• Transactions of Materials Processing
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• v.25 no.5
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• pp.306-312
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• 2016

Effects of manufacturing conditions, such as austenitizing temperature, patenting temperature and carbon content in steels, on mechanical properties, especially on reduction of area (RA), of hyper-eutectoid steel wires were investigated. RA increased and then decreased with transformation temperature. This was attributed to the presence of abnormal structures in steels transformed at low transformation temperatures and the occurrence of shear cracking during tensile testing of steels transformed at high transformation temperatures. The increase of austenitizing temperature resulted in the increased austenite grain size and consequently the decrease of RA. The decrease of RA with increasing the carbon content in steels was attributed to the increased fraction of cleavage fracture in tensile fractured surfaces.

• Transactions of Materials Processing
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• v.13 no.4
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• pp.350-358
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• 2004

The effects of alloying elements on microstructural features and mechanical properties in 0.55%C medium carbon steels were investigated. The samples were austenitized at 105$0^{\circ}C$ for 30min. followed by quenching in a salt bath in the temperature range of 500 ~ $620^{\circ}C$. The addition of Cr resulted in the decrease of the volume fraction of pro-eutectoid ferrite and interlamellar spacing in pearlite and the increase of strength. However, the addition of B caused the increase of the volume fraction of pro-eutectoid ferrite. Reduction of area and Charpy impact values were influenced by the combined effect of microstructural features, such as the volume fraction of pro-eutectoid ferrite, interlamellar spacing and the thickness of lamellar cementite in pearlite.

• Journal of the Korean Society for Heat Treatment
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• v.1 no.1
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• pp.1-7
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• 1988

In this study the improvement of mechanical properties of ion-nitrided SACM-1 steel was investigated by analysing microstructural developments and hardness increase in the nitrided surface layer. Specimens were quenched at $570^{\circ}C$, which is lower than the eutectoid temperature ($590^{\circ}C$) of Fe-N binary system after nitrided at temperature of $460-570^{\circ}C$ for 2-8 hours under constant pressure of 8 torr. The depths of diffusion and compound layers were appeared to proportional to the root mean square time of nitriding. And the hardness showed the maximun value Hv = 1200 for the specimen nitrided at $530^{\circ}C$. Hardness distribution of the. ion-nitrided steels were increased by diffusion treatment below the eutectoid temperature of the Fe-N binary system. A prolonged heat treatment below the eutectoid temperature was attributed to the increase in the depth of diffusion layer at the expense of the decrease in surface hardness of the ion nitreded steel.

• Journal of the Korean Society for Heat Treatment
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• v.26 no.3
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• pp.126-131
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• 2013

In this study, effects of silicon addition on the spheroidizing annealing of hyper-eutectoid steel was investigated. Heat treatment at various temperatures in the ${\gamma}+{\theta}$ region was also conducted in order to systematically control the kinetics of undissolved cementite. It was found that small amount of Si addition could increase both $A_1$ and $A_{cm}$ transformation temperature by both the JMat Pro evaluation and dilatometric measurement. It was also revealed by the microstructural observation that the volume fraction of retained cementite during heat treatment increased with decreasing temperature as well as increasing Si content. Based on the results obtained, it could be suggested that spheroidization at relatively higher temperature above $950^{\circ}C$ could be achieved by small addition of Si.

• Journal of the Korean Society for Heat Treatment
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• v.30 no.1
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• pp.6-12
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• 2017

In this study tensile and impact properties of three hypo-eutectoid steels containing different micro-alloying elements were investigated in terms of microstructural factors such as pro-eutectoid ferrite grain size, pearlite fraction, interlamellar spacing, and cementite thickness. Yield point phenomenon appeared in all the steel specimens during tensile testing, and ultimate tensile stress was mainly dependent on pearlite fraction. On the other hand, the refinement of austenite grain size caused by the addition of micro-alloying elements resulted in the increment of ferrite volume fraction and carbon contents in pearlite because of the refinement of pro-eutectoid ferrite grain size. As a result, cementite thickness in pearlite increased and had an effect on deteriorating the low temperature impact toughness.

• Journal of the Korean Society for Heat Treatment
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• v.27 no.2
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• pp.72-78
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• 2014

Isothermal transformation behavior of a 10% Cr heat resistant steel fabricated by centrifugal casting process was investigated. Normalized specimen at $1100^{\circ}C$ for 1 hour was isothermally annealed at temperature range between $600^{\circ}C$ and $700^{\circ}C$ with various time. The annealed specimen had eutectoid structure which was generated along austenitic grain boundary during isothermal annealing. Areal fraction of eutectoid structure increased up to 25% after holding at $700^{\circ}C$ for 20 hours. It was observed that austenitic matrix was transformed to ferrite structure and fine $M_{23}C_6$ carbides with increase of annealing time. Time-temperature-transformation diagram of the centrifugally cast 10% Cr steel with 0.18 wt% C was plotted based on the results of isothermal transformation behavior.

