• 제목/요약/키워드: Filler content

검색결과 396건 처리시간 0.024초

NCA 물성에 따른 극미세 피치 COG (Chip on Glass) In, Sn 접합부의 신뢰성 특성평가 (Improvement of Reliability of COG Bonding Using In, Sn Bumps and NCA)

  • 정승민;김영호
    • 마이크로전자및패키징학회지
    • /
    • 제13권2호
    • /
    • pp.21-26
    • /
    • 2006
  • NCA의 물성이 미세피치 Chip on glass (COG) 접합부의 신뢰성에 미치는 영향을 연구하였다. Si 위에 Sn을, 유리기판 위에 In을 열증발 방법으로 증착하고 lift-off 방법을 이용하여 $30{\mu}m$ 피치를 가지는 솔더범프를 형성하였으며 열압착 방법으로 $120^{\circ}C$에서 In 범프와 Sn 범프를 접합하였다. 접합할 때 세 종류의 Non conductive adhesive (NCA)를 적용하였다. 신뢰성은 $0^{\circ}C$$100^{\circ}C$ 사이로 열충격시험을 2000회까지 실시하여 평가하였다. 4단자 저항측정법을 이용하여 접합부의 저항을 측정하였다. 필러의 양이 증가할수록 열충격시험 후 접합부의 저항이 가장 적게 증가하여 신뢰성이 우수하였다. 필러의 양이 증가할수록 NCA의 열팽창이 작아지기 때문이다.

  • PDF

열전도성 점착제 응용을 위한 고분자 기반 탄소나노소재 복합체 제조 및 특성 평가 (Fabrication and characterization of polymer-based carbon nanomaterial composites for thermal conductive adhesive application)

  • 이병주;조성일;윤은혜;이애리;이우영;허성규;황재성;정구환
    • 한국표면공학회지
    • /
    • 제53권4호
    • /
    • pp.160-168
    • /
    • 2020
  • A polymer-based carbon nanomaterial composite was fabricated and characterized for the application of a thermal conductive adhesive. Low-dimensional carbon nanomaterials with excellent thermal conductivity such as carbon nanotube (CNT) and graphene were selected as a filler in the composite. Thermal, electrical and adhesive properties of the composite were investigated with respect to the morphology and content of the low-dimensional carbon nanomaterials. As a result, the composite-based adhesive fabricated by the loading of surface-treated MWCNTs of 0.4 wt% showed uniform dispersion, moderate adhesion and effective heat dissipation properties. Finally, it was confirmed through the thermal image analysis of LED module that the temperature reduction of 10℃ was achieved using the fabricated composite adhesive with MWCNT-6A. Expecially, heat dissipation performance of the optimized composite adhesive was evident at the hot spot in the module compared to other samples mixed with graphene or different MWCNT loading ratios.

고농축 복합화약 시뮬란트: Exact/Dechlorane 현탁계의 유변물성 (Highly Concentrated Polymer Bonded Explosive Simulant: Rheology of Exact/Dechlorane Suspension)

  • 이상묵;홍인권;이재욱;이근득
    • 폴리머
    • /
    • 제38권3호
    • /
    • pp.286-292
    • /
    • 2014
  • 에너지 고분자인 poly(BAMO-AMMO)와 유사한 특성을 갖는 폴리에틸렌 플라스토머인 Exact를 고분자 결합제로, RDX(research department explosive)와 유사한 특성을 갖는 dechlorane을 충전제로 사용한 고농축 복합화약 시뮬란트 현탁계의 유변물성을 연구하였다. 회분식 용융혼련기를 사용하여 현탁계의 혼화거동을 조사하였는데 상당한 점성소산열이 발생하였다. 충전율이 70 v% 이상에서는 토크의 지속적인 감소가 있었는데 이는 벽면 미끌어짐 현상에 기인한다고 사료되었다. SEM 관찰 결과 충전제 입자들은 잘 분산되어 있었고 혼화 조건의 영향은 크지 않은 것으로 판단되었다. 현탁계의 뚜렷한 전단박화(shear thinning) 특성으로 인하여 낮은 전단속도의 평판-평판 레오미터에서 측정이 어려운 고충전 현탁계도 높은 전단속도의 모세관 레오미터에서 유변물성 측정이 가능하였다.

