• Title/Summary/Keyword: Emulsion Stability

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Effect of Glutamic Acid and Monosodium Glutamate on Oxidative Stability of Riboflavin Photosensitized Oil-in-Water Emulsion

  • Ji-Yun Bae;Mi-Ja Kim
    • The Korean Journal of Food And Nutrition
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    • v.37 no.1
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    • pp.48-56
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    • 2024
  • Effects of glutamic acid (Glu) and monosodium glutamate (MSG) on oxidative stability of oil-in-water (O/W) emulsions with different emulsifier charges during riboflavin (RF) photosensitization were evaluated by analyzing headspace oxygen content and conjugated dienes. Cetyltrimethylammonium bromide (CTAB), Tween 20, and sodium dodecyl sulfate (SDS) were used as cationic, neutral, and anionic emulsifiers, respectively. Glu acted as an antioxidant in CTAB- and Tween-20-stabilized O/W emulsions during RF sensitization, whereas Glu acted as prooxidants in SDS-stabilized O/W emulsions in the dark. However, adding MSG did not have a constant impact on the degree of oxidation in O/W emulsions irrespective of the emulsifier charge. In RF-photosensitized O/W emulsions, the emulsifier charge had a greater influence on antioxidant properties of Glu than on those of MSG.

Performance Evaluation of 100% RAP Asphalt Mixtures using Rapid-Setting Polymer-Modified Asphalt Emulsion for Spray Injection Application (스프레이 패칭 긴급보수용 개질 유화 아스팔트와 100% 순환골재를 사용한 상온 아스팔트 혼합물의 성능 평가)

  • Lim, Jeong-un;Kwon, Bong Ju;Kim, Doo Youl;Lee, Sang Yum;Rhee, Suk Keun
    • International Journal of Highway Engineering
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    • v.18 no.2
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    • pp.61-71
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    • 2016
  • PURPOSES: The objective of this study was to determine the optimum ratio of mix design, for a reclaimed asphalt pavement (RAP) content of 100%, for spray injection application. METHODS: A literature review revealed that spray injection is an efficient and cost-effective application for fixing small defective regions of an asphalt pavement. Rapid-setting polymer-modified asphalt mixtures prepared from two types of rapid-setting polymer asphalt emulsion were subjected to Marshall stability and wet track abrasion tests, in order to identify the optimum mix designs. RESULTS and CONCLUSIONS : Different mix designs of type A and type B emulsions were prepared using RAP and virgin aggregates, in order to compare the performance and determine the optimum mix design. The performance of mixtures prepared with RAP was superior to that of mixtures containing virgin aggregates. Moreover, for optimum ratio of the design, the binder content prepared from RAP was set to 1~2% lower than that consisting of virgin aggregates. Compared to their Type A counterparts, type B mixtures consisting of a reactive emulsion performed better in the Marshall stability and wet track abrasion tests. The initial results confirmed the advantages associated with using RAP for spray injection applications. Further studies will be performed to verify the difference in the optimum mix design and performance obtained in the lab-scale test and tests conducted at the job site by using the spray injection machine.

Combined Effect of Kimchi Powder and Onion Peel Extract on Quality Characteristics of Emulsion Sausages Prepared with Irradiated Pork

  • Lee, Soo-Yoen;Kim, Hyun-Wook;Hwang, Ko-Eun;Song, Dong-Heon;Choi, Min-Sung;Ham, Youn-Kyung;Choi, Yun-Sang;Lee, Ju-Woon;Lee, Si-Kyung;Kim, Cheon-Jei
    • Food Science of Animal Resources
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    • v.35 no.3
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    • pp.277-285
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    • 2015
  • This study was conducted to investigate the effects of kimchi powder and onion peel extract on the quality characteristics of emulsion sausage manufactured with irradiated pork. The emulsion sausages were formulated with 2% kimchi powder and/or 0.05% onion peel extract. The changes in pH value of all treatments were similar, depending on storage periods. The addition of kimchi powder increased the redness and yellowness of the emulsion sausage. The addition of onion peel extract decreased the thiobarbituric acid reactive substances value of the emulsion sausages prepared with irradiated pork. The volatile basic nitrogen value of the emulsion sausage prepared with kimchi powder was the highest, whereas that of the emulsion sausage prepared with onion peel extract was the lowest. The treatment without kimchi powder or onion peel extract and the treatments prepared with onion peel extract showed lower microbial populations than the other treatment. Sensory evaluations indicated that a higher acceptability was attained when kimchi powder was added to the emulsion sausages manufactured with irradiated pork. In conclusion, our results suggest that combined use of kimchi powder and onion peel extract could improve quality characteristics and shelf stability of the emulsion sausage formulated with irradiated pork during chilled storage.

