• Title/Summary/Keyword: Ductile-to-brittle transition temperature

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Degradation Degree Evaluation of Heat Resisting Steel by Electrochemical Technique Part 2 : Effect of Testing Conditions on Evaluation Value of Degradation Degree and Changes of Mechaical Properties (전기화학적 방법에 의한 내열강의 열화도측정 제2보 : 열화도측정치에 미치는 측정조건들의 영향과 기계적성질 변화에 대해서)

  • 정희돈;권영각;장래웅
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.2
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    • pp.300-312
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    • 1993
  • The material deterioration of service-exposed boiler tube steels in fossil power plant was evaluated by using the electrochemical technique namely, modified electrochemical potentiokinetic reactivation(EPR). It was focused that the passivation of Mo$_{6}$C carbide which governs the mechanical properties of Mo alloyed steels did not occur even in the passivity region of steel in sodium molybdate solution and the reactivation peak current (Ip) observed as the result of non-passivation indicating the precipitation of Mo$_{6}$C carbides. To obtain the optimal test conditions for the field test by using the specially designed electrochemical cell, the effects of scan rate, the surface roughness and the pH of electrolyte on Ip value were also investigated. Furthermore, the change of mechanical properties occurred during the long time exposure at high temperature was evlauated quantitatively by small punch(SP) tests and micro hardness test taking account of the metallurgical changes. It is known that reactivation peak current (Ip) has a good relationship with Larson-Miller Parameter(LMP) which represents the information about material deterioration occurred at high temperature environment. In addition it was possible to estimate the ductile-brittle transition temperature (DBTT) by means of the SP test. The Sp test could be, therefore, suggested as a reliable test method for evaluating the material degradation of boiler tube steels. From the good correaltion between the SP DBTT and Ip values shown in this study, it was knows that the change of mechanical properties could be evaluated non-destructively by measurring only Ip values.ues.

Flexural Properties and Thermal Stability of Bifunctional/Tetrafunctional Epoxy Blends (2 -관능성 에폭시 수지 블렌드의 굴곡 특성과 열 안전성)

  • Yu, Hui-Yeol;Lee, Jae-Rak;Lee, Jong-Mun
    • Korean Journal of Materials Research
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    • v.4 no.1
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    • pp.75-80
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    • 1994
  • Flexural properties and thermal stability have been studied as a function of blend composition in bifunctional DGERA (diglycidyl ether of hisphenol A)/tetrafunctional TGDDM(tetrag1ycidyl diamino diphenyl methane) cured with DDM(4, 4'-diamino diphenyl methane). The flexural modulus and the glass transition temperature increase with an increase of TGDDM and show discontinuous dependence on blend composition around the composition range of 80/20~60/40(L)GEBA/TGDDM). This can be explained with a structural phase inversion (ductile-to-brittle) in crosslinking networks. With increasing TGDDM, the maximum decomposition temperature(Ts) increases, whereas the activation energy during thermal degradation decreases.

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Effects of microstructure on impact transition temperature of low carbon HSLA steels (저탄소 HSLA강의 천이 온도 미치는 미세 조직의 영향)

  • Kang, J.S.;Lee, C.W.;Park, C.G.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.05a
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    • pp.431-434
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    • 2008
  • Effects of microstructure on the toughness of low carbon HSLA steels were investigated. Nickel decreased the ferrite-austenite transformation temperature, resulted in increase of the fraction of bainitic ferrite. However, it was decreased with increasing deformation amount at austenite region. Since fine austenite grains formed by dynamic recrystallization under large strain transformed to acicular ferrite or granular bainite rather than bainitic ferrite. The effective grain size, thus, was decreased by deformation and it resulted in lower ductile-brittle transition temperature (DBTT). The bainitic ferrite was thought to inhibit the fracture crack initiation and to delay the crack propagation by its high dislocation density and hard interlath $2^{nd}$ phase constituents, respectively. Thus, DBTT was also decreased by Ni addition in low carbon HSLA steels.

