• Title/Summary/Keyword: Fine powder

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Preparation of Multicomponent Ceramic Powders by Ultrasonic Spray Pyrolysis

  • Youn, Jeong-Han;Chung, Byung-Joo;Sim, Soo-Man
    • The Korean Journal of Ceramics
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    • v.6 no.1
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    • pp.58-63
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    • 2000
  • The preparation of Y-doped $SrZrO_3$powder by ultrasonic spray pyrolysis was investigated as a representative system, in order to produce fine, single phase multicomponent oxide powders. A precursor solution containing metal nitrates, citric acid and ethylene glycol was atomized glycol was atomized with an ultrasonic spray nozzle. Gel particles formed by organic functional groups were pyrolyzed and subsequently calcined at $800^{\circ}C$ to obtain well-crystallized, single perovskite phase. Most of large particles exhibited macroscopic pores and weak agglomeration between primary particles. However, strong agglomeration was observed in the surfaces of large particles. The effect of the microstructures of these particles on size reduction to submicron particles was described.

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The Effects of Oxidation Conditions on the Magnetic Properties of Cu-Zn Ferrite Powder (산화 조건에 따른 Cu-Zn Ferrite분말의 자기적 특성)

  • Shin, K.H.;SaGong, G.
    • Proceedings of the KIEE Conference
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    • 1993.11a
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    • pp.222-224
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    • 1993
  • In this paper, The optimum oxidation conditions for the formation of Cu-Zn ferrite were investigated using precipitates obtained by the mixture of $CuCl_2{\cdot}2H_2O$, $ ZnCl_2$, $FeCl_3{\cdot}6H_2O$ and NaOH. The precipitates were prepared by coprecipitation method on various temperatures and oxidation conditions. The oxidation products were examined by SEM, XRD, and VSM. The particles obtained at 70($^{\circ}C$) were more spherical and fine than that of prepared at 25($^{\circ}C$), 50($^{\circ}C$), 60($^{\circ}C$), respectively. By $H_2O_2$ oxidation, the saturation magnetization of the powders was little influenced, But, by air oxidation the saturation magnetization of the powders was influenced intricately. According to our experimental data, the saturation magnetization of the powders increased with reaction time and was saturated at 9 hours.

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The Investigation for the Possibility to Utility on the Natural Zeolite and Mud Stone as Admisxture (혼화재로서 천연제올라이트 및 이암의 활용성 검토에 관한 연구)

  • 김화중;김태섭;박정민;한종훈
    • Proceedings of the Korea Concrete Institute Conference
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    • 1993.10a
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    • pp.167-172
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    • 1993
  • In domestic, there are not adequate admixtures for concrete now, so the study on that is required deeply, Accordingly the purpose of this study is to analyze the application possibilities of Natural Zeolite and Mud Stone as admixtures for concrete through comparing the compressive strength prorerties of mortar mixed with imported Silica Fume those mixed with domestic Zeolite and Mud Stone. As the results from this study, the optimum displacement rate of Silica Fume, Zeolite and Mud Stone is 15%, 5~10%, 15% respectively. In Zeolite and Mud Stone, the compressive strength is higher in proportion as the powder is fine. Consequentely, the application possibility the application possibility of Zeolite and Mud Stone is very sufficient as admixtures for concrete.

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Heat Conductivity Test and Conduction Mechanism of Nanofluid (나노유체의 열전도율 실험과 열전달 메커니즘의 제시)

  • Park, Kweon-Ha;Lee, Jin-A;Kim, Hye-Min
    • Journal of Advanced Marine Engineering and Technology
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    • v.32 no.6
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    • pp.862-868
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    • 2008
  • Many studies have been conducted to increase heat transfer in fluid. One of the various heat transfer enhancement techniques is suspending fine metallic or nonmetallic solid powder in traditional fluid. Nanofluid is defined as a new kind of heat transfer fluid containing a very small quantity of nanometer particles that are uniformly and stably suspended in a liquid. This study investigates the effect of nanofluid containing diamond, CuNi and CuAg nanometer particles, and proposes the heat transport mechanism of nanofluid. The test result shows that the thermal conductivity of nanofluid is much higher than that of traditional fluid, and the increasing rate of the conductivity is dependent on the conductivity of the solid metal.

A Study on the Structure and Strength of Rapidly Solidified HSLA Steels (급냉응고한 HSLA강의 조직과 강도에 의한 연구)

  • Nam, Tea-Woon
    • Journal of Korea Foundry Society
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    • v.10 no.2
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    • pp.162-170
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    • 1990
  • The major effects of RSP sre 1) extension of solid solubilities, 2) formation of metastable phaeses, 3) microstructural refinement 4) segregationless. The main trust of this study was to investigate the effects of superimposing RSP on the structure and properties of HSLA steels. Powder was made by NGA (Nitrogen Gas Atomization) process, and consolidated by HIP. The high grain-coarsening resistance of NGA-HIP steels was attributed to a fine dispersion of oxide precipitates. The average grain size for the NGA-HIP steels was somewhat finer than that for the conventional HSLA steels, The impact properteis of NGA-HIP steels were improved over those of the conventional HSLA steels.

