• Title/Summary/Keyword: FE analysis method

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Synthesis and spectroscopic characterization of zinc ferrite nanoparticles

  • Arora, Shefali;Nandy, Subhajit;Latwal, Mamta;Pandey, Ganesh;Singh, Jitendra P.;Chae, Keun H.
    • Advances in nano research
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    • v.13 no.5
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    • pp.437-451
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    • 2022
  • Synthesis approaches usually affect the physical and chemical properties of ferrites. This helps ferrite materials to design them for desired applications. Some of these methods are mechanical milling, ultrasonic method, micro-emulsion, co-precipitation, thermal decomposition, hydrothermal, microwave-assisted, sol-gel, etc. These methods are extensively reviewed by taking example of ZnFe2O4. These methods also affect the microstructure and local structure of ferrite which ultimately affect the physical and chemical properties of ferrites. Various spectroscopic techniques such as Raman spectroscopy, Fourier Transform Infrared spectroscopy, Ultra Violet-Visible spectroscopy, Mossbauer spectroscopy, extended x-ray absorption fine structure, and electron paramagnetic resonance are found helpful to reveal this information. Hence, the basic principle and the usefulness of these techniques to find out appropriate information in ZnFe2O4 nanoparticles is elaborated in this review.

Caption Detection and Recognition for Video Image Information Retrieval (비디오 영상 정보 검색을 위한 문자 추출 및 인식)

  • 구건서
    • Journal of the Korea Computer Industry Society
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    • v.3 no.7
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    • pp.901-914
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    • 2002
  • In this paper, We propose an efficient automatic caption detection and location method, caption recognition using FE-MCBP(Feature Extraction based Multichained BackPropagation) neural network for content based retrieval of video. Frames are selected at fixed time interval from video and key frames are selected by gray scale histogram method. for each key frames, segmentation is performed and caption lines are detected using line scan method. lastly each characters are separated. This research improves speed and efficiency by color segmentation using local maximum analysis method before line scanning. Caption detection is a first stage of multimedia database organization and detected captions are used as input of text recognition system. Recognized captions can be searched by content based retrieval method.

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Determination of Heavy Metals Concentrations in Urban Air using ICP Method : in the Area of Chung-Ang University (ICP법에 의한 도시대기중 중금속 농도 측정: 중앙대학교를 중심으로)

  • 손동헌;신혜숙;정성윤;정원태
    • Journal of Korean Society for Atmospheric Environment
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    • v.9 no.3
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    • pp.222-229
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    • 1993
  • Total suspended particles in the atmosphere were collected on the quartz fiber filters using an ANdersen Hi-volume air sampler from March 1989 to October 1989 and from June 1990 to February 1991, at Chung-Ang University in Seoul. A total amount of eight heavy metals (Cr, Zn, Cd, Pb, Fe, V, Ti, Mn) in total suspended particles were determined by ICP spectrophotometer. The annual arithmetic mean concentration of total suspended particle was 162.3$\mug/m^3$ and eight metals(Cr, Zn, Cd, Pb, Fe, V, Ti, Mn) were 11.6, 609.2, 3.5, 337.1, 2739.5, 15.1, 89.4 and 100.5ng/$m^3$, respectively. The concentration of total suspended particle was highest in the spring(343.7$\mug/m^3$) and lowest in the summer(91.8$\mug/m^3$). These heavy metals were distinguished into two groups in terms of their particle size distribution. The contents of first-group heavy metals (Fe, Ti, Mn) were increased in accordance with the growth of the particle size. The contents of the second-group ones such as Pb, Cd, V, and Zn, on the contrary, came to increase according as the particle size reduced. Statistical analysis indicated that there was a correlation between total suspended particle and Fe in coarse particles, and between total Suspended Particle and Zn, Pb in fine particle.