A Study on Nano-emulsion for Enhanced Transdermal Delivery of Hippophae rhamnoides Leaf Extract (비타민나무 잎 추출물의 피부 흡수 증진을 위한 나노에멀젼 연구)

  • Chae, Kyo Young;Kwon, Soon Sik;Park, Soo Nam
    • Applied Chemistry for Engineering
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    • v.24 no.3
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    • pp.260-265
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    • 2013
  • In this study, nano-emulsions containing 0.01, 0.03, 0.05, and 0.10% ethyl acetate fraction of Hippophae rhamnoides (H. rhamnoides) leaf extracts were prepared. The particle size, particle size distribution and skin permeability of the nano-emulsions were evaluated for five weeks. Nano-emulsion was prepared by the sequential use of homogenizer and microfluidizer. Nano-emulsion containing the ethyl acetate fraction exhibited a monodispersed form. Nano-emulsion containing 0.03% ethyl acetate fraction was the most stable for five weeks. The in vitro skin permeation study of nano-emulsion containing 0.03% ethyl acetate fraction was carried out using Franz diffusion cell. The nano-emulsion showed a better skin permeability than that of O/W emulsion. These results indicate that the nano-emulsion containing the ethyl acetate fraction of H. rhamnoides leaf extract showed a remarkable stability and skin permeability than that of O/W emulsion.

Stability of Henna Natural Hair Dye Cream Formulation According to Cetyl Alcohol Contents (Cetyl alcohol 함량에 따른 크림 제형 Henna 천연 염모제의 안정성)

  • Kang, Eyoung;Lee, Seunghee;Kim, Woonjung;Jung, Jongjin
    • Journal of the Korean Applied Science and Technology
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    • v.38 no.4
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    • pp.1176-1182
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    • 2021
  • In this study, the emulsion stability of henna, a natural hair dye, according to the content of cetyl alcohol, one of the emulsification stabilizers, was analyzed, and the content of cetyl alcohol showing the most stable emulsification was confirmed. To analyze the emulsion stability, differences in particle size, particle shape, viscosity, and color after dyeing were compared according to the content of cetyl alcohol. As a result of dynamic light scattering (DLS) zeta analysis, cetyl alcohol 3% showed the highest zeta potential value of 115.9 mV, and the particle size distribution was henna in which a cream-type hair dye containing 3% cetyl alcohol was dispersed in distilled water. The width of the particle size distribution was narrow compared to. As a result of viscometer analysis, the viscosity increased as the content of cetyl alcohol increased. As a result of measuring the henna pH of the cream formulation, it was measured in a pH range suitable for the scalp. As a result, emulsion stability increases as the content of cetyl alcohol increases in henna cream formulations for hair dye.

Effects of duck fat and κ-carrageenan as replacements for beef fat and pork backfat in frankfurters

  • Shin, Dong-Min;Yune, Jong Hyeok;Kim, Yea Ji;Keum, Sang Hoon;Jung, Hyun Su;Kwon, Hyuk Cheol;Kim, Do Hyun;Sohn, Hyejin;Jeong, Chang Hee;Lee, Hong Gu;Han, Sung Gu
    • Animal Bioscience
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    • v.35 no.6
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    • pp.927-937
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    • 2022
  • Objective: Frankfurters are emulsion-type sausages that are widely consumed worldwide. However, some concerns regarding negative health effects have been raised because of the high fat content and the type of fat. This study aimed to evaluate the effects of duck fat and κ-carrageenan as replacements for beef fat and pork backfat in frankfurters. Methods: The different formulations for the frankfurters were as follows: 20% beef fat (BF), 20% pork backfat (PBF), 20% duck fat (DF), 20% soybean oil (SO), 20% duck fat/1% κ-carrageenan (DFC), and 20% soybean oil/1% κ-carrageenan (SOC). Physicochemical (fatty acid profile, color, rheological properties, cooking loss, water holding capacity, emulsion stability, and texture profile analysis), oxidative stability and sensory properties of frankfurters were evaluated. Results: Duck fat and κ-carrageenan improved rheological properties of meat batter, and physicochemical properties (emulsion stability, cooking loss, and hardness) of frankfurters. Moreover, duck fat added-frankfurters (DF and DFC) had higher oxidative stability than that of soybean-added frankfurters (SO and SOC) during refrigerated storage for 28 days. In sensory evaluation, flavor, texture, and overall acceptability of DFC were acceptable to untrained panelists. Conclusion: Our data suggest that duck fat and κ-carrageenan can replace beef fat and pork backfat in frankfurters. Duck fat and κ-carrageenan contributed to improve the physicochemical properties and oxidative stability while maintaining sensory properties. Therefore, the use of duck fat and κ-carrageenan may be a suitable alternative for replacing beef fat or pork backfat in frankfurters.

