• Bulletin of the Korean Chemical Society
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• v.18 no.6
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• pp.588-594
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• 1997

Gelation time, gel structure and volatility of by-products during gelation of PZT sol-gel processing were investigated by FT-IR spectroscopy. FT-IR spectroscopic study was performed on PZT gels with the various H₂O contents (1, 2 and 3 mol) and the several types (HNO₃, NH₄OH) and amounts (0.1, 0.2 mol) of catalysts, monitoring temporal (0, 1, 3, 10 weeks, 3 months and 3 years) and thermal (100-700 ℃) changes of FT-IR spectra. The interpretation of temporal change of the spectra revealed two trends. One is under the condition of 1 mol H₂O, 1 mol H₂O+0.1 mol HNO₃, 3 mol H₂O and the other is for 1 mol H₂O+0.1 mol NH₄OH, 2 mol H₂O, 1 mol H₂O+0.2 mol HNO₃. The gel structures and the gelation times for these conditions were discussed in comparison with the reported results of SiO₂, and we suggested the reaction mechanisms for these structural characteristics. Thermal variation of FT-IR spectra was interpreted as the evolution processes of gel by investigating the evaporation of solvent and the decomposition of organic residues.

• Applied Chemistry for Engineering
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• v.22 no.5
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• pp.579-581
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• 2011

Spectroscopic evaluation of hair chemical damage was performed by SEM/EDS, CLSM, and FT-IR spectroscopy. In SEM/EDS, hydrogen peroxide treated hair showed the loose packing of surface scales, lower ratio of sulfur element and higher ratio of oxygen atom. In the optical single section by using CLSM, high fluorescent intensity appeared in untreated hair. However, in case of treated hair, low fluorescent intensity appeared. This results the aromatic amino acids which can be autofluorescent were more abundant than bleached hair. FT-IR spectra showed that cysteic acid band intensity was increased by performing the bleaching treatments. These results indicate that the oxidative damage cleaves the S-S bond and results in the lower working force of hair fiber.

• Applied Chemistry for Engineering
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• v.22 no.5
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• pp.582-585
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• 2011

In this study, surface-adsorbed species of 1,2-dichlorobenzene (1,2-DCB) on mesoporous $V_2O_5/TiO_2$ catalysts synthesized by spray pyrolysis were investigated through the adsorption/desorption performed using in situ FT-IR cell. Also, the comparison of adsorbed species with $TiO_2$ and $V_2O_5/TiO_2$ synthesized by the incipient wetness was carried out.

• Analytical Science and Technology
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• v.18 no.1
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• pp.1-4
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• 2005

The stable $Ti(OPr^i)_2(OAc)_2$ sol which reacts with a solution of prehydrolysed $Si(OEt)_4$ was made by addition of acetic acid. The structure evolution of the reaction mixture was monitered by $^1H$, $^{29}Si$ NMR and FT-IR spectroscopy.

• Journal of the Korean Crystal Growth and Crystal Technology
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• v.8 no.2
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• pp.292-298
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• 1998

${\alpha}-Fe_2O_3$films were prepared by a dip-coating method using the mixed solution of ferric nitrate, ethylene glycol and acethyl acetone. The polymerization effect of the mixed solution was studied by FT-IR spectroscopic analysis, and the decomposition of organic parts and crystallization of the dip-coated film were investigated by FT-IR, XRD and DSC. In addition, AFM and SEM were employed to analyze the surface roughness and the thickness of ${\alpha}-Fe_2O_3$films.

• KSBB Journal
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• v.11 no.5
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• pp.557-564
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• 1996

The interaction between poly(2-hydroxyethylmethacrylate)(poly(HEMA)) which is a material of contact lens containing approximately 45%o water and water soluble amino acids (alanine, arginine, glycine, lysine, methionine, proline, and serine) was investigated by using FT-IR and Raman spectroscopy. The results revealed that arginine and lysine had the strongest interaction with poly(HEMA) among amino acids. The interaction depended on the quantity of charges on ammo acids. They interacted predominately with hydroxyl groups in poly(HEMA).

• Proceedings of the KSR Conference
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• 2008.06a
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• pp.2213-2217
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• 2008

The important factor is keeping the temperature condition in quantifying several toxic components in combustion gases. In case of not keeping the temperature as it was in combustion, the change of component and concentration of smoke gases was inevitable. To solve this problem, FT-IR spectroscopy with gas cell was applied. But, there is also a difficulty in quantitative analysis of specific toxic component because of water vapor. Thus, in this study, water vapor FT-IR spectra with different concentrations were obtained and applied them to quantitative analysis.

• Journal of Applied Biological Chemistry
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• v.49 no.1
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• pp.8-10
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• 2006

Compositions of methionine-metal chelates have been investigated by FT-IR and XRD studies to elucidate their molecular structures. It was concluded that Copamin and Zincamin contain a high percentage of crystalline products, presumably 2:1 Methionine-Cu or Zn complexes. On the contrary, FT-IR and XRD spectra of Ferramin didn't show any characteristics of the chelate and it was concluded to contain major components of starting $FeSO_4$ and methionine without chelation.

• Analytical Science and Technology
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• v.34 no.1
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• pp.17-22
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• 2021

In this study, flame retardant mixtures of decabromodiphenylethane (DBDPE) and Sb2O3 were analyzed using Fourier transform infrared (FT-IR) spectroscopy. The experimentally obtained wavenumbers of DBDPE and Sb2O3 were 1321 and 949 cm-1, respectively, whereas those obtained by theoretical calculation were 1370 and 818 cm-1, respectively. Strong correlation was observed between the mixing molar ratios and observed peak area ratios, suggesting that FT-IR analysis can be used to obtain relative amounts of the individual components of flame retardant mixture.

• Proceedings of the Materials Research Society of Korea Conference
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• 1992.05a
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• pp.68-69
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• 1992