• 대한치과교정학회지
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• 제32권4호
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• pp.293-300
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• 2002

본 연구의 목적은 산부식된 법랑질에 수분이나 타액이 오염되어도 적절한 접착력을 얻을 수 있다고 소개된 교정용 친수성 프라이머를 이용한 교정용 브라켓 접착시 타액 오염 정도에 따른 전단결합강도와 접착 파절 양상을 기존의 소수성 프라이머와 비교함으로써 임상적 유용성을 평가하는 것이다. 사람의 소구치를 강철 원통에 교정용 레진으로 포매하여 만든 시편에 기존의 소수성인 Transbond XT primer와 친수성인 Transbond MIP primer각각에 대하여 광중합형 접착 레진으로 브라켓을 접착시, 인공 타액을 이용한 오염정도에 따른 전단결합강도를 만능시험기로 측정하고, 접착 파절 양상을 stereomicroscope로 관찰하여 다음과 같은 결과를 얻었다. 1. 건조 상태에서 Transbond XT primer와 Transbond MIP primer의 전단결합강도는 유의한 차이가 없었다. 2. 타액 오염시 그 정도에 상관없이 Transbond MIP primer는 Transbond XT primer에 비해 유의하게 높은 전단결합 강도를 나타냈다(p<0.001). 3. Transbond MIP primer는 한 겹의 타액 오염시 건조 상태와 전단결합강도의 유의한 차이가 없었으나, 두 겹의 타액 오염시에는 유의하게 낮은 결합강도를 나타냈다(p<0.01). 4. 접착 파절 형태는 타액 오염의 정도에 따라 평균 접착제 잔류 지수가 낮아지는 경향을 나타냈다. Transbond MIP primer는 타액 오염시에도 반 이상이 브라켓-레진 계면에서의 파절을 보였으나, Transbond XT primer는 타액 오염시 대부분의 경우 레진-법랑질 계면에서의 파절을 나타냈다. 이상의 실험 결과, 교정용 친수성인 Transbond MIP primer는 수분 조절이 어려운 임상 상황에서 적절한 결합강도를 얻을 수 있는 좋은 방법으로 생각된다.

• International Journal of Aeronautical and Space Sciences
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• 제13권2호
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• pp.229-237
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• 2012

In this study, the failure mechanism of sandwich-to-laminate T-joints under pull-off loading was investigated by experiment and the finite element method. A total of 26 T-joint specimens were manufactured and tested in order to investigate the effects of both adhesive thickness (0.4, 2.0, and 4.0 mm) and environmental conditions on the failure of the joints. The results showed that failure occurred mainly as intralaminar failure in the first layer of the sandwich face, which was contacted to the paste adhesive. The failure load did not significantly change with increasing adhesive thickness in both RTD (Room Temperature and Dry) and ETW (Elevated Temperature and Wet) conditions. In the case of ETW conditions, however, the failure load increased slightly with an increase in adhesive thickness. The joints tested in ETW conditions had higher failure loads than those tested in RTD conditions. In addition to the experiment, a finite element analysis was also conducted to investigate the failure of the joint. The stress inside the first ply of the sandwich face was of interest because during the experiment, failure always occurred there. The analysis results showed good agreement with the trend of experimental results, except for the case of the smallest adhesive thickness. The highest stress was predicted in the regions where initial failure was observed in the experiment. The maximum stress was almost constant when the adhesive thickness was beyond 2 mm.

• Journal of the Korean Wood Science and Technology
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• 제39권6호
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• pp.498-504
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• 2011

The purpose of this study was to investigate and develop an eco-frendly wood adhesive based on vegetable oil (especially soybean oil), the renewable and sustainable natural resources, using ozonification technology for the chemical structure modification. The waste soybean oil (WSBO) was reacted with $O_3$ at the rate of $450m{\ell}$(acetone) : $50m{\ell}$ (WSBO) for different times, 1, 2, 3 hrs. The investigation of the modified chemical strecture of the ozonied WSBOs were conducted using FT-IR. As ozonification time increased, the peak of the unsaturated double bonds was disappeared especially ozonized-3hrs and aldehyde or carboxyl peak appeared because ozonification broke the oil into small molecules. The plywood were made at $150^{\circ}C$ with 4 minutes hot-press time using the different ozonized 3 hrs WSBO/pMDI adhesives and were tested for the dry, wet, cyclic boil test according to the Korea Industrial Standard F3101 Ordinary plywood. The bond strengths gradually increased until 1 : 0.5~1 : 3, but it decreased 1 : 4, as the contents of pMDI increased. The results of the dry, wet and cyclic bond strengths the equivalent ratio was formed approximately between 1 : 2~1 : 3. And the 1 : 1~1 : 4 strengths met constantly the standard requirement of 7.0kgf/$cm^2$ (KS F3101). From the comprehensive view on the results of above experiment, it could be confirmed that ozonized WSBO/pMDI has characteristics of effective reactivity and wet stability showed as an excellent candidate of wood adhesive applications.

