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Monolithic zirconia crowns: effect of thickness reduction on fatigue behavior and failure load

  • Prott, Lea Sophia;Spitznagel, Frank Akito;Bonfante, Estevam Augusto;Malassa, Meike Anne;Gierthmuehlen, Petra Christine
    • The Journal of Advanced Prosthodontics
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    • v.13 no.5
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    • pp.269-280
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    • 2021
  • PURPOSE. The objective of this study was to evaluate the effect of thickness reduction and fatigue on the failure load of monolithic zirconia crowns. MATERIALS AND METHODS. 140 CAD-CAM fabricated crowns (3Y-TZP, inCorisTZI, Dentsply-Sirona) with different ceramic thicknesses (2.0, 1.5, 1.0, 0.8, 0.5 mm, respectively, named G2, G1.5, G1, G0.8, and G0.5) were investigated. Dies of a mandibular first molar were made of composite resin. The zirconia crowns were luted with a resin composite cement (RelyX Unicem 2 Automix, 3M ESPE). Half of the specimens (n = 14 per group) were mouth-motion-fatigued (1.2 million cycles, 1.6 Hz, 200 N/ 5 - 55℃, groups named G2-F, G1.5-F, G1-F, G0.8-F, and G0.5-F). Single-load to failure was performed using a universal testing-machine. Fracture modes were analyzed. Data were statistically analyzed using a Weibull 2-parameter distribution (90% CI) to determine the characteristic strength and Weibull modulus differences among the groups. RESULTS. Three crowns (21%) of G0.8 and five crowns (36%) of G0.5 showed cracks after fatigue. Characteristic strength was the highest for G2, followed by G1.5. Intermediate values were observed for G1 and G1-F, followed by significantly lower values for G0.8, G0.8-F, and G0.5, and the lowest for G0.5-F. Weibull modulus was the lowest for G0.8, intermediate for G0.8-F and G0.5, and significantly higher for the remaining groups. Fatigue only affected G0.5-F. CONCLUSION. Reduced crown thickness lead to reduced characteristic strength, even under failure loads that exceed physiological chewing forces. Fatigue significantly reduced the failure load of 0.5 mm monolithic 3Y-TZP crowns.

BINDING NUMBER AND HAMILTONIAN (g, f)-FACTORS IN GRAPHS

  • Cai, Jiansheng;Liu, Guizhen
    • Journal of applied mathematics & informatics
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    • v.25 no.1_2
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    • pp.383-388
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    • 2007
  • A (g, f)-factor F of a graph G is Called a Hamiltonian (g, f)-factor if F contains a Hamiltonian cycle. The binding number of G is defined by $bind(G)\;=\;{min}\;\{\;{\frac{{\mid}N_GX{\mid}}{{\mid}X{\mid}}}\;{\mid}\;{\emptyset}\;{\neq}\;X\;{\subset}\;V(G)},\;{N_G(X)\;{\neq}\;V(G)}\;\}$. Let G be a connected graph, and let a and b be integers such that $4\;{\leq}\;a\;<\;b$. Let g, f be positive integer-valued functions defined on V(G) such that $a\;{\leq}\;g(x)\;<\;f(x)\;{\leq}\;b$ for every $x\;{\in}\;V(G)$. In this paper, it is proved that if $bind(G)\;{\geq}\;{\frac{(a+b-5)(n-1)}{(a-2)n-3(a+b-5)},}\;{\nu}(G)\;{\geq}\;{\frac{(a+b-5)^2}{a-2}}$ and for any nonempty independent subset X of V(G), ${\mid}\;N_{G}(X)\;{\mid}\;{\geq}\;{\frac{(b-3)n+(2a+2b-9){\mid}X{\mid}}{a+b-5}}$, then G has a Hamiltonian (g, f)-factor.