3종의 간접수복용 복합레진의 굴곡강도 비교 및 표면관찰 (Evaluation of Flexural strength and surface porosity of three indirect composite resins)

  • 김준태;박진영;김웅철;김지환
    • 대한치과기공학회지
    • /
    • 제39권1호
    • /
    • pp.9-16
    • /
    • 2017
  • Purpose: The purpose of this study was to evaluate flexural strength, composite surface and fractured surface of three different indirect composite resins. Methods: Fifteen bar-shaped specimens ($25mm{\times}2mm{\times}2mm$) were fabricated for each FL group (Flow type and Light curing) and PLP group (Putty type and Light, Pressure curing) and PL group (Putty type and Light curing) according to manufacturer's instructions and ISO 10477. Fabricated specimens were stored in the distilled water for 24 hours at the temperature of $37^{\circ}C$. Three-point bending strength test was performed to measure flexural strength using universal testing machine at a crosshead speed of 1mm/min (ISO 10477). Surface and fractured surface of specimens were observed by digital microscope. Results were analyzed with Kruskal-wallis tests (${\alpha}=0.05$). Results: Mean (SD) of three different indirect composite resins were 83.38 (6.67) MPa for FL group, 139.90(16.53) MPa for PLP group and 171.72(16.74) MPa for PL group. Flexural strength were statistically significant (p<0.05). Differences were not observed at fractured surface among three groups. However, many pores over $100{\mu}m$ were observed at PL group in observing surface of specimen. Conclusion: Flexural strength of composite resins was affected by second polymerization method and content of inorganic filler.

Electrical Properties of the Epoxy Nano-composites according to Additive

  • Shin, Jong-Yeol;Park, Hee-Doo;Choi, Kwang-Jin;Lee, Kang-Won;Lee, Jong-Yong;Hong, Jin-Woong
    • Transactions on Electrical and Electronic Materials
    • /
    • 제10권3호
    • /
    • pp.97-101
    • /
    • 2009
  • The use of a filler material in epoxy composite materials is an essential condition for reducing the unit cost of production and reinforcing mechanical strength. However, the dielectric strength of insulators decreases rapidly due to interactions between the epoxy resin and filler particles. In contrast to existing composite materials, nano-composite materials have superior dielectric strength, mechanical strength, and enduring chemical properties due to an increase in the bond strength of the polymer and nano material, It is reported that nano-fillers provide new characteristics different from the properties of the polymer material. This study is to improve the insulation capability of epoxy resins used in the insulation of a power transformer apparatus and many electronic devices mold. To accomplish this, the additional amount of nano-$SiO_2$ to epoxy resin was changed and the epoxy/$SiO_2$ nano composite materials were made, and the fundamental electrical properties were investigated using a physical properties and an analysis breakdown test. Using allowable breakdown probability, the optimum breakdown strength for designing an electrical apparatus was determined. The results found that the electrical characteristics of the nano-$SiO_2$ content specimens were superior to the virgin specimens. The 0.4 wt% specimens showed the highest electrical properties among the specimens examined with an allowable breakdown probability of 20 %, which indicates stable breakdown strength in insulating machinery design.

NR과 SBR 가황물의 경도와 강성도 대한 온도의 영향 (Effects of temperature on Hardness and Stiffness of NR and SBR Vulcanizates)

  • 진현호;홍창국;조동련;강신영
    • Elastomers and Composites
    • /
    • 제42권3호
    • /
    • pp.143-150
    • /
    • 2007
  • 본 연구에서는 고무제품의 수치 안정성과 성능유지에 직접적으로 영향을 미치는 중요한 특성 중 하나인 온도변화에 따른 고무재료의 경도변화를 고찰하였다. 새롭게 제작된 Inter-national Rubber Hardness Degree(IRHD, Normal type) 경도측정 시험기를 사용하여 미충전된 NR과 SBR 시편의 여러 온도에서 경도변화를 측정하였으며 Young's modulus 값과 비교하였다. NR과 SBR 모두 유리전이온도 근처에서 경도와 Young's modulus의 급격한 변화를 보였다. 온도가 증가함에 따라 경도와 Young's modulus 값이 증가하는 경향을 보였으며 이는 분자의 운동성과 엔트로피 영향으로 해석할 수 있다. 카본블랙과 실리카가 충전된 NR과 SBR의 경우 충전제의 함량이 증가함에 따라 경도에 미치는 온도의 영향이 감소함을 관찰하였다.

고무 복합재료의 압저항 효과 (Rubber Composites with Piezoresistive Effects)

  • 정준호;윤주호;김일;심상은
    • Elastomers and Composites
    • /
    • 제48권1호
    • /
    • pp.76-84
    • /
    • 2013
  • 압저항 효과(piezoresistive effect)는 가해진 외부 압력이나 힘에 의해 전기적 저항이 변하는 것을 말한다. 이러한 압저항 효과는 압력, 진동, 가속 등을 탐지하는 센서에 많이 이용되고 있다. 압저항 효과를 갖는 재료가 많지만 그 중에서도 특히, 전도성 충전제를 첨가한 고무 복합체는 충전제의 종류, 입자 크기, 입자 모양, 입자 종횡비(aspect ratio), 그리고 입자의 양 등을 조절하여 다양한 압력 범위에서의 압저항 효과를 발현할 수 있고, 고무를 기질로 사용함으로써 복합체에 탄성과 유연성을 줄 수 있기 때문에 많은 관심을 받고 있다. 본 논문에서는 압저항 효과의 기본원리 및 다양한 고무 복합체의 압저항 효과에 대해 알아본다.

