• Title/Summary/Keyword: Dual Column

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Dual Capillary Column System for the Qualitative Gas Chromatography: 2. Comparison between Splitless and On-Column Injection Modes

  • Kim, Kyoung-Rae;Kim, Jung-Han;Park, Hyoung-Kook;Oh, Chang-Hwan
    • Bulletin of the Korean Chemical Society
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    • v.14 no.2
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    • pp.250-255
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    • 1993
  • A dual capillary column system is described for the simultaneous analysis of a given sample and measurement of retention index (RI) and area ratio (AR) values of each peak on two capillary columns of different polarity, DB-5 & DB-1701 from a single injection. Both capillary columns were connected to either a splitless injector or an on-column injector via a deactivated fused-silica capillary tubing of 1 m length and a 'Y' splitter. Both injection modes allowed to measure RI and AR values with high reproducibility (<0.01% RSD) and high accuracy (<10% RE), respectively with the exception that the trace and high boiling solutes required the on-column mode for the accurate quantification and AR comparison. When the dual capillary column system in on-column injection mode was applied to the blind samples containing organic acids, each acid was positively indentified by the combined computer RI library search-AR comparison.

Influence of dual layer confinement on lateral load capacity of stone columns: An experimental investigation

  • Akash Jaiswal;Rakesh Kumar
    • Geomechanics and Engineering
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    • v.32 no.6
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    • pp.567-581
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    • 2023
  • Enhanced vertical load capacity of the ground reinforced with the stone columns drew great attention by the researchers as it deals with many of the geotechnical difficulties associated with the weak ground. Recently, it has been found that the stone columns are also prone to fail under the shear load when employed beneath the embankments or the foundations susceptible to lateral loads. In this study, the effect of various encasement conditions on the lateral deflection of stone columns is investigated. A method of dual layers of encasement has been introduced and its the effect on lateral load capacity of the stone columns has been compared with those of the single encased stone column and the un-encased stone columns. Large shear box tests were utilised to generate the shear deformation on the soil system under various normal pressure conditions. The stiffness of the soil-stone column combined system has been compared for various cases of encasement conditions with different diameters. When subjected to lateral deformation, the encased columns outperformed the un-encased stone columns installed in loose sand. Shear stress resistance is up to 1.7 times greater in dual-layered, encased columns than in unencased columns. Similarly, the secant modulus increases as the condition changes from an unencased stone column to single-layer encasement and then to dual-layer encasement, indicating an improvement in the overall soil-stone column system.

A Low Power Dual CDS for a Column-Parallel CMOS Image Sensor

  • Cho, Kyuik;Kim, Daeyun;Song, Minkyu
    • JSTS:Journal of Semiconductor Technology and Science
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    • v.12 no.4
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    • pp.388-396
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    • 2012
  • In this paper, a $320{\times}240$ pixel, 80 frame/s CMOS image sensor with a low power dual correlated double sampling (CDS) scheme is presented. A novel 8-bit hold-and-go counter in each column is proposed to obtain 10-bit resolution. Furthermore, dual CDS and a configurable counter scheme are also discussed to realize efficient power reduction. With these techniques, the digital counter consumes at least 43% and at most 61% less power compared with the column-counters type, and the frame rate is approximately 40% faster than the double memory type due to a partial pipeline structure without additional memories. The prototype sensor was fabricated in a Samsung $0.13{\mu}m$ 1P4M CMOS process and used a 4T APS with a pixel pitch of $2.25{\mu}m$. The measured column fixed pattern noise (FPN) is 0.10 LSB.

Dynamic Adsorptive Characteristics of Dual Adsorbents Bed Packed with Activated Carbon and Zeolite 13X for Benzene Adsorption (활성탄 및 제올라이트 13X를 충진한 이중흡착층 내에서 벤젠의 동적흡착 특성)

  • Kang, Sung-Won;Suh, Sung-Sup;Min, Byung-Hoon
    • Clean Technology
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    • v.10 no.3
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    • pp.159-168
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    • 2004
  • Benzene adsorption experiment was carried out for activated carbon and zeolite 13X adsorbents. Single column and dual column packed with two adsorbents were used to investigate the dynamic adsorptive characteristics. Effect of feed flow rate on the breakthrough curve was not significant. Specific adsorption amount of benzene for activated carbon was larger than that for zeolite 13X. On the contrary, adsorption amount per column volume was larger for zeolite 13X column because the density of zeolite 13X was larger. In the dynamic experiment using dual adsorbents column, length of mass transfer zone was changed by the feed direction. Breakthrough time was longer and breakthrough curve was sharper when activated carbon was packed in feed inlet and zeolite 13X was packed in column outlet. Also breakthrough time and breakthrough curve slope were affected by the packing ratio of the two adsorbents.

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Mechanical behavior of outer square inner circular concrete-filled dual steel tubular stub columns

  • Ding, Fa-xing;Wang, Wenjun;Liu, Xue-mei;Wang, Liping;Sun, Yi
    • Steel and Composite Structures
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    • v.38 no.3
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    • pp.305-317
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    • 2021
  • The mechanical behavior of the outer square inner circular concrete-filled dual steel tubular (SCCFT) stub columns under axial compression is investigated by means of experimental research, numerical analysis and theoretical investigation. Parameters such as diameter ratio, concrete strength and steel ratio were discussed to identify their influence on the mechanical properties of SCCFT short columns on the basis of the experimental investigation of seven SCCFT short columns. By establishing a finite element model, nonlinear analysis was performed to discuss the longitudinal and transverse stress of the dual steel tubes. The longitudinal stress characteristics of the core and sandwich concrete were also analyzed. Furthermore, the failure sequence was illustrated and the reasonable cross-section composition of SCCFT stub column was proposed. A formula to predict the axial load capacity of SCCFT stub column was advanced and verified by the results from experiment and the finite element.