A Study on the Development of a Microbial Insecticide -(With special emphasis on formulation)- (미생물(微生物) 살충제(殺蟲劑)의 개발(開發)에 관(關)한 연구(硏究) -(제제화(製劑化)를 중심(中心)으로)-)

  • Lee, Jae-Koo;Kim, Ki-Cheol;Kim, Do-Young
    • Applied Biological Chemistry
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    • v.22 no.2
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    • pp.123-134
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    • 1979
  • For the purpose of developing a microbial insecticide utilizing Bacillus thuringiensis Berliner, research was done and the following results were obtained. 1) As the freeze-dried matter of the cocoon-cooked water discarded from the filature contains much crude protein(51.825%) and a lot of inorganic salts, it can make a good nutrition source for the culture cf B. thuringiensis Berliner. 2) Based on the suspensibility, formula F-5 turned out to be the most suitable for insecticidal use. Its composition includes 0.2 g of the cell-spore-crystal mixture, 25 g of 200-mesh kaolin, 2.5 g of New Kalgen-NX-150, and 2.5 g of glycerine admixed with 8 ml of distilled water and granulated in 80-mesh size. 3) All the components of F-5, F-6 and F-7 are identical except that the amounts of cell-spore-crystal mixture of F-5, F-6, and F-7 are 0.2 g, 0.4 g, and 0.6 g, respectively. Accordingly, their physical properties are almost all the same. 4) Formulas F-5, F-6, and F-7 exhibited an excellent toxicity to Anomis mesogona Walker, Dendrolimus spectabilis Butler, and Margaronia perspectalis Walker at the concentration of 5%. 5) Formulas F-8 and F-9 which contain $NaHCO_3$ as one of their components showed a remarkably reduced toxicity to Anomis mesogona Walker and Dendrolimus spectabilis Butler than F-6 which does not contain $NaHCO_3$. 6) A maximum of $2.97{\times}10^9$ spores per ml was obtained by incubating B. thuringiensis in M-3 which has a pH of 7.05 and comprises 0.2% of ammonium sulphate and 0.8% of glucose dissolved in the cocoon-cooked water, with aeration for 96 hours. 7) Formula F-6 exhibited a somewhat reduced toxicity to Anomis mesogona Walker and Dendrolimus spectabilis Butler, when stored at room temperature for 70 days after formulation and it is desirable to keep it in a dark and cold place. 8) In held applications, formula F-6 showed a good activity in controlling Monema flavescens Walker. Margaronia perspectalis Walker, and Macrosiphum ibarae Matsumura.

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GENERALIZED HYERES{ULAM STABILITY OF A QUADRATIC FUNCTIONAL EQUATION WITH INVOLUTION IN QUASI-${\beta}$-NORMED SPACES

  • Janfada, Mohammad;Sadeghi, Ghadir
    • Journal of applied mathematics & informatics
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    • v.29 no.5_6
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    • pp.1421-1433
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    • 2011
  • In this paper, using a fixed point approach, the generalized Hyeres-Ulam stability of the following quadratic functional equation $f(x+y+z)+f(x+{\sigma}(y))+f(y+{\sigma}(z))+f(x+{\sigma}(z))=3(f(x)+f(y)+f(z))$ will be studied, where f is a function from abelian group G into a quasi-${\beta}$-normed space and ${\sigma}$ is an involution on the group G. Next, we consider its pexiderized equation of the form $f(x+y+z)+f(x+{\sigma}(y))+f(y+{\sigma}(z))+f(x+{\sigma}(z))=g(x)+g(y)+g(z)$ and its generalized Hyeres-Ulam stability.

Luminous efficiency of ZnS:Sm,F TFEL devices (ZnS:Sm,F 형광체 박막 EL 소자의 발광효율)

  • 최광호;임영민;이철준;장보현
    • Korean Journal of Optics and Photonics
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    • v.3 no.2
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    • pp.111-116
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    • 1992
  • ZnS:Sm, F TFEL devices with double insulating layer are prepared by e-beam evaporation method. Electroluminescence and luminous efficiency of the device fabricated at various conditions are investigated. The main transitions on the emission spectra for ZnS:Sm, F TFEL device occur at$^4G_{5/2}\to^6H_{9/2}^4G_{5/2}\to^6H_{7/2}, \;^4G_{5/2}\to^6H_{5/2}\to$.Among them, the dominant spectral line and its corresponding transition occur at $^4G_{5/2}\to^6H_{9/2}$(650 nm) and results in an orange-red emission color. The optimum concentration and substrate temperature for the ZnS:Sm, F TFEL device are around 1 wt% and $200^{\circ}C$. Luminous efficiency for the device is the largest at optimum condition.