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Formation and Dissociation Processes of Gas Hydrate Composed of Methane and Carbon Dioxide below Freezing

  • Hachikubo, Akihiro;Yamada, Koutarou;Miura, Taku;Hyakutake, Kinji;Abe, Kiyoshi;Shoji, Hitoshi
    • Ocean and Polar Research
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    • v.26 no.3
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    • pp.515-521
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    • 2004
  • The processes of formation and dissociation of gas hydrates were investigated by monitoring pressure and temperature variations in a pressure cell in order to understand the kinetic behavior of gas hydrate and the controlling factors fur the phase transition of gas hydrate below freezing. Gas hydrates were made kom guest gases ($CH_4,\;CO_2$, and their mixed-gas) and fine ice powder. We found that formation and dissociation speeds of gas hydrates were not controlled by temperature and pressure conditions alone. The results of this study suggested that pressure levels at the formation of mixed-gas hydrate determine the transient equilibrium pressure itself.

A Study on Mixing of Silicon Nitride Fine Powder and Binder System for Ceramic Injection Molding (세라믹 사출성형을 위한 질화규소 미세분말과 결합체 시스템의 혼합에 대한 연구)

  • 윤재륜
    • The Korean Journal of Rheology
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    • v.2 no.1
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    • pp.67-78
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    • 1990
  • 세라믹 분말의 사출성형성을 평가하기 위하여 다양한 혼합체 시스템에 대한 혼합도 와 유변학적 성질을 질화규소 미세분말의 부피비를 변화시키면서 조사하였다. 열가소성 결 합체 시스템은 폴리에틸린 폴리에틸렌 왁스 그리고 미소량의 첨가제를 혼합하여 사용하였 다. 혼합성능을 평가하기 위하여 비분산혼합에서는 총접촉면적비를 그리고 분산혼합에서는 총파괴표면적비를 혼합척도로서 사용하여 정성적으로 모형화하였다. 사용된 혼합기내의 유 동장을 해석하기 위하여 뉴우톤유체를 가정하여 유동해석을 수행하였다. 혼합물의 혼합도는 각각 5분 30분 동안 혼합된 시편을 주사전자현미경 사진에 의해 관찰하여 평가하였다. 또한 혼합물의 사출성형성 그리고 혼합질 점도 토우크 곡선 사이의 관계를 규명하기 위하여 전단 변형를 속도를 따른 점도를 모세관 점도계를 사용하여 측정하였으며 질화규소의 부피비가 60%일 때까지는 만족할 만한 성형성과 혼합질을 가짐을 알 수 있었다.

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A Feasibility Study for Application of On-Line Wear Condition Monitoring Technique to the High-powered Diesel Engine (고출력 디젤 엔진의 On-Line 마모상태진단 기술 적용을 위한 기초연구)

  • 윤민호;정동윤;공호성
    • Proceedings of the Korean Society of Tribologists and Lubrication Engineers Conference
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    • 1997.10a
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    • pp.59-65
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    • 1997
  • The calibration of O.M.D is carried out experimentally and is analysed theoretically. O.M.D experimentally measures the change in optical density of artificially contaminated oil which contains Fe powder of 5, 10, 20, 30, 40, 50, 70, 100, 200 ppm. The change in optical density, D$_1$ means the logarithmic transmittance of I$_0$ over $I_1 D_2$ denotes the logarithmic transmittance I$_2$ over I$_1$ on electromagnetic force which arranges the ferrous particles along the line of magnetic force. The theoretical D$_1$ which increases linearly as increasing Fe concentrations, is analysed by light attenuation theory. The difference between theoretical D$_1$ and experimental D$_1$ is due to the attenuation of micro bubbles and the agglomeration of fine particles in the sample oil. The calibrated O.M.D is applied to the sample oil from the high-powered diesel engine. Also the results are compared with those out of the off-line techniques such as JOAP and ICP.

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Quantification Method of Macro Stickies for Recycled Pulps (재생펄프의 점착성 이물질 정량 분석 방법)

  • 윤병태;오세균
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.31 no.2
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    • pp.86-91
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    • 1999
  • A new test method has been developed for a quantitative evaluation of macro-stickies in recycled pulps. The method uses a fine slot screen to separate a sticky particles form fiber in the pulp samples. The obtained sticky particles were spread on filter paper and covered with silicon carbide powder in order to make the stickies area with sufficient contrast between stickies and background. The stickies are then counted by a scanner-based image analysis system. The validity of this evaluation method of stickies of KOCC, ONP and white ledger wastepaper recycling plants respectively. It is shown that this method can be applied for a quantitative determination of stickies content in various recycled pulp samples. With this testing method, reproducible and reliable data were obtained for the actual mill pulp samples.

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An Experimental Study on the Durability of SFRC Using Fly Ash (플라이애쉬를 이용한 강섬유보강 콘크리트의 내구성에 관한 실험적 연구)

  • 박승범;오광진;이택우;권혁준
    • Proceedings of the Korea Concrete Institute Conference
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    • 1997.10a
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    • pp.339-344
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    • 1997
  • During recent years the durability of concrete structures has attracted considerable interest in concrete practice, material research and long-term deformation. To preserve the brittleness of concrete as well as energy absorption and impact resistance, amount of fiber usage has greatly increased year to year in the field of public works. When fly ash, fine powder, mixed into concrete, it condensed the void of concrete structure. Expecially, there's a great effect for strength improvement of concrete by initial pozzolanic reactions. Pozzolan reaction, between cement particle and fly ash, can elaborate the micro structure of matrix. So it was able to improve the effect of fiber reinforced by increased adhesion between cement paste and steel fiber. And so, in this paper, we dealt SFRC for the purpose of efficiently using of industrial by-products and its economical manufacturing. Also we performed the test for durability such as chemical resistance, freeze-thaw resistance and accelerated carbonation of SFRC using fly ash.

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