• Title/Summary/Keyword: Extraction Process

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Simultaneous Extraction and Separation of Oil and Azadirachtin from Seeds and Leaves of Azadirachta indica using Binary Solvent Extraction

  • Subramanian, Sheela;Salleh, Aiza Syuhaniz;Bachmann, Robert Thomas;Hossain, Md. Sohrab
    • Natural Product Sciences
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    • v.25 no.2
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    • pp.150-156
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    • 2019
  • Conventional extraction of oil and azadirachtin, a botanical insecticide, from Azadirachta indica involves defatting the seeds and leaves using hexane followed by azadirachtin extraction with a polar solvent. In order to simplify the process while maintaining the yield we explored a binary extraction approach using Soxhlet extraction device and hexane and ethanol as non-polar and polar solvents at various ratios and extraction times. The highest oil and azadirachtin yields were obtained at 6 h extraction time using a 50:50 solvent mixture for both neem leaves (44.7 wt%, $720mg_{Aza}/kg_{leaves}$) and seeds (53.5 wt%, $1045mg_{Aza}/kg_{leaves}$), respectively.

Optimization of Extraction Process for Mass Production of Paclitaxel from plant Cell Cultures (Paclitaxel 대량생산을 위한 추출공정 최적화)

  • 김진현
    • KSBB Journal
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    • v.15 no.4
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    • pp.346-351
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    • 2000
  • Several solvents or combinations of solvents were tested for the extraction of wet or dried biomass at different extraction mode from plant cell cultures. Methanol gave the highest paclitaxel recovery with the least amount of solvent usage. before extraction drying of biomass wass helpful to decrease solvent usage in extraction step./ in this case drying method was very important to obtain high yield from dried biomass. In thid mode of operation counter-current extraction process can be able to decrease solvent usage but paclitaxel recovery was almost same with both batch and counter-current mode of operation. The number of extraction times was at least four to obtain high yield(>99%) from cell and one to obtain highyield(>96%) from cell debris in batch mode. Equilibrium (i.e. the ratio of paclitaxel in biomass to paclitaxel in the extraction solvent) was reached within 5 minutes. The minimum methodal concentration (90%) and solvent amount(biomass : solvent=1 Kg : 1L) are enough to obtain high yield(>98%) for extraction from biomass.

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Antioxidant Characteristics of Artemisis capillaris Hot-water Extract Using Response Surface Methodology (반응표면분석법을 이용한 인진쑥 열수추출물의 항산화적 특성)

  • Kim, Seong-Ho
    • Journal of Life Science
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    • v.24 no.4
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    • pp.419-427
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    • 2014
  • In order to examine antioxidative characteristics of Artemisia capillaris response surface methodology was used to optimize the hot water extraction process by analyzing and monitoring the extraction condition. For total phenolic compounds content, the optimal extraction temperature, time and amount of solvent per sample were $94.50^{\circ}C$, 2.06 hr and 25.03 ml/g, respectively. Also, the optimal conditions for electronic donating ability were $91.82^{\circ}C$, 2.90 hr and 20.88 ml/g, respectively. The nitrile scavenging ability (pH 1.2) was optimized using the extraction temperature of $97.36^{\circ}C$, extraction time 2.75 hr and 15.19 ml/g as the amount of solvent per sample. Regression equations of total phenolic compounds content, electron donating ability and nitrile scavenging ability as dependent variable were deduced from each analyzed extraction condition. And finally, their response surfaces were superimposed with the optimal conditions to obtain values for each extraction process factor. The predicted results through superimposing were extraction temperature $90{\sim}95^{\circ}C$, extraction time 2.5~3.5 hr and amount of solvent per sample 17~24 ml/g.

A Review of the Opinion Target Extraction using Sequence Labeling Algorithms based on Features Combinations

  • Aziz, Noor Azeera Abdul;MohdAizainiMaarof, MohdAizainiMaarof;Zainal, Anazida;HazimAlkawaz, Mohammed
    • Journal of Internet Computing and Services
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    • v.17 no.5
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    • pp.111-119
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    • 2016
  • In recent years, the opinion analysis is one of the key research fronts of any domain. Opinion target extraction is an essential process of opinion analysis. Target is usually referred to noun or noun phrase in an entity which is deliberated by the opinion holder. Extraction of opinion target facilitates the opinion analysis more precisely and in addition helps to identify the opinion polarity i.e. users can perceive opinion in detail of a target including all its features. One of the most commonly employed algorithms is a sequence labeling algorithm also called Conditional Random Fields. In present article, recent opinion target extraction approaches are reviewed based on sequence labeling algorithm and it features combinations by analyzing and comparing these approaches. The good selection of features combinations will in some way give a good or better accuracy result. Features combinations are an essential process that can be used to identify and remove unneeded, irrelevant and redundant attributes from data that do not contribute to the accuracy of a predictive model or may in fact decrease the accuracy of the model. Hence, in general this review eventually leads to the contribution for the opinion analysis approach and assist researcher for the opinion target extraction in particular.

Study on the Preparation of Alumina Powders used os a Rubber Filler with a Microwave Extraction System (마이크로파에 의한 고무용 충전제로서의 Alumina Powder의 제조에 관한 연구)

  • Park, Chan-Young;Hwang, Eun-Hee;Han, Seong-Kee
    • Elastomers and Composites
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    • v.33 no.3
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    • pp.201-209
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    • 1998
  • Alumina powders used as a filler in rubber compounding was extracted from kaolin in $H_2SO_4$ solution employing conventional thermal and microwave energy resources. Maximum degrees of alumina extraction from kaolin were 72.8% at $80^{\circ}C$, 1M $H_2SO_4$, and 180min in the conventional thermal extraction process and were 99.0% at $90^{\circ}C$, 1M $H_2SO_4$,, and 60min in the microwave extraction one, respectively. The samples synthesized in both processes were analyzed by means of TG/DTA, XRD, SEM, Atomic Emission Spectroscopy, and BET method. Studies are presently under way to unravel the basic interaction mechanisms between microwave and alumina power for high rates of alumina extraction from kaolin in the microwave ex-traction process.