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A Study the Behavior of Plastic Deformation in Weld HAZ of Mild Steel (軟鋼 熔接熱影響部의 塑性變形擧動에 關한 硏究 II)

  • 박창언;정세희
    • Journal of Welding and Joining
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    • v.10 no.1
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    • pp.43-51
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    • 1992
  • The plastic zone formed around a notch tip is important in analyzing the fracture toughness of structures and particularly weld cracks existed in the weld HAZ (heat affected zone) which produces local plastic deformation at the crack tip. Therefore, in order to analyze the fracture toughness in weld HAZ, it is necessary to investigate the new fracture toughness parameter $K_{c}$ $^{*}$ and critical plastic strain energy $W_{p}$ $^{c}$ according to the shape and size of the plastic zone. 1) If the temperature corresponding to $K_{c}$ $^{*}$=130kg-m $m^{-3}$ 2/ is determined, transition temperature $T_{tr}$ the magnitude of plastic zone size, and heat input change depending on the fracture toughness. The blunted amounts of the parent and weld HAZ show mild linear variation until .delta.=0.4mm and then increase very steeply there after. 2) The relation between the plastic strain energy( $W^{p}$ ) and transition temperature( $T_{*}$tr) in parent metal is more sensitive than that of weld HAZ. However, the plastic strain energy depends on the transition temperature, and thus the yield stress, .sigma.$_{ys}$ becomes an important parameter for plastic strain energy. 3) The critical plastic strain energy( $W_{p}$ $^{c}$ ) absorbed by the plastic zone at the notch tip indicated in case of parent metal: 60J/mm, in case of heat input(20KJ/cm): 75J/mm, in case of heat input(30KJ/cm); 50J/mmJ/mm.

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Mechanical behavior of Beishan granite samples with different slenderness ratios at high temperature

  • Zhang, Qiang;Li, Yanjing;Min, Ming;Jiang, Binsong
    • Geomechanics and Engineering
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    • v.24 no.2
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    • pp.157-166
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    • 2021
  • This paper aims at the temperature and slenderness ratio effects on physical and mechanical properties of Beishan granite. A series of uniaxial compression tests with various slenderness ratios and temperatures were carried out, and the acoustic emission signal was also collected. As the temperature increases, the fracture aperture of intercrystalline cracks gradually increases, and obvious transcrystalline cracks occurs when T > 600℃. The failure patterns change from tensile failure mode to ductile failure mode with the increasing temperature. The elastic modulus decreases with the temperature and increases with slenderness ratio, then tends to be a constant value when T = 1000℃. However, the peak strain has the opposite evolution as the elastic modulus under the effects of temperature and slenderness ratio. The uniaxial compression strength (UCS) changes a little for the low-temperature specimens of T < 400℃, but a significant decrease happens when T = 400℃ and 800℃ due to phase transitions of mineral. The evolution denotes that the critical brittle-ductile transition temperature increases with slenderness ratio, and the critical slenderness ratio corresponding to the characteristic mechanical behavior tends to be smaller with the increasing temperature. Additionally, the AE quantity also increases with temperature in an exponential function.

The Effect of Specimen Size in Charpy Impact Testing (샬피 충격시험에 있어서 시험편 크기의 영향)

  • Kim, Hoon;Kim, Joo-Hark;Chi, Se-Hwan;Hong, Jun-Hwa
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.21 no.1
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    • pp.93-103
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    • 1997
  • Charpy V-notch impact tests were performed on the full-, half-and third-size specimens from two ferritic SA 508 Cl. 3 steels for nuclear pressure vessel. New normalization factors were proposed to predict the upper shelf energy(USE) and the ductile-brittle transition temperature(DBTT) of full-size specimens from the measured data on sub-size specimens. The factors for the USE and the DBTT are $(Bb^2/Kt); and; (Bb/R)^1/2/, $ respectively, where B the width, b the ligament size, $K_{t}$ the elastic stress concentration factor, and R the notch root radius. These correlations successfully estimated the USE and DBTT of the full-size specimens based on sub-size specimen data. In addition, the size effects were studied to develop the correlations among absorbed energy, lateral expansion(LE) and displacement. It was also found that the LE was able to be estimated from the displacement obtained by the instrumented impact test, and that the displacement would be used as a criterion for the toughness of the steels corresponding to change in their yield strength.h.