Analysis of PCBs in Food by Dual Column-HRGC/ECD (Dual Column-HRGC/ECD를 이용한 식품 중 PCBs 오염 실태조사)

  • Suh, Junghyuck;Kim, Jungmi;Hong, Mooki;Kim, Changmin;Choi, Dongmi
    • Analytical Science and Technology
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    • v.16 no.2
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    • pp.166-173
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    • 2003
  • To determine levels of PCBs in food, beef, pork, chicken, egg, mackerel, yellow croaker, anchovy, common squid and little neck clam were chosen and collected at markets in Seoul, Busan and Kwangju. Among 209 PCB congeners, 7 congeners (#28, #52, #101, #118, #138, #153 and #180) were selected as target compounds that were known as indicator congeners. Samples were homogenized, treated in alkali solution for 1 hour, and extracted with organic solvents. After extraction, extracts were cleaned up by sulfuric acid, purified on silica gel column chromatography, analyzed by dual column-HRGC/ECD and then confirmed by HRGC/MSD. As results, PCBs were detected in fish samples ranged from 0.0002 to 0.001 mg/kg. Both PCB #101 and PCB #118 were the major contributors among 7 congeners.

Experimental investigations on resilient beam-column end-plate connection with structural fuse

  • Arunkumar Chandrasekaran;Umamaheswari Nambiappan
    • Steel and Composite Structures
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    • v.47 no.3
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    • pp.315-337
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    • 2023
  • The steel structure is an assembly of individual structural members joined together by connections. The connections are the focal point to transfer the forces which is susceptible to damage easily. It is challenging to replace the affected connection parts after an earthquake. Hence, steel plates are utilised as a structural fuse that absorbs connection forces and fails first. The objective of the present research is to develop a beam-column end plate connection with single and dual fuse and study the effect of single fuse, dual fuse and combined action of fuse and damper. In this research, seismic resilient beam-column end plate connection is developed in the form of structural fuse. The novel connection consists of one main fuse was placed horizontally and secondary fuse was placed vertically over main fuse. The specimens are fabricated with the variation in number of fuse (single and dual) and position of fuse (beam flange top and bottom). From the fabricated ten specimens five specimens were loaded monotonically and five cyclically. The experimental results are compared with Finite Element Analysis results of Arunkumar and Umamaheswari (2022). The results are critically assessed in the aspect of moment-rotation behaviour, strain in connection components, connection stiffness, energy dissipation characteristics and ductility. While comparing the performance of total five specimens, the connection with fuse exhibited superior performance than the conventional connection. An equation is proposed for the moment of resistance of end-plate connection without and with structural fuse.

Design and Evaluation of a CMOS Image Sensor with Dual-CDS and Column-parallel SS-ADCs

  • Um, Bu-Yong;Kim, Jong-Ryul;Kim, Sang-Hoon;Lee, Jae-Hoon;Cheon, Jimin;Choi, Jaehyuk;Chun, Jung-Hoon
    • JSTS:Journal of Semiconductor Technology and Science
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    • v.17 no.1
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    • pp.110-119
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    • 2017
  • This paper describes a CMOS image sensor (CIS) with dual correlated double sampling (CDS) and column-parallel analog-to-digital converter (ADC) and its measurement method using a field-programmable gate array (FPGA) integrated module. The CIS is composed of a $320{\times}240$ pixel array with $3.2{\mu}m{\times}3.2{\mu}m$ pixels and column-parallel 10-bit single-slope ADCs. It is fabricated in a $0.11-{\mu}m$ CIS process, and consumes 49.2 mW from 1.5 V and 3.3 V power supplies while operating at 6.25 MHz. The measured dynamic range is 53.72 dB, and the total and column fixed pattern noise in a dark condition are 0.10% and 0.029%. The maximum integral nonlinearity and the differential nonlinearity of the ADC are +1.15 / -1.74 LSB and +0.63 / -0.56 LSB, respectively.

Dual-Sensitivity Mode CMOS Image Sensor for Wide Dynamic Range Using Column Capacitors

  • Lee, Sanggwon;Bae, Myunghan;Choi, Byoung-Soo;Shin, Jang-Kyoo
    • Journal of Sensor Science and Technology
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    • v.26 no.2
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    • pp.85-90
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    • 2017
  • A wide dynamic range (WDR) CMOS image sensor (CIS) was developed with a specialized readout architecture for realizing high-sensitivity (HS) and low-sensitivity (LS) reading modes. The proposed pixel is basically a three-transistor (3T) active pixel sensor (APS) structure with an additional transistor. In the developed WDR CIS, only one mode between the HS mode for relatively weak light intensity and the LS mode for the strong light intensity is activated by an external controlling signal, and then the selected signal is read through each column-parallel readout circuit. The LS mode is implemented with the column capacitors and a feedback structure for adjusting column capacitor size. In particular, the feedback circuit makes it possible to change the column node capacitance automatically by using the incident light intensity. As a result, the proposed CIS achieved a wide dynamic range of 94 dB by synthesizing output signals from both modes. The prototype CIS is implemented with $0.18-{\mu}m$ 1-poly 6-metal (1P6M) standard CMOS technology, and the number of effective pixels is 176 (H) ${\times}$ 144 (V).