• Restorative Dentistry and Endodontics
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• 제38권4호
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• pp.234-240
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• 2013

Objectives: This study evaluated the effects of intraradicular moisture on the pushout bond strength of a fibre post luted with several self-adhesive resin cements. Materials and Methods: Endodontically treated root canals were treated with one of three luting cements: (1) RelyX U100, (2) Clearfil SA, and (3) G-Cem. Roots were then divided into four subgroups according to the moisture condition tested: (I) dry: excess water removed with paper points followed by dehydration with 95% ethanol, (II) normal moisture: canals blot-dried with paper points until appearing dry, (III) moist: canals dried by low vacuum using a Luer adapter, and (IV) wet: canals remained totally flooded. Two 1-mm-thick slices were obtained from each root sample and bond strength was measured using a push-out test setup. The data were analysed using a two-way analysis of variance and the Bonferroni post hoc test with p = 0.05. Results: Statistical analysis demonstrated that moisture levels had a significant effect on the bond strength of luting cements (p < 0.05), with the exception of G-Cem. RelyX U100 displayed the highest bond strength under moist conditions (III). Clearfil SA had the highest bond strength under normal moisture conditions (II). Statistical ranking of bond strength values was as follows: RelyX U100 > Clearfil SA > G-Cem. Conclusions: The degree of residual moisture significantly affected the adhesion of luting cements to radicular dentine.

• 문화기술의 융합
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• 제8권5호
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• pp.749-754
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• 2022

다양한 의료 응용 분야에서 웨어러블 및 피부 부착형 전자 패치에 피부 표면의 높은 접착력과 내수성이 요구된다. 본 연구에서는 탄소 기반 전도성 고분자 복합 소재에 개구리 발바닥의 육각 채널와 문어 빨판의 흡착 구조 패턴을 모사한 신축성 있는 전자 패치를 보고한다. 개구리의 발바닥을 모사한 육각 채널 구조는 수분을 배수하며, 균열억제 효과를 통해 점착력을 향상 시키며, 문어 빨판을 모사한 흡착 구조는 젖은 표면에서 높은 점착력을 나타낸다. 또한 고점착 전자패치는 실리콘(max. 4.06 N/cm²), 피부 복제 표면(max. 1.84 N/cm²) 등 다양한 표면에 건조 및 젖은 조건에서 우수한 접착력을 가지고 있다. 고분자 매트릭스와 탄소 입자를 기반으로한 고분자 복합소재를 통해 제작된 고점착 전자 패치는 건조 및 습한 환경에서 심전도(ECG)을 안정적으로 감지할 수 있다. 이 연구에서 보여진 특성을 기반으로 제안된 전자 패치는 다양한 생체 신호의 진단을 위한 웨어러블 및 피부 부착 센서 디바이스를 구현하는 잠재적 응용 가능성을 제시한다.

• 대한전자공학회:학술대회논문집
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• 대한전자공학회 2008년도 하계종합학술대회
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• pp.379-380
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• 2008

This paper presents a wafer-level package using a Dry Film Resist(DFR) for RF MEMS devices. Vertical interconnection is made through the hole formed on the glass cap. Bonding using the DFR has not only less effects on the surface roughness but also low process temperature. We used DFR as adhesive polymer and made the vertical interconnection through Au electroplating. Therefore, we developed a wafer-level package that is able to be used in RF MEMS devices and vertical interconnection.

• Restorative Dentistry and Endodontics
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• 제21권1호
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• pp.321-338
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• 1996