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Process Balance of Natural Indigo Production based on Traditional Niram Method

  • Shin, Younsook;Yoo, Dong Il;Kim, Kangwha
    • Textile Coloration and Finishing
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    • v.24 no.4
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    • pp.253-259
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    • 2012
  • In this work, the natural indigo production process from Polygonum tinctorium was balanced based on the traditional Niram method in Korea. A standard procedure was determined considering the conditions of indican extraction from plant material, the amount of alkali for precipitation, storage of extract, etc. The effect of experimental conditions on the yield of crude dye was investigated. The contents of indigo and indirubin of the crude dyes were analyzed by HPLC. Increase of the amount of crude dye was observed within 1-2.5 days of extraction time. Longer extraction beyond 2.5 days resulted in a slight decrease in the amount of crude dye. There was no consistency in terms of indigo content depending on extraction pH. We found that the storage of extract or harvested plants affected adversely to dye yield and dye quality. Based on the lab scale extraction, large scale extraction was performed for 2-2.5 days in water and 2.0-2.5 g/L of $Ca(OH)_2$ was applied for precipitation of indigo dye. We obtained natural indigo dye containing about 15% of pure indigo in scale-up production using whole plant except root.

Higher Production of Biolipids from Botryococcus braunii using Pre-treated Solvent Extraction Methods (해양생물 Botryococcus braunii에서 유래한 바이오연료의 고급생산기술: 전처리 용매추출법)

  • Kwon, Sung-Hyun;Cho, Daechul
    • Journal of Environmental Science International
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    • v.28 no.11
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    • pp.927-933
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    • 2019
  • A lipid-enriched strain of Botryococcus braunii (UTEX 572) was cultivated in a semi-batch aeration tank to enhance biomass as well as to develop intracellular lipids and fatty acids. A 30 day period of incubation produced 1.39 g/L of biomass and 0.31 g/L of total lipids in the biomass. The grown biomass was pre-treated using several methods to extract the total lipid content efficiently: ultrasonication was found to yield the highest percentage of lipids-namely 19.8% per biomass. Direct heating of biomass in an autoclave also showed better performance than when using only conventional solvent extraction. To enhance the biomass harvest and lipid extraction efficiency, coagulation and flocculation steps were added to the extraction process. It is noteworthy that not only the solvent type but also the solvent/biomass ratio greatly affected efficiency. In addition, the moisture content of the harvested(wet) biomass affected the efficiency significantly. This study elucidated the need for future research on optimizing this extraction process.

Recovery of Cobalt from the Wastewater produced during Malonate Process by Solvent Extraction (말로네이트 제조 공정 폐수로부터 코발트 회수: 용매추출법 적용)

  • 문영환
    • Journal of Environmental Science International
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    • v.6 no.2
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    • pp.133-139
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    • 1997
  • The solvent extraction method was applied on the wastewater produced during malonate(malonic acid esters) process to recover cobalt. DEHPA and PC88A were used as organic solvent From separation funnel experiment(batch experiment), the effects of vari- ous parameters (pH, cobalt concentration, reaction rate, and stripping temperature) on solvent extraction were examined and these data were used to derive equilibrium curve. A mixer-settler experiment (continuous experiment) of bench scale was also carried out for the plant construction and a Mccabe-Thiele diagram was obtained. The results of these experiments indicate that cobalt is recoverable above 99 oyo and that its purity as cobalt sulfate Is higher than 99.9 wt%.

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Supercritical Fluid Extraction of Physiologically Active materials from Agaricus blazei Fruiting Bodies (Agaricus blazei 자실체로부터 초임계 유체를 이용한 생리활성물질 추출공정)

  • 최정우
    • KSBB Journal
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    • v.15 no.4
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    • pp.408-410
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    • 2000
  • The supercritical fluid extraction(SFE) technique was applied for the isolation and purification of nonpolar physiologically acitve mateials from Agaricus blazei fruiting bodies. the qualitative analysis of extract was accomplished by gas chromatography-mass spectrometer(GC-MS) and extract was determined as linoleic acid(cis-9 cis-12-octadecadienoic acid) In order to obtain the optimum operating conditions of supercritical fluid extraction process the various temperatures and pressures were applied for process operation. From the comparison of exraction efficiencies $50^{\circ}C and 200 kg_f/cm^2$ were determined as optimum conditions.

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Digital image processing techniques of digital holographic PTV measurement (디지털 holographic PTV 측정을 위한 디지털 영상처리기법에 관한 연구)

  • Kim, Seok;Lee, Sang-Joon
    • 한국가시화정보학회:학술대회논문집
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    • 2005.12a
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    • pp.1-5
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    • 2005
  • The digital HPTV velocity field measurement consists of four steps: recording, numerical reconstruction, particle extraction and velocity extraction. In the velocity extraction process, we improved PTV algorithm to extract the displacement of particle each placed in 3D space. Because a digital recording device was used, some factors such as a spatial resolution, numerical aperture, and particle concentration can affect the performance of the digital HPTV. Especially, a particle concentration ($C_{o}$) affected tile reconstruction efficiency in numerical reconstruction and particle extraction process. In this paper, the reconstruction efficiency was analyzed experimentally with different particle concentration. Optimal reconstruction efficiency was shown in the range of $C_{o}$=$13\∼15$ particles/$mm^{3}$.

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