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Crossability, Variation in Chromosome Number, and Agronomic Characters in Hybrid of Hexaploid Triticale with Tetraploid Rye (6배체 트리티케일과 4배체호밀 교잡에서의 교잡율, 염색체수 변이 및 작물학적 특성)

  • 황종진;하용웅;이홍석
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.37 no.4
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    • pp.305-312
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    • 1992
  • This experiment was carried out to investigate seed set, variation in chromosome number, and agronomic characteristics of the progeny in the cross between hexaploid triticale variety, Sinkihomil(P$_1$) and tetraploid rye variety, Dooroohomil(P$_2$). Seed set rate obtained was 30.5% in the cross of Sinkihomil with Dooroohomil, whereas 3.26% in reciprocal cross using Dooroohomil as female. Alsoseed set was 8.75% in F$_1$/P$_1$, 7.20% in F$_1$/P$_2$, and 1.53% in F$_2$(=F$_1$ /F$_1$, respectively. Germination rate of crossed seed was 37% in cross of P$_1$ with P$_2$, 39.0% in F$_1$/P$_1$(BC$_1$), 50% in F$_1$/P$_2$(BC$_2$) and 43.0% in F$_1$/F$_1$(F$_2$), and 1,000 grain wight was 20.7g in the cross of P$_1$ with P$_2$, which have 41.9g and 47.7g, respectively, 24.5g in F$_1$/P$_1$, 23.6g in F$_1$/P$_2$, and 24.5g in F$_1$/F$_1$, respectively. In pollen fertility of F$_1$ plant, 69.8% turned out to be abnormal or sterile pollen grains, whereas 30.2% was fertile or normal. In meiosis of pollen mother cell of F$_1$ plant, 13.5 univalents, 8.89 bivalent and 1.24 trivalent were appeared. Somatic chromosome number of 35 in F$_1$, both 32 to 33 and 35 to 36 in F$_2$, 35 to 39 in BC$_1$ and 28 to 36 in BC$_2$ which mean producing female gamate was 14 to 18 chromosome in PMC of F$_1$ plant. Rate of fertile plant turned out to be 100% in F$_1$, 4.5% in F$_2$, 42.9% in BC$_1$, and 50.0% in BC$_2$, respectively. Number of seed set per spike appeared to be 1.17 in F$_1$ plant, 13.3 in F$_2$, 2.36 in BC$_1$, and 3.75 in BC$_2$, respectively. Days to heading of F$_1$ was intermediate, but F$_2$ was later than both parents. Plant height of F$_1$ , BC$_1$ ,and BC$_2$ was shorter than both parent, but F$_2$, longer than both parents.

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BINDING NUMBERS AND FRACTIONAL (g, f, n)-CRITICAL GRAPHS

  • ZHOU, SIZHONG;SUN, ZHIREN
    • Journal of applied mathematics & informatics
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    • v.34 no.5_6
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    • pp.435-441
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    • 2016
  • Let G be a graph, and let g, f be two nonnegative integer-valued functions defined on V (G) with g(x) ≤ f(x) for each x ∈ V (G). A graph G is called a fractional (g, f, n)-critical graph if after deleting any n vertices of G the remaining graph of G admits a fractional (g, f)-factor. In this paper, we obtain a binding number condition for a graph to be a fractional (g, f, n)-critical graph, which is an extension of Zhou and Shen's previous result (S. Zhou, Q. Shen, On fractional (f, n)-critical graphs, Inform. Process. Lett. 109(2009)811-815). Furthermore, it is shown that the lower bound on the binding number condition is sharp.