The purpose of this study was to evaluate the effect of moistening and air-drying of acid conditioned dentin and enamel on the marginal microleakage. In this study, Class V cavity were prepared on both buccal and lingual surface of sixty extracted human premolars with cementum margin. These specimens were randomly devided into three groups and three dentin adhesives(Scotchbond Multi-Purpose, All bond 2, Prisma Universal Bond 3) were applied to each group. The specimens in each group were subdevided into four groups (Wet/primed, Dry/primed, Wet/not primed, Dry/not primed) and the etched dentin and enamel surface were treated these four surface treatments prior to the placement of a bonding agent or adhesive. Wet/primed group was simply blot-dried with a damp facial tissue before primer placement ; Dry/primed group was air dried for 30 seconds before the placement of a primer ; Wet/not primed group and Dry/not primed group were not primed after blot dried and air dried for 30 seconds each group. The bonding agent and composite resin were applied for each group. All specimens were exposed to 500 cycle of thermal stress. Specimens were placed in a silver nitrate solution and then sectioned buccolingually through the center of the restoration. The dye penetrations of the specimens were observed with a stereo microscope. The statistical test were applied to the results using a one way analysis variance (ANOVA) and Duncan's multiple range test. The aspects of silver ion penetration into the resin/dentin interface were examined under scanning electron microscopy. The results were as follows. 1. In all groups, the enamel margin showed significantly lower leakage value than the cementum margin (p<0.05). 2. Regardless of various surface treatment and dentin adhesives, there was no significant difference at the enamel margins (p>0.05). 3. At the dentin margins, the leakage values of Dry/not primed group showed significantly higher than that of the other groups (p<0.05). The leakage values of Wet/primed group showed significantly lower than that of the other groups, but, there was no significant difference between Wet group and Dry group. 4. There was no significantly difference between the dentin adhesives regarding the surface treatments in all groups(p>0.05). 5. On the backscatterd scanning electron microscopy observation, the penetration of the silver ion occured at the bonding resin/dentin interface. In the Wet/primed group, resindentin hybrid zone and resin penetration into the dentin was observed. The resin tags were compactively formed to a thickness of $3\sim4{\mu}m$ at the upper part of dentinal tubules. In the Dry/primed group, the thickness of the hybrid zone and the diameter, depth of the resin tags diminished. In the Non-primed groups, the hybrid zone was not identified and few resin tag was observed. There was the gap formation in the resin/dentin interface.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2008년도 추계 학술논문 발표대회
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• pp.49-52
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• 2008

The present study was to develop a dry PFB method similar to the existing gypsum board construction method in order to apply the existing wet PFB method that uses fire-resistant adhesive. It was found that the existing wet method can produce concrete compressive strength of 80MPa and fire resistance of 3 hours with 30mm PF boards. The goal of development in this study was fire resistance of 3 hours through dry construction of 15mm fire-resistant boards. 1. Improved PF board was prepared by adding inorganic fiber to existing board and using aggregate with grain size of 3mm or less. Molding was done at temperature higher than that for existing PF board molding. While wet curing is used for existing PF boards, this study used dry curing in order to enhance heat insulation performance. 2. According to the results of fire resistance test, when the dry PF method was applied, the temperature of the main reinforcing bar was 116℃ in 15mm, 103.8℃ in 20mm, and 94℃ in 25mm, and these results satisfied the current standards for fire resistance control presented by the Ministry of Land, Transport and Maritime Affairs. When a 3-hour fire resistance test was performed and the external properties of the specimen were examined, the outermost gypsum board hardly remained and internal PF board maintained its form without thermal strain.

• Animal cells and systems
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• 제13권2호
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• pp.161-167
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• 2009

The cuticle of spider's exoskeleton is a hydrophobic and non-adhesive material, but the jumping spiders have the distinctive attachment apparatus for adhesion on smooth dry surface without sticky fluids. We have examined the whole tarsal appendages of the jumping spider, Plexippus setipes with using scanning electron microscope to reveal the fine structural characteristics of the dry adhesion system. All eight legs have the scopulae with a pair of claws on the tip of feet. Each scopula is composed of two groups of setae that are capable of dry adhesion on smooth surface, and the hook structure of the claw is advanced to move on the rough surface. The setae toward the bottom of the tarsal segment are densely covered by numerous setules on the underside which broadened from middle to distal portion. It has been revealed by this research that the contact area of the setule is always a triangular shape, and these cuticular surfaces are connected by the elongated stalks from the underlying setae. It is likely that the nano-scale structures including a triangular depression and a longitudinal groove on each setule could functionate when the spider detach its feet from the substrate.

• 한국구조물진단유지관리공학회 논문집
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• 제12권2호
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• pp.67-74
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• 2008

본 연구에서는 탄소섬유접착보강공법의 박리와 연관한 부착특성에 대하여 검토하였다. 그 결과를 요약하면, 온도변화에 따른 변형 특성에서는 바탕 콘크리트의 강도에 관계없이 온도 변화에 따라서 각 재료들의 변형 폭도 커지는 것을 알 수 있었다. 초음파 전파 속도도 온도변화에 따라 작아지는 것으로 나타나 계면에서 박리가 발생하였음을 알 수 있었다. 부착강도는 온도 변화가 클수록 부착강도의 값은 작아지는 것으로 나타났는데, 파괴형태는 계면파괴와 모재파괴 형태로 나타났다. 건습 변화에 따라서는 4사이클까지 각 재료의 변형 및 초음파 전파 속도에서 큰 변화를 나타내지 않아 건습 자체의 반복에는 큰 영향이 없는 것으로 판단된다. 단, 부착강도는 40%정도 저하하는 것으로 나타났지만 비교적 양호한 강도를 나타내었다. 동결융해 시험결과는 온도변화 요인과 유사한 경향으로서 동결융해 작용을 받을 경우 4사이클 이내에 박리가 일어날 수 있는 것으로 분석되었다.