• 한국수자원학회논문집
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• 제31권4호
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• pp.429-437
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• 1998

기존의 DWOPER 모형에 대해서도 불확실도 기법을 이용한 홍수범람 해석을 위해 DWOPER-LEV 모형을 개발하였고, 하천의 홍수범람에 따른 제방의 월류위험도와 가능 범람범위를 예측할 수 있도록 하엿다. 본 연구에서는 홍수추적에 있어서의 하도단면의 기하형상과 수리저항계수에 기인한 불확실도의 영향을 검토하기 위해 Monte-Carlo 기법을 적용하였다. 개발된 모형은 남한강 유역의 실제 제방붕괴로 인한 홍수범람에 적용하여 제방의 월류위험도와 제내지에서의 가능 범람범위와 범람수심을 산정하였다.

• 한국광학회지
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• 제21권2호
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• pp.46-52
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• 2010

본 논문에서는 양방향 반사율 분포함수의 이론과 제작된 측정시스템 및 측정불확도의 평가방법을 소개한다. (380~1500) nm의 분광 양방향 반사율 분포함수를 $(-75{\sim}75)^{\circ}$의 각도 범위에서 측정할 수 있는 측정시스템을 제작하였고, 상관관계가 있는 불확도 성분과 상관관계가 없는 불확도 성분으로 나누어 측정불확도를 평가하였다. 평가 결과, 제작된 양방향 반사율 분포함수 측정시스템의 상대확장불확도는 3% (k=2) 이하로 평가되었다.

• Nuclear Engineering and Technology
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• 제48권2호
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• pp.299-303
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• 2016

Prompt gamma activation analysis using a thermal neutron-guided beam at Japan Atomic Energy Agency JRR-3M was applied for the precise determination of Si in silicon nitride ceramic reference materials [Japan Ceramic Reference Material (JCRM) R 003]. In this study, the standard addition method coupled with internal standard was used for the nondestructive determination of Si in the sample. Cadmium was used as internal standard to obtain the linear calibration curves and to compensate for the neutron beam variability. The analytical result of determining Si in JCRM R 003 silicon nitride fine powder ceramic reference materials using prompt gamma activation analysis was in good agreement with that obtained by classical gravimetric analysis. The relative expanded measurement uncertainty (k = 2) associated with the determined value was 2.4%.

• Nuclear Engineering and Technology
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• 제49권6호
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• pp.1226-1233
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• 2017

Measurements of the isotopic contents of spent nuclear fuel provide experimental data that are a prerequisite for validating computer codes and nuclear data for many spent fuel applications. Under the auspices of the Organisation for Economic Co-operation and Development (OECD) Nuclear Energy Agency (NEA) and guidance of the Expert Group on Assay Data of Spent Nuclear Fuel of the NEA Working Party on Nuclear Criticality Safety, a new database of expanded spent fuel isotopic compositions has been compiled. The database, Spent Fuel Compositions (SFCOMPO) 2.0, includes measured data for more than 750 fuel samples acquired from 44 different reactors and representing eight different reactor technologies. Measurements for more than 90 isotopes are included. This new database provides data essential for establishing the reliability of code systems for inventory predictions, but it also has broader potential application to nuclear data evaluation. The database, together with adjoint based sensitivity and uncertainty tools for transmutation systems developed to quantify the importance of nuclear data on nuclide concentrations, are described.

• 한국전자파학회논문지
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• 제17권4호
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• pp.387-392
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• 2006

K-대역에서 동작하는 3.5 mm 동축형 감쇠량 표준기를 개발하고 그 측정 불확도를 평가하였다. 전력비 전달방식의 4개의 모듈로 구성된 이 표준기는 18 GHz부터 26.5 GHz까지의 광대역에서 동작하며 각 모듈은 약 20 dB의 감쇠량을 가진다. 측정 가능한 최대 감쇠량은 80 dB이고 이때의 확장 불확도는 약 95% 신뢰수준에서 0.01 dB이다.

• 대한기계학회논문집B
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• 제32권9호
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• pp.712-719
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• 2008

Light Oil Flow Standard System(LOFSS), as a national oil flow standard system, in Korea Research Institute of Standards and Science(KRISS) was developed for oil flowmeter calibration, and the expanded uncertainty of flow quantity determination was estimated within 0.04 %. In order to improve the reliability of the LOFSS measurement, a proficiency test was carried out in the flow range of 20 and $240\;m^3/h$ (Reynolds number $20,000{\sim}900,000$). A turbine flowmeter was used as a transfer package in round robin test. The water flow standard system of KRISS, the pipe prover of the national calibration and test organization and the master meter calibrator of the turbine flowmeter supplier, which used the different working fluid respectively, were compared with the turbine flowmeter measurement. The maximum difference of measurement was 0.15 % between the LOFSS and the pipe prover. The En numbers of the each system measurement were evaluated at the same Reynolds number. It was found that the En numbers were less than 1 in the comparison, which means the procedures of the uncertainty estimation of the each calibrators were reasonable and reliable.