Strength Evaluation and Life Prediction of the Multistage Degraded Materials (다단계 모의 열화재의 재료강도 평가와 수명예측)

  • 권재도;진영준;장순식
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.9
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    • pp.2271-2279
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    • 1993
  • In the case of life prediction on the structures and machines after long service, it is natural to consider a degradation problems. Most of degradation data form practical structures are isolated data obtained at the time of periodical inspection or repair. From such data, it may be difficult to obtain the degradation curve available and necessary for life prediction. In this paper, for the purpose of obtaining a degradation curves, developed the simulate degradation method and fatigue test and Charpy impact test were conducted on the degraded, simulate degraded and recovered materials. Fatigue life prediction were conducted by using the relationship between fracture transition temperature (DBTT : vTrs) obtained from the Charpy impact test through the degradation process and fatigue crack growth constants of m and C obtained from the fatigue test.

Dislocation Behavior around Crack Tips in Single Crystal Alumina (단결정 알루미나의 균열첨단에서 전위거동)

  • Kim, Hyeong-Sun;Robers, S.G
    • Korean Journal of Materials Research
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    • v.4 no.5
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    • pp.590-599
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    • 1994
  • A work on the brittle to ductile transition (BDT) in single crystal alumina has been performed to understand and assess the dynamics of dislocation mobility around crack tip of brittle material. The critical stress intensity factor and yield strengths were obtained from bending test using precracked specimens at elevated temperatures. It was found that the BDT temperature was dependent on strain rate and orientation of specimen : for (1120) fracture surface, $1034^{\circ}C$, $1150^{\circ}C$ for $4.2 \times 10^{-6}$, $4.2 \times 10^{-7}s^{-1}$ respectively. Under a 4 point bending test, the moving distance of dislocation generated near crack front in ductile range is determined by an etch pits method. The velocity of dislocation in sapphire obtained from the double etching method was applied to modelling study.

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Simulation of impact toughness with the effect of temperature and irradiation in steels

  • Wang, Chenchong;Wang, Jinliang;Li, Yuhao;Zhang, Chi;Xu, Wei
    • Nuclear Engineering and Technology
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    • v.51 no.1
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    • pp.221-227
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    • 2019
  • One of the important requirements for the application of reduced activation ferritic/martensitic steel is to retain proper mechanical properties in irradiation and high temperature conditions. In order to simulate the impact toughness with the effect of temperature and irradiation, a simulation model based on energy balance method consisted of crack initiation, plastic propagation and cleavage propagation stages was established. The effect of temperature on impact toughness was analyzed by the model and the trend of the simulation results was basicly consistent with the previous experimental results of CLAM steels. The load-displacement curve was simulated to express the low temperature ductile-brittle transition. The effect of grain size and inclusion was analyzed by the model, which was consistent with classical experiment results. The transgranular-intergranular transformation in brittle materials was also simulated.

Effect of Thermal Aging on Microstructure and Mechanical Properties of China Low-Activation Martensitic Steel at 550℃

  • Wang, Wei;Liu, Shaojun;Xu, Gang;Zhang, Baoren;Huang, Qunying
    • Nuclear Engineering and Technology
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    • v.48 no.2
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    • pp.518-524
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    • 2016
  • The thermal aging effects on mechanical properties and microstructures in China low-activation martensitic steel have been tested by aging at $550^{\circ}C$ for 2,000 hours, 4,000 hours, and 10,000 hours. The microstructure was analyzed by scanning and transmission electron microscopy. The results showed that the grain size and martensitic lath increased by about $4{\mu}m$ and $0.3{\mu}m$, respectively, after thermal exposure at $550^{\circ}C$ for 10,000 hours. MX type particles such as TaC precipitated on the matrix and Laves-phase was found on the martensitic lath boundary and grain boundary on aged specimens. The mechanical properties were investigated with tensile and Charpy impact tests. Tensile properties were not seriously affected by aging. Neither yield strength nor ultimate tensile strength changed significantly. However, the ductile-brittle transition temperature of China low-activation martensitic steel increased by $46^{\circ}C$ after aging for 10,000 hours due to precipitation and grain coarsening.