Preparation and Properties of W/O Emulsion by D Phase Emulsification (D상 유화물을 이용한 W/O 유화물의 제조와 특성)

  • Kim, H.J.;Jeong, N.H.;Yun, Y.K.;Park, K.S.;Nam, K.D.
    • Journal of the Korean Applied Science and Technology
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    • v.15 no.2
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    • pp.25-32
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    • 1998
  • The emulsion stability of W/O emulsion prepared by D phase emulsification during storage and handling is studied by using phase diagrams. The process of D phase emulsification begins with the formation of isotropic surfactant solution, followed by formation of oil-in-surfactant (O/D) gel emulsion by dispersion of octamethylcyclotetrasiloxane(OMCS) in the surfactant solution. Polyols were essential components for this purpose. To understand the function of polyols, the solution behavior of nonionic surfactant/oil/water/polyol systems were investigated by the ternary phase diagrams of polyoxyethylene oleyl ether/OMCS/propylene glycol(PG) aqueous solutions. The addition of PG increased the solubility of oil in the isotropic surfactant phase. D phase emulsification method has been applied to a new type of cosmetics. By using this emulsification technique, O/W emulsion were formed without a need for adjust of HLB. Fine and stable W/O emulsions were prepared by D phase emulsion.

Utilization of Dried Garlic Powder and α-Tocopherol to Improve the Shelf-life of Emulsion-type Sausage during Refrigerated Storage

  • Kim, Young-Jik;Choi, In-Hag
    • Food Science of Animal Resources
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    • v.32 no.6
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    • pp.725-731
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    • 2012
  • This study investigated the shelf life of emulsion-type sausages containing garlic powder and/or ${\alpha}$-tocopherol during storage at $4^{\circ}C$ for 0, 10, 20, and 30 d. Six groups of emulsion-type sausages were included: control (no additives), GP1 (1% garlic powder), GP3 (3% garlic powder), AT100 (100 IU of ${\alpha}$-tocopherol/kg of sausage), AT200 (200 IU of ${\alpha}$-tocopherol/kg of sausage), and GP1+AT100 (1% garlic powder+100 IU of ${\alpha}$-tocopherol/kg of sausage). During storage, the pH, thiobarbituric acid reactive substances, and residual nitrite content were reduced by the addition of garlic powder and/or ${\alpha}$-tocopherol relative to the control (p<0.05). In addition, emulsion-type sausages supplemented with garlic powder and/or ${\alpha}$-tocopherol improved color stability (p<0.05). The results suggest that a higher amount of garlic powder and their different combinations could improve the shelf life of emulsion-type sausages and protect against lipid oxidation.

Batch and dynamic study of lactic acid extraction using emulsion liquid membrane

  • Berrama, Tarek;Pareau, Dominique;Durand, Gerard
    • Membrane and Water Treatment
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    • v.6 no.4
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    • pp.277-292
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    • 2015
  • The extraction of lactic acid by an emulsion liquid membrane (ELM), in batch and continuous mode, has been reported. On the basis of preliminary experiments, the optimum composition of the organic phase (membrane) is determined. When the SPan 80 is used as surfactant, the emulsion breakage exceeds 50%, but only 10% is obtained when the ECA4360 is used. The effects of surfactant, carrier and solute concentrations, phase volume ratio, and stirring speed on the extraction yield were examined and optimized. Surfactant, carrier and diluent used were ECA4360, trilaurylamine (TLA) and dodecane, respectively; 2-ethylhexane-1,3-diol (EHD) is used as a co-surfactant. Under optimal conditions, emulsion breaking is very low and the swelling is kept at its lowest level. Under the pH conditions of fermentation medium, the extraction yield is lower. A mixer-settler continuous system was used for testing these conditions. The residence time, the number of extraction stages and the stability of the emulsion were studied and optimized. The extraction yield obtained exceeds 90%.

Preparation and Properties of Poly($\varepsilon$-caprolactone) Nanocapsules Containing Phytoncide Oil by Emulsion-diffusion Method(1) (유화확산법을 이용한 피톤치드오일 함유 폴리입실론카프로락톤 나노캡슐의 제조와 성질(1))

  • Jeong, Cheon-Hee;Kim, Hea-In;Park, Soo-Min
    • Proceedings of the Korean Society of Dyers and Finishers Conference
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    • 2008.04a
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    • pp.114-116
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    • 2008
  • Poly(${\varepsilon}$-caprolactone) nanocapsules(nanoPCL) containing phytoncide oil were synthesized by emulsion diffusion method using ethyl acetate as organic solvent. The influence of the degree of hydrolyzation of poly(vinyl acohol) used as an emulsion stabilizer, and the different weight ratio of core material to wall material on the particle size, morphology, and emulsion stability was investigated to design nanocapsules. The encapsulated nanoPCL were characterized by FT-IR spetrometry, Scanning electron microscope, Differential scanning calorimetry, and Thermogravimetry analysis, respectively.

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