• 한국축산식품학회지
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• 제43권6호
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• pp.949-960
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• 2023

This research aimed to validate a high-performance liquid chromatography method for the quantitative determination of bixin and norbixin in various foods. The Diode Array Detector (495 nm) technique was used. Method was validated for specificity, linearity, limit of detection (LOD), limit of quantification (LOQ), precision, and accuracy, and the measurement uncertainty was assessed. The calibration curve showed excellent linearity (r²≥0.9999) over the tested concentration range of 0.2-25 mg/L. The LOD and LOQ were 0.03-0.11 and 0.02-0.05 mg/L for bixin and norbixin, respectively. The intra-and inter-day accuracies and precisions were 88.0±1.3-97.0±0.5% and 0.2%-2.6% relative SD (RSD) for bixin and 88.2±0.8-105.8±0.8% and 0.3%-2.7% RSD for norbixin, respectively. Inter-laboratory validation for accuracy and precision was conducted in three laboratories, and these results all met the AOAC guidelines. In addition, the relative expanded uncertainty (<22%) satisfied the CODEX recommendation. Furthermore, products distributed in Korea were monitored for annatto extracts using the proposed method to demonstrate its application. The developed analytical method is reliable for quantifying bixin and norbixin in various foods.

• 한국정밀공학회지
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• 제23권6호
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• pp.96-103
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• 2006

To establish of standard technique of nano-length measurement in 2D plane, new AFM system has been designed. In the long range (about several tens of ${\mu}m$), measurement uncertainty is dominantly affected by the Abbe error of XY scanning stage. No linear stage is perfectly straight; in other words, every scanning stage is subject to tilting, pitch and yaw motion. In this paper, an AFM system with minimum offset of XY sensing is designed. And XY scanning stage is designed to minimize rotation angle because Abbe errors occur through the multiply of offset and rotation angle. To minimize the rotation angle optimal design has performed by maximizing the stiffness ratio of motion direction to the parasitic motion direction of each stage. This paper describes the design scheme of full AFM system, especially about XY stage. Full range of fabricated XY scanner is $100{\mu}m\times100{\mu}m$. And tilting, pitch and yaw motion are measured by autocollimator to evaluate the performance of XY stage. As a result, XY scanner can have good performance. Using this AFM system, 3um pitch specimen was measured. The uncertainty of total system has been evaluated. X and Y direction performance is different. X-direction measuring performance is better. So to evaluate only ID pitch length, X-direction scanning is preferable. Its expanded uncertainty(k=2) is $\sqrt{(3.96)^2+(4.10\times10^{-5}{\times}p)^2}$ measured length in nm.

• 한국식품과학회지
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• 제49권6호
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• pp.591-598
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• 2017

This study aimed to evaluate the measurement uncertainty for the quantitative determination of chlorite and chlorate in ready-to-eat fresh-cut vegetables using ion chromatography with a hydroxide-selective column. One gram of the homogenized sample in deionized water was sonicated and centrifuged at 8,500 rpm. The supernatant was purified by passing it through a Sep-Pak tC18 cartridge, followed by chromatographic determination using a Dionex IonPac AS27 column. The linearity of the calibration curves, recovery, repeatability, and reproducibility of the method were satisfactory. The method detection limit was estimated to be approximately 0.5 mg/kg. Each uncertainty component was evaluated separately, and the combined and expanded uncertainty values were calculated at the 95% confidence level. The measured concentrations for 3 mg/kg of chlorite and chlorate standard materials were $3.18{\pm}0.32$ and $3.10{\pm}0.42mg/kg$, respectively. These results confirmed the reliability of the developed method for measuring the two chlorine-based oxyanions in fresh-cut vegetables.

• 한국정밀공학회지
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• 제21권11호
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• pp.75-82
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• 2004

A metrological atomic force microscope (M-AFM) was developed fur the length measurements of nanometer range, through the modification of a commercial AFM. To eliminate nonlinearity and crosstalk of the PZT tube scanner of the commercial AFM, a two-axis flexure hinge scanner employing built-in capacitive sensors is used for X-Y motion instead of PZT tube scanner. Then two-dimensional displacement of the scanner is measured using two-axis heterodyne laser interferometer to ensure the meter-traceability. Through the measurements of several specimens, we could verify the elimination of nonlinearity and crosstalk. The uncertainty of length measurements was estimated according to the Guide to the Expression of Uncertainty in Measurement. Among several sources of uncertainty, the primary one is the drift of laser interferometer output, which occurs mainly from the variation of refractive index of air and the thermal stability. The Abbe error, which is proportional to the measured length, is another primary uncertainty source coming from the parasitic motion of the scanner. The expanded uncertainty (k =2) of length measurements using the M-AFM is √(4.26)$^2$+(2.84${\times}$10$^{-4}$ ${\times}$L)$^2$(nm), where f is the measured length in nm. We also measured the pitch of one-dimensional grating and compared the results with those obtained by optical diffractometry. The relative difference between these results is less than 0.01 %.