• Title/Summary/Keyword: Fine Powder

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Nanostructure Ceramics of Silicon Nitride Produced by Spark Plasma Sintering

  • Hojo, Junichi;Hotta, Mikinori
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.323-324
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    • 2006
  • The nanostructure control of $Si_3N_4$ ceramics can be achieved by using fine starting powder and retardation of grain growth. The spark plasma sintering technique is useful to retard the grain growth by rapid heating. In the present work, the change of microstructure was investigated with emphasis on the particle size of starting powder, the amount of sintering additive and the heating schedule. The rapid heating by spark plasma sintering gave the fine microstructure consisting of equiaxed grains with the same size as starting particles. The spark plasma sintering of $Si_3N_4$ fine powder was effective to control the microstrucutre on nano-meter level.

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The Effects of Gagbungyunsoo-tanghap Zeungsonbakchul-san (GYZB) Hot Water Extract & Ultra-fine Powder on the Alzheimer's Disease Model (각병연수장합증손백출산(却病延壽場合增損白朮散) 열수추출물, 초미세분말제형이 Alzheimer's Disease 병태(病態) 모델에 미치는 영향)

  • Choi, Bo-Yoon;Lee, Sang-Ryong;Jung, In-Chul
    • The Journal of Korean Medicine
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    • v.28 no.2 s.70
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    • pp.137-154
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    • 2007
  • Objective : This experiment was designed to investigate the effect of the GYZB hot water extract & ultra-fine powder on the Alzheimer's disease model induced by amyloid ${\beta}$ protein (${\beta}A$). Method : We measured the effects of the GYZB hot water extract on expression of $IL-1{\beta}$, IL-6 mRNA and production of IL-6, $TNF-{\alpha}$ in the BV2 microglial cell line treated with lipopolysaccharide (LPS). The effects of the GYZB hot water extract & ultra-fine powder on (1) the behavior, (2) expression of $IL-1{\beta}$ and $TNF-{\alpha}$, (3) glucose in serum, (4) the infarction area of the hippocampus, and brain tissue injury in mice induced with Alzheimer's diseased by ${\beta}A$ were investigated. Results : The GYZB hot water extract suppressed the expression of $IL-1{\beta}$ and IL-6 mRNA and significantly suppressed the production of IL-6 and $TNF-{\alpha}$ in the BV2 microglial cell line treated with LPS. The GYZB hot water extract & ultra-fine powder showed a significant inhibitory effect on the memory deficit of the mice with Alzheimer's disease induced by ${\beta}A$ in the Morris water maze experiment, which measured stop-through latency and distance movement-through latency. The GYZB ultra-fine powder significantly suppressed the expression of $IL-1{\beta}$ and $TNF-{\alpha}$ protein, and the GYZB hot water extract significantly suppressed the expression of $TNF-{\alpha}$ protein in the microglial cell of mice with Alzheimer's disease induced by ${\beta}A$. The GYZB hot water extract & ultra-fine powder reduced the infarction area of hippocampus in the mice with Alzheimer's disease induced by ${\beta}A$. Conclusions : These results suggest that GYZB hot water extract & ultra-fine powder may be effective for the prevention and treatment of Alzheimer's disease. Investigation into the clinical use of GYZB for Alzheimer's disease is suggested for future research.

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Physical Properties of Polymer Modified Mortar Containing FRP Wastes Fine Powder (폐FRP 미분말을 사용한 폴리머 시멘트 모르타르의 물성)

  • 황의환;한천구;최재진;이병기
    • Journal of the Korea Concrete Institute
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    • v.14 no.2
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    • pp.190-198
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    • 2002
  • In this research the physical properties of polymer modified mortar containing pulverized FRP(Fiber-Reinforced Plastics) wastes fine powder as a part of fine aggregate were investigated. Styrene-butadiene rubber(SBR) latex, polyacrylic ester(PAE) emulsion and ethylene-vinyl acetate(EVA) emulsion were used as Polymer modifier. Polymer modified mortars containing FRP wastes fine powder were prepared with various FRP wastes fine powder replacement(5∼30 wt%) for fine aggregate and polymer-cement ratios(5∼20 wt%). The water-cement ratio, water absorption rates and hot water immersion test, compressive and flexural strengths of polymer modified mortars were tested and the results compared to those of ordinary portland cement mortar. As the results, compressive and flexural strengths of polymer modified mortar containing FRP wastes fine powder depend on the contents of FRP wastes fine powder, type and additional amounts of polymer modifier. Some of them showed higher compressive and flexural strengths than those of ordinary portland cement mortar. Especially, SBR-modified mortar showed the highest strengths properties among three types of polymer modifier. Also water absorption rates, compressive and flexural strengths of SBR-modified mortar were more superior than those of PAE or EVA-modified mortar. The optimum mix proportions of SBR-modified mortar was 20 wt% of polymer-cement ratio and 20 wt% of FRP wastes fine powder replacement. Otherwise heat cured polymer modified mortar accelerated the improvement of early compressive and flexural strengths.

Development of Spherical Fine Powders by High-pressure Water Atomization Using Swirl Water Jet (II)

  • Terai, Shinji;Kikukawa, Masato;Inaba, Tsuneta;Koyama, Tadashi
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.16-17
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    • 2006
  • In order to obtain spherical fine powder, we have developed a new method of high-pressure water atomization system using swirl water jet with the swirl angle $(\omega)$. The effect of nozzle apex angle $(\theta)$ upon the morphology of atomized powders was investigated. Molten copper was atomized by this method, with $\omega=0.2$ rad (swirl water jet) and $\omega=0$ rad (conical water jet). It was found that the median diameter $(D_{50})$ of atomized powders decreased with decreasing $(\theta)$ down to 0.35 rad in each $\omega$, but under ${\theta}<\;0.35$ rad, $D_{50}$ increased abruptly with decreasing $\theta$ for $\omega=0$ rad, while it was still decreased with decreasing $(\theta)$ for $\omega=0.2$ rad.

