening was attributed to the dislocation annihilation rate exceeding the dislocation generation rate. Other probable factor for cyclic softening was some cavities formed around grain boundaries after 20 cycles. WQ and FC have a similar LCF behavior at RT and $600^{\circ}C$ as shown in the cyclic stress response curves.

Experimental Study on Double Skin Composite Walls Subjected to Cyclic Loading (주기하중을 받는 이중강판합성벽의 실험연구)

  • Eom, Tae Sung;Park, Hong Gun;Kim, Jin Ho;Chang, In Hwa
    • Journal of Korean Society of Steel Construction
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    • v.20 no.2
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    • pp.289-301
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    • 2008
  • Double skin composite (DSC) wall is a structural wall that is filed with concrete between two steel plate skins connected by tie bars. This type of wall was developed to enhance the structural performance of wall, to reduce wall thickness, and to enhance constructibility, eliminating the use of formwork and re-bars. In this study, cyclic tests were performed to investigate the inelastic behavior and earthquake resistance of isolated and coupled DSC walls with rectangular and T-shapedcross-sections. The DSC walls showed stable cyclic behaviors, exhibiting excellent energy dissipation capacity. The te st specimens failed by the tensile fracture of welded joints at the wall base and coupling beam and by the severe local buckling of the steel plate. The deformation capacity of the walls varied with the connection details at the wall base and their cross-sectional shapes. The specimens with well-detailed connections at the wall base showed relatively god deformation capacity ranging from 2.0% to 3.7% drift ratio. The load-carrying capacities of the isolated and coupled wall specimens were evaluated considering their inelastic behavior. The results were compared with the test results.