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Effect of Ni Bond Coat on Adhesive Properties of Fe Coating Thermal Sprayed on Al Substrate (Ni 본드코팅이 Al 기지에 고온 용사 코팅된 Fe 코팅층의 접합특성에 미치는 영향)

  • Kwon, Eui-Pyo;Kim, Dae-Young;Lee, Jong-Kweon
    • Korean Journal of Materials Research
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    • v.26 no.10
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    • pp.542-548
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    • 2016
  • The influence of NiCrAlY bond coating on the adhesion properties of an Fe thermal coating sprayed on an Al substrate was investigated. By applying a bond coat, an adhesion strength of 21MPa was obtained, which was higher than the 15.5MPa strength of the coating without the bond coat. Formation of cracks at the interface of the bond coat and the Al substrate was suppressed by applying the bond coat. Microstructural analysis of the coating interface using EBSD and TEM indicated that the dominant bonding mechanism was mechanical interlocking. Mechanical interlocking without crack defects in the coating interface may improve the adhesion strength of the coating. In conclusion, the use of an NiCrAlY bond coat is an effective method of improving the adhesion properties of thermal sprayed Fe coatings on Al substrates.

FATIGUE LIFE ASSESSMENT OF REACTOR COOLANT SYSTEM COMPONENTS BY USING TRANSFER FUNCTIONS OF INTEGRATED FE MODEL

  • Choi, Shin-Beom;Chang, Yoon-Suk;Choi, Jae-Boong;Kim, Young-Jin;Jhung, Myung-Jo;Choi, Young-Hwan
    • Nuclear Engineering and Technology
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    • v.42 no.5
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    • pp.590-599
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    • 2010
  • Recently, efficient operation and practical management of power plants have become important issues in the nuclear industry. In particular, typical aging parameters such as stress and cumulative usage factor should be determined accurately for continued operation of a nuclear power plant beyond design life. However, most of the major components have been designed via conservative codes based on a 2-D concept, which do not take into account exact boundary conditions and asymmetric geometries. The present paper aims to suggest an effective fatigue evaluation methodology that uses a prototype of the integrated model and its transfer functions. The validity of the integrated 3-D Finite Element (FE) model was proven by comparing the analysis results of individual FE models. Also, mechanical and thermal transfer functions, known as Green's functions, were developed for the integrated model with the standard step input. Finally, the stresses estimated from the transfer functions were compared with those obtained from detailed 3-D FE analyses results at critical locations of the major components. The usefulness of the proposed fatigue evaluation methodology can be maximized by combining it with an on-line monitoring system, and this combination, will enhance the continued operations of old nuclear power plants.

Preparation and Electromagnetic Properties of an Electromagnetic Wave Absorber

  • Sun, Chang;Sun, Kangning;Pang, Laixue;Liu, Jian
    • Journal of Magnetics
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    • v.21 no.1
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    • pp.61-64
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    • 2016
  • In this study, we report the as-prepared MgO-doped $BaFe_{12}O_{19}$, which was prepared by calcination technique and high-energy ball milling process, as an electromagnetic wave absorber. The phase analysis of $BaFe_{12}O_{19}$ and the as-prepared MgO-doped $BaFe_{12}O_{19}$ was detected utilizing X-ray Diffractometer (XRD). The microstructure was characterized using Scanning Electron Microscope (SEM). By means of the transmission/reflection coaxial line method, the electromagnetic properties and microwave absorbing properties of the as-prepared electromagnetic wave absorber were studied. It is found that the electromagnetic wave absorber has a minimum reflection loss value of -41 dB at 4.27 GHz with a matching thickness of 2.6 mm. The experiment results revealed that the as-prepared electromagnetic wave absorber could find potential applications in many military as well as commercial industries.