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A Study on the Mix Design Model of 40MPa Class High Strength Mortar with Rice Husk Powder Using Neural Network Theory (신경망 이론을 적용한 40MPa급 증해추출 왕겨분말을 혼입한 고강도 무시멘트 모르타르 배합설계모델에 관한 연구)

  • Cho, Seung-Bi;Kim, Young-Su
    • Proceedings of the Korean Institute of Building Construction Conference
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    • 2022.04a
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    • pp.156-157
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    • 2022
  • The purpose of this study is to propose a 40MPa mortar mixed design model that applies the neural network theory to minimize wasted effort in trial and error. A mixed design model was applied to each of the 60 data using fly ash, blast furnace slag fine powder and thickened rice husk powder. And in the neural network model, the optimized connection weight was obtained by repeatedly applying it to the MATLAB. The completed mixed design model was demonstrated by analyzing and comparing the predicted values of the mixed design model with those measured in the actual compressive strength test. As a result of the mixed design verification experiment, the error rates of the double mixed non-cement mortar using blast furnace slag fine powder and rice husk powder at a height of 40MPa were 3.24% and 3.4%. Mixed with fly ash and rice husk powder had an error rate of 3.94% and 5.8%. The error rate of the triple mixed non-cement mortar of the rice husk powder, fly ash, and blast furnace slag fine powder was 2.5% and 5.1%.

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Effect of Powder and Aggregates on Compactability of High Performance Concrete

  • Lee, Seung-Han;Han, Hyung-sub
    • KCI Concrete Journal
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    • v.11 no.3
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    • pp.19-28
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    • 1999
  • This study treated self-compacting high Performance concrete as two Phase materials of Paste and aggregates and examined the effect of powder and aggregates on self-compacting high performance, since fluidity and segregation resistance of fresh concrete are changed mainly by paste. To improve the fluidity and self-compactibility of concrete, optimum powder ratio of self-compacting high performance concrete using fly ash and blast-furnace slag as powders were calculated. This study was also designed to provide basic materials for suitable design of mix proportion by evaluating fluidity and compactibility by various volume ratios of fine aggregates, paste, and aggregates. As a result, the more fly ash was replaced, the more confined water ratio was reduced because of higher fluidity. The smallest confined water ratio was determined when 15% blast-furnace slag was replaced. The lowest confined water ratio was acquired when 20% fly ash and 15% blast-furnace slag were replaced together. The optimum fine aggregates ratio with the best compactibility was the fine aggregate ratio with the lowest percentage of void in mixing coarse aggregate and fine aggregate In mixing the high performance concrete. Self-compacting high performance concrete with desirable compactibility required more than minimum of unit volume weight. If the unit volume weight used was less than the minimum, concrete had seriously reduced compactibility.

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Effect of Powder Size on the Rheological Characteristics of Sm-Co Type Compound for Powder Injection Molding (사출성형용 컴파운드의 유연학적 특성에 미치는 SH-CO 계 분말의 입도 영향)

  • 정우상;김윤배;정원용
    • Journal of the Korean Magnetics Society
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    • v.11 no.4
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    • pp.157-162
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    • 2001
  • Rheological characteristics of Sm-Co type plastic magnet compound for powder injection molding process were investigated with the variation of the magnetic powder size, their relative contents and volume fraction using the mixture of fine and coarse powder. Shear viscosity of Sm-Co type compound was decreased with increasing the size of coarse powder due to the increase of powder packing density. However, the smaller the average size of fine powder resulted in the higher viscosity of compound due to the increase of agglomeration force. In case of mechanically milled Sm-Co type powder, the viscosity of compound with the mixture of coarse powder of 125∼75 ㎛ and fine powder of average size of 4.9 ㎛ greatly depends on their relative contents and shows a minimum value at the 60 % coarse powder fraction. This means that the compound shows a maximum packing density at the 60% coarse powder fraction. Compound viscosities satisfied well the rheological model with the volume fraction of magnetic powder, and maximum volume fraction of magnetic powder in Sm-Co type compound for powder injection molding was about 66%.

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Fine-Pitch Solder on Pad Process for Microbump Interconnection

  • Bae, Hyun-Cheol;Lee, Haksun;Choi, Kwang-Seong;Eom, Yong-Sung
    • ETRI Journal
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    • v.35 no.6
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    • pp.1152-1155
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    • 2013
  • A cost-effective and simple solder on pad (SoP) process is proposed for a fine-pitch microbump interconnection. A novel solder bump maker (SBM) material is applied to form a 60-${\mu}m$ pitch SoP. SBM, which is composed of ternary Sn3.0Ag0.5Cu (SAC305) solder powder and a polymer resin, is a paste material used to perform a fine-pitch SoP through a screen printing method. By optimizing the volumetric ratio of the resin, deoxidizing agent, and SAC305 solder powder, the oxide layers on the solder powder and Cu pads are successfully removed during the bumping process without additional treatment or equipment. Test vehicles with a daisy chain pattern are fabricated to develop the fine-pitch SoP process and evaluate the fine-pitch interconnection. The fabricated Si chip has 6,724 bumps with a 45-${\mu}m$ diameter and 60-${\mu}m$ pitch. The chip is flip chip bonded with a Si substrate using an underfill material with fluxing features. Using the fluxing underfill material is advantageous since it eliminates the flux cleaning process and capillary flow process of the underfill. The optimized bonding process is validated through an electrical characterization of the daisy chain pattern. This work is the first report on a successful operation of a fine-pitch SoP and microbump interconnection using a screen printing process.