• Journal of Technologic Dentistry
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• v.31 no.3
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• pp.9-14
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• 2009

This study evaluated the mechanical properties of Ti-Cu alloys with the hope of developing an alloy for dental casting with better mechanical properties than unalloyed titanium. Ti-Cu alloys with four concentrations of Cu(2,5,10wt%) were made in an argon-arc melting furnace. The microstructure and micro-Vickers hardness were determined. X-ray diffraction pattern test was performed on the polished specimens. The microstructure of 2%Cu and 5%Cu alloys are shown acicular ${\alpha}Ti$ phase formed on the surfaces of previously formed $\beta$grains. The 10%Cu alloys has essentially a eutectoid structure; this structure includes lamella of ${\alpha}Ti$ and $Ti_2Cu$ phase that transformed from ${\alpha}Ti$ at the eutectoid temperature. The micro-Vickers hardness of CP Ti specimens was significantly(p<0.05) lower than that of any of the other alloys. Among the Ti-Cu alloys, the 10%Cu alloys exhibited a significantly(p<0.05) higher hardness value. but lower than that of Ti-6%Al-4%V alloy. From these results, it was concluded that new alloys for dental castings should be designed as Ti-Cu based alloys if other properties necessary for dental castings were obtained.

• Transactions of Materials Processing
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• v.13 no.5
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• pp.415-421
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• 2004

The effect of transformation temperature on microstructural features and their effects on ductility in 0.55%C steels were investigated, compared with in 0.82%C eutectoid steel. The samples were austenitized at 100$0^{\circ}C$ for 30min. followed by quenching in a salt bath in the temperature range of 500 ~ $620^{\circ}C$. It was found that reduction of area(RA) increased with increasing transformation temperature and then, decreased after reaching its maximum value in steels containing pro-eutectoid ferrite less than 6%. The thickness of lamellar cementite was found to be the main factor controlling RA. Additionally, the presence of cementite thickness for the maximum ductility in all the tested steels was observed as about 0.015${\mu}{\textrm}{m}$ for tested steels.

• Journal of Welding and Joining
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• v.23 no.6
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• pp.93-98
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• 2005

The purpose of this study is to investigate the characteristics of pb-free $Zn-(3\~6)\%Al-(1\~6)\%Cu$ solder alloys for ultra high temperature(>573K) which applied to air craft, space satellite, automotive, oil, gas well exploration and data logging of geo-thermal wells. Melting range, solderability, electric resistivity, microstructure and mechanical properties were examined with solder alloys casted in Ar gas atmosphere. $Zn-4\%Al-(1\~3)\%Cu,\;Zn-5\%Al-(2\~4)\%Cu\;and\;Zn-6\%Al-(3\~5)\%Cu$ alloys satisfied the optimum melting range of 643 to 673k for ultra high temperature solder. A melting temperature increased with increasing Cu content, but decreased with increasing Al content. The spreadability was improved with increasing hi content. But the content of Cu had no effect on the spreadability. The electric resistivity was lowered with increasing Al and decreasing Cu content. In all Zn-Al-Cu solder alloys, primary dendritic $\varepsilon$ phase(Zn-Cu), dendritic $\eta$ phase(Zn-Cu-Al), $\alpha(Al-Zn)-\eta$ eutectic and eutectoid phase were observed. The addition of Al increased the volume fraction of eutectic and eutectoid phase and it decreased f phases. Also, the addition of Cu increased slightly the volume fraction of e, the eutectic and eutectoid phases. With increasing total content of Al and Cu, a hardness and a tensile strength were linearly increased, but anelongation was linearly decreased.

• Journal of Technologic Dentistry
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• v.27 no.1
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• pp.65-71
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• 2005

Experimental Ti-13%Zr and Ti-13%Zr-5%Cu alloys were made in an argon-arc melting furnace. The grade 2 CP Ti was used to control. The alloys were cast into phosphate bonded $SiO_2$ investment molds using an argon-arc casting machine, and The hardness and microstructures of the castings were investigated in order to reveal their possible use for new dental casting materials and to collect useful data for alloy design. The hardness of the Ti-13%Zr-5%Cu alloy(379Hv) became higher than that of Ti-13%Zr(317Hv) alloy, and the hardness of this alloys became higher than that of CP Ti(247Hv). Increasing in the hardness of the Ti-13%Zr-5%Cu alloy was considered to be solid solution hardening as the Ti-Zr system shows a completely solid solution for both high temperature $\beta$phase and low temperature $\alpha$ phase and also the inclusion of the eutectoid structure($\alpha Ti+Ti_{2}Cu$). No martensitic structures are observed in the specimen made of CP Ti, but Ti-13%Zr and Ti-13%Zr-5%Cu alloys show a kind of martensitic structure. Ti-13%Zr-5%Cu shows the finest microstructure. From these results, it was concluded that new alloys for dental casting materials should be designed as Ti-Zr-Cu based alloys.