The Construction of Initial Analytical Models Structural Health Monitoring of a Masonry Structure

  • Kim, Seonwoong;Kim, Ji Young;Hwang, In Hwan
    • International Journal of High-Rise Buildings
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    • v.4 no.3
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    • pp.191-198
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    • 2015
  • It is important to accurately predict structural responses to external excitations such as typhoons and earthquakes when designing structures for serviceability. One of the key procedures to predict reliable vibration responses is to evaluate accurate structural dynamic properties using finite element (FE) models, which properly represent the realistic behavior of buildings. In the case of historic masonry buildings, structural damage could also be caused by ambient vibrations or impacts. Therefore, the preservation plans of historic buildings for low-level vibrations or impacts should be provided by analyzing structural damages within serviceability levels. For this purpose, it is required to provide FE model construction and response analysis methods verified with field measurement data. In this research, long-term field measurement was performed for a cathedral and its dynamic properties were evaluated using measured data. Then, the model was calibrated based on the measured dynamic properties and an overall construction method for the masonry cathedral was proposed. Using the measured accelerations, the vibrations of the belfry were analyzed using the calibrated FE model and finally, the FE model for the cathedral was verified by comparing the measured accelerations with the modeled results.

Pattern Classification of PM -10 in the Indoor Environment Using Disjoint Principal Component Analysis (분산주성분 분석을 이용한 실내환경 중 PM-10 오염의 패턴분류)

  • 남보현;황인조;김동술
    • Journal of Korean Society for Atmospheric Environment
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    • v.18 no.1
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    • pp.25-37
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    • 2002
  • The purpose of the study was to survey the distribution patterns of inorganic elements of PM-10 in the various indoor environments and analyze the pollution patterns of aerosol in various places of indoor environment using a pattern recognition method based on cluster analysis and disjoint principal component analysis. A total of 40 samples in the indoor had been collected using mini-vol portable samplers. These samples were analyzed for their 19 bulk inorganic compounds such as B, Na, Mg, Al, K, Ca, Ti, V, Cr, Fe, Ni, Cu, Zn, As, Se, Cd, Ba, Ce, and Pb by using an ICP-MS. By applying a disjoint principal component analysis, four patterns of the indoor air pollutions were distinguished. The first pattern was identified as a group with high concentrations of PM-10, Na, Mg, and Ca. The second pattern was identified as a group with high concentrations B, Mg, At, Ca, Fe, Cu, and Ba. The third pattern was a group of sites with high concentrations of K, Zn. Cd. The fourth pattern was a group with low concentrations PM-10 and all inorganic elements. This methodology was found to be helpful enough to set the criteria standard of indoor air quality, corresponding pollutants, and classification of indoor environment categories when making an indoor air quality law.

Fe-doped beta-tricalcium phosphate; crystal structure and biodegradable behavior with various heating temperature (Fe 이온 치환 beta-tricalcium phosphate의 하소 온도에 따른 미세구조 및 분해 특성)

  • Yoo, Kyung-Hyeon;Kim, Hyeonjin;Sun, Woo Gyeong;Yoon, Seog-Young
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.30 no.6
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    • pp.244-250
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    • 2020
  • β-Tricalcium phosphate (β-TCP, Ca3(PO4)2) is a kind of biodegradable calcium phosphate ceramics with chemical and mineral compositions similar to those of bone. It is a potential candidate for bone repair surgery. To improve the bioactivity and osteoinductivity of β-TCP, various ions doped calcium phosphate have been studied. Among them, Iron is a trace element and its deficiency in the human body causes various problems. In this study, we investigated the effect of Fe ions on the structural variation, degradation behavior of β-TCP. Fe-doped β-TCP powders were synthesized by the coprecipitation method, and the heat treatment temperature was set at 925 and 1100℃. The structural analysis was carried out by Rietveld refinement using the X-ray diffraction results. Fe ions existed in a different state (Fe2+ or Fe3+) with different heat treatment temperatures, and the substitution sites (Ca-(4) and Ca-(5)) also changed with temperature. The degradation rate was fastest at Fe-doped β-TCP with heated at 1100℃. The cell viability behavior was also enhanced with the substitution of Fe ions. Therefore, the substitution of Fe ion has accelerated the degradation of β-TCP and improved the biocompatibility. It could be more utilized in biomedical devices.