A NOTE ON EXTREMAL LENGTH AND CONFORMAL IMBEDDINGS

  • Chung, Bo-Hyun
    • Journal of applied mathematics & informatics
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    • v.28 no.5_6
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    • pp.1315-1322
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    • 2010
  • Let D be a plane domain whose boundary consists of n components and $C_1$, $C_2$ two boundary components of D. We consider the family $F_1$ of conformal mappings f satisfying f(D) $\subset$ {1 < |w| < ${\mu}(f)$}, $f(C_1)=\{|w|=1\}$, $f(C_2)=\{|w|={\mu}(f)\}$. There are conformal mappings $g_0$, $g_1({\in}F_1)$ onto a radial and a circular slit annulus respectively. We obtain the following theorem, $$\{{\mu}(f)|f\;{\in}\;F_1\}=\{\mu|\mu(g_1)\;{\leq}\;{\mu}\;{\leq}\;{\mu}(g_0)\}$$. And we consider the family $F_n$ of conformal mappings $\tilde{f}$ from D onto a covering surfaces of the Riemann sphere satisfying some conditions. We obtain the following theorems, {$\mu|1$ < ${\mu}\;{\leq}\;{\mu}(g_1)$} ${\subset}\;\{{\mu}(\tilde{f})|\tilde{f}\;{\in}\;F_2\}\;{\subset}\;\{{\mu}(\tilde{f})|\tilde{f}\;{\in}\;F_n\}$ and ${\mu}(\tilde{f})\;{\leq}\;{\mu}(g_0)^n$.

Friction and Wear Behaviors of WC-Co/WC-Co Pairs in Air

  • Hosokawa, H.;Nakajima, T.;Shimojima, K.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09a
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    • pp.629-630
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    • 2006
  • To investigate sliding friction and wear behaviors of WC-Co/WC-Co pairs containing different WC grain sizes, the ball-on-disc test in air were carried out, where WC grain sizes a $0.5\;{\mu}m$ (F.G.) and $1.5\;{\mu}m$ (C.G.). The wear volume of F.G. pin for F.G. pin/C.G. disc is larger than that of F.G. pin for F.G. pin/F.G. disc due to higher friction coefficient, and the surfaces after wear test are richer in oxygen compared to those before test. Furthermore, the wear debris, which is composed of nona-scale grain, after the wear test are remarkably richer in oxygen than to those before test.

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Biosorption of Lead and Cadmium by Fucoidan from Undariafinnatifida (미역 포자엽 fucoidan의 중금속 흡착 특성)

  • KOO Jae-Geun
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.34 no.5
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    • pp.521-525
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    • 2001
  • Screening tests of different fucoidan fractions from Sporophylls of Undazia pinnatifida, Laminaria religiosa, Hizikia fusiforme and Sagassum fulvellum revealed that the highest biosorptive Pb and Cd uptake fraction was Undaria finnatifida Fr-3.0 prepared by dissolving the precipitated complex (crude fucoidan and cetylpyridinum chloride) with 3.0 M $CaCl_2$ solution, The Pb and Cd uptake by Undaria finnatifida Fr-3.0 was quantitatively evaluated using sorption isotherms and Langmuir sorption model. The Pb and Cd uptake by Undaria finnatifida Fr-3.0 increased with increasing pH values at high equilibrium residual concentration. The highest experimentally observed Pb and Cd uptake value in the sorption isotherm for pH 5.5 were 94 mg/g (at $C_f=164\;mg/L$) and 64 mg/g (at $C_f=197\;mg/L$) respectively, and $q_{max}$ of Pb and Cd calculated by Langmuir sorption model were 178 mg/g and 122 mg/g, respectively. In the low equilibrium concentration range, up to 20 mg/L, the Pb uptake remained unchanged in the presence of Cd, but decreased at higher equilibrium concentration range.

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