탄소강과 스테인리스강의 진공브레이징에 관한 연구 (A study on the vacuum brazing of carbon steels to a stainless steel)

  • 이창동;나석주
    • 대한기계학회논문집
    • /
    • 제12권5호
    • /
    • pp.1083-1091
    • /
    • 1988
  • 본 연구에서는 위의 두번째 연구동향과 맥락을 같이하는 것으로서 스테인리스 강(SUS304)에 대한 진공브레이징 연구 및 탄소강의 진공 브레이징에 대한 연구결과들 을 토대로 하여 SUS304와 탄소강과의 진공브레이징 현상을 연구하였는데 특히 모재의 탄소함유량, 브레이징시간 및 접합부 틈새(joint clearance)등에 따라 접합부에 나타 나는 여러 금속학적 현상의 규명 및 접합강도(joint strength)에 대해 변수들이 미치 는 영향을 연구 하였다.

Fiber Surface Engineering to Improve Papermaking Raw Material Quality

  • Wang Eugene I-Chen;Perng Yuan Shing
    • 한국펄프종이공학회:학술대회논문집
    • /
    • 한국펄프종이공학회 2006년도 PAN PACIFIC CONFERENCE vol.2
    • /
    • pp.271-278
    • /
    • 2006
  • We used polymers of alternating cationic and anionic nature to build up shells on fiber surfaces, strengthen the worn-out fibers and improve paper properties made from such fibers. OCC and ONP pulps were either dipped or salted out in the cationic polyallylamine, polyacrylamide and starch solutions. After centrifugal drying, these were followed by treatments in anionic polyacrylic acid, poly-acrylamide, and starch solutions, respectively. The shell-enhanced fibers were formed into handsheets and their physical properties evaluated. The results show that building multiple shells on worn-out fiber surfaces can strengthen the fibers and paper. The simpler and more practical impregnation-centrifuging treatment provided the desired effects, whereas salting out the polymers produced somewhat superior fibers. The latter process, were impractical, however. The first pair of polymeric shells imparted marked strength improvement, whereas later layers had diminishing efficacies. Overall, the methods can improve fiber quality, attaining paper strength requirements without resorting to expensive measures. Alternate cationic polymer and filler powders were also deposited on fiber surface based on the micriparticle system in an anticipation of stiffness gains. Platy minerals, such as montmorillonite, bentonite, sericite, clay and talc were added following cationic PAM. After dewatering of polymer-pigment shelled fiber of one to 3 pairs of layers, handsheets either calendered or uncalendered were evaluated. The results indicate that regardless of calendaring, stiffness of the handsheets did not improve appreciably while certain other strength properties showed gains. We also attempted the novel starch gel filler addition method wherein tapioca starch and filers (PCC, sericite or clay) were mixed at high solids content of 50% and cooked until gelatinized. The filled handsheets were dried under various conditions and then tested for their properties. Improvements in strengths of modified filled paper were observed.

  • PDF

혼합물 실험계획법을 이용한 유색 EPDM의 첨가제 배합비에 따른 기계적 특성 분석 (Analysis of Mechanical Properties of Colored EPDM Based on Additive Mixing Ratio Using Mixture Design of Experimental Method)

  • 박윤아;전의식;김영신;이현승
    • 한국기계가공학회지
    • /
    • 제21권8호
    • /
    • pp.79-86
    • /
    • 2022
  • With the recent increase in the demand for electric vehicles, it is necessary to identify the high current safety of automobile parts. Among the automobile parts, the EPDM parts required colored parts from the existing black; therefore, it was necessary to change the basic filler from carbon black to silica. The rubber used in automobile parts is flexible and exhibits basic characteristics of high strength and elongation. However, as the filler is changed to silica, its physical properties, such as tensile strength and elongation, are lower than those of the existing carbon black base. Therefore, it is necessary to evaluate the mechanical properties with the addition of the EPDM compound using silica as a base without degrading the physical properties of EPDM. In this study, an experiment based on the additive content was performed using the mixture experimental planning method to analyze the mechanical properties according to the additive type and mixing ratio of silica-based EPDM. The mixing ratio of the four additives was set using a simplex lattice design, and the tensile strength, elongation, modulus 300%, and permanent compression reduction rate were analyzed for mechanical characteristics, and rheometer experiments were performed for vulcanization characteristics. Through statistical analysis of the measured data, the main effects and interactions of the EPDM-blended rubber additives were analyzed. These results can be used to derive a mixing ratio of additives that satisfies the required characteristics